• Title/Summary/Keyword: Heating Period

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Synchrotron SAXS Study on the Micro-Phase Separation Kinetics of Segmented Block Copolymer

  • Lee, Han-Sup;Yoo, So-Ra;Seo, Seung-Won
    • Fibers and Polymers
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    • v.2 no.2
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    • pp.98-107
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    • 2001
  • The phase transition behavior isothermal micro-phase separation kinetics of polyester-based thermoplastic elastomer were studied using the synchrotron X-ray scattering(SAXS) method. The structural changes occurring during heating period were investigated by determining the changes of the one-dimensional correlation function, interfacial thickness and Porod constant. Based on the abrupt increases of the domain spacing and interfacial thickness, a major structural change occurring well below the melting transition temperature is suggested. Those changes are explained in terms of melting of the thermodynamically unstable hard domains or/and the interdiffusion of the hard and soft segments in the interfacial regions. SAXS profile changes during the micro-phase separation process were also clearly observed at various temperatures and the separation rate was found to be sensitively affected by the temperature. The peak position of maximum scattering intensity stayed constant during the entire course of the phase separation process. The scattering data during the isothermal phase separation process was interpreted with the Cahn-Hilliard diffusion equation. The experimental data obtained during the early stage of the phase separation seems to satisfy the Cahn-Hilliard spinodal mechanism. The transition temperature obtained from the extrapolation of the diffusion coefficient to zero value turned out to be about 147$\pm$$2^{\circ}$, which is close to the order-disorder transition temperature obtained from the Porod analysis. The transition temperature was also estimated from the inveriant growth rate. By extrapolating the inveriant growth rate to zero, a transition temperature of about 145$\pm$$\pm$$2^{\circ}$ was obtained.

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Seismic behaviors of twin tunnel with flexible segment (Flexible Segment가 설치된 병렬터널의 지진시 동적거동)

  • Kwak, Chang-Won;Park, Inn-Joon
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.17 no.6
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    • pp.695-702
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    • 2015
  • Recently, the improvement of mechanical and theoretical issues in geo-centrifuge test enhances the applicability and accuracy of the test. Geo-centrifuge test is appropriate to simulate the behaviors of underground structures like tunnel, since tunnel interacts with the soil and/or rock around it and the test can embody the in-situ stress conditions effectively. In this study, the seismic behaviors of twin tunnel were analyzed based on geo-centrifuge test. Flexible segment to mitigate seismic acceleration were implemented in the model with thin and thick thickness. Based on the test results, it was found that flexible segment can decrease the peak acceleration generally, however, thin flexible segment was not able to reduce peak acceleration in short-period seismic wave. Thick flexible segment was more effective in case of high bedrock acceleration condition. Additionally, 3-dimensional numerical analysis was performed to verify the characteristics of seismic behavior and the effect of flexible segment. Consequently, the numerical analysis result showed good agreement with the test result.

OSL Age Determination of the Hearths in a Bronze Age Dwelling Site by using Bayesian Statistics (베이지안 통계학을 이용한 청동기시대 주거지내 화덕자리들의 광자극발광(OSL) 연대 결정)

  • Kim, Myung-Jin;Yang, Hye-Jin;Hong, Duk-Geun
    • Journal of Radiation Protection and Research
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    • v.36 no.2
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    • pp.52-58
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    • 2011
  • OSL dating for three hearths having the sequence of use and discard in No. 29 and 29-1 dwelling sites at Sogol cultural site was carried out. Resulting from the deconvolution of natural CW-OSL decay curve and thermal zeroing test, it was turned out that OSL signal was entirely composed of the heat- and light-sensitive fast component with high photoionization cross-section and all quartz OSL signals were thermally bleached under $300^{\circ}C$ which is the minimum temperature related to heating and cooking in Bronze age. After dose recovery test and plateau test, paleodose of each hearth sample was evaluated by using SAR method, and OSL age was determined from the ratio of paleodose to annual dose rate. For the purpose of the precision improvement of OSL age, Bayesian statistics was applied to each hearth's age and the archaeological sequence information. Finally, it could be concluded to the accurate use period of each hearth from the resultant OSL ages.

Microwave assisted processing of silver thick films for microelectronic applications

  • Rane, Sunit;Bhatkar, Rushna;Mulik, Uttam;Amalnerkar, Dinesh
    • Advances in materials Research
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    • v.2 no.3
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    • pp.133-140
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    • 2013
  • This paper aims to focus on the microwave processing of thick films which is a fast, cheap technique and could be the alternative to the currently used conventional high temperature processing technique. Microwave processing has gained worldwide acceptance as a novel method for heating and sintering a variety of materials, as it offers specific advantages in terms of speed, energy efficiency, process simplicity, finer microstructures and lower environmental hazards. Silver conducting thick films were prepared and processed in the household microwave oven. The films sintered at different time period by keeping the other parameter such as microwave power, film thickness etc constant. The microstructure analysis revealed that the surface morphology of the microwave processed films become compact with respect to the processing time. The sheet resistance for microwave sintered silver films is in the range of 0.003 to $1.207{\Omega}/{\Box}$ where as the films fired at 750 and $850^{\circ}C$ showed the resistance of 0.009 and $0.003{\Omega}/{\Box}$ which can be comparable. The results revealed that the microstructure of the microwave sintered films has more uniform and compact surface than that of the conventionally fired films. The paper reports upon the preparation of silver thick film by screen printing technique and processing the same by microwave which also compared with the conventionally processed thick films.

Dynamics Associated with Prolonged Ensiling and Aerobic Deterioration of Total Mixed Ration Silage Containing Whole Crop Corn

  • Wang, Huili;Ning, Tingting;Hao, Wei;Zheng, Mingli;Xu, Chuncheng
    • Asian-Australasian Journal of Animal Sciences
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    • v.29 no.1
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    • pp.62-72
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    • 2016
  • This study investigated the dynamics associated with prolonged ensiling and aerobic deterioration of whole crop corn (WCC) silages and total mixed ration (TMR) silages containing WCC (C-TMR silages) to clarify the differences that account for the enhanced aerobic stability of TMR silages. Laboratory-scale barrel silos were randomly opened after 7, 14, 28, and 56 d of ensiling and were subjected to analyses of fermentation quality, microbial and temperature dynamics during aerobic exposure. WCC and C-TMR silages were both well preserved and microorganisms were inhibited with prolonged ensiling, including lactic acid bacteria. Yeast were inhibited to below the detection limit of 500 cfu/g fresh matter within 28 d of ensiling. Aerobic stability of both silages was enhanced with prolonged ensiling, whereas C-TMR silages were more aerobically stable than WCC silages for the same ensiling period. Besides the high moisture content, the weak aerobic stability of WCC silage is likely attributable to the higher lactic acid content and yeast count, which result from the high water-soluble carbohydrates content in WCC. After silo opening, yeast were the first to propagate and the increase in yeast levels is greater than that of other microorganisms in silages before deterioration. Besides, increased levels of aerobic bacteria were also detected before heating of WCC silages. The temperature dynamics also indicated that yeast are closely associated with the onset of the aerobic deterioration of C-TMR silage, whereas for WCC silages, besides yeast, aerobic bacteria also function in the aerobic deterioration. Therefore, the inclusion of WCC might contribute to the survival of yeast during ensiling but not influence the role of yeast in deterioration of C-TMR silages.

The Analysis of Changma Structure using Radiosonde Observational Data from KEOP-2007: Part I. the Assessment of the Radiosonde Data (KEOP-2007 라디오존데 관측자료를 이용한 장마 특성 분석: Part I. 라디오존데 관측 자료 평가 분석)

  • Kim, Ki-Hoon;Kim, Yeon-Hee;Chang, Dong-Eon
    • Atmosphere
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    • v.19 no.2
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    • pp.213-226
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    • 2009
  • In order to investigate the characteristics of Changma over the Korean peninsula, KEOP-2007 IOP (Intensive Observing Period) was conducted from 15 June 2007 to 15 July 2007. KEOP-2007 IOP is high spatial and temporal radiosonde observations (RAOB) which consisted of three special stations (Munsan, Haenam, and Ieodo) from National Institute of Meteorological Research, five operational stations (Sokcho, Baengnyeongdo, Pohang, Heuksando, and Gosan) from Korea Meteorological Administration (KMA), and two operational stations (Osan and Gwangju) from Korean Air Force (KAF) using four different types of radiosonde sensors. The error statistics of the sensor of radiosonde were investigated using quality control check. The minimum and maximum error frequency appears at the sensor of RS92-SGP and RS1524L respectively. The error frequency of DFM-06 tends to increase below 200 hPa but RS80-15L and RS1524L show vice versa. Especially, the error frequency of RS1524L tends to increase rapidly over 200 hPa. Systematic biases of radiosonde show warm biases in case of temperature and dry biases in case of relative humidity compared with ECMWF (European Center for Medium-Range Weather Forecast) analysis data and precipitable water vapor from GPS. The maximum and minimum values of systematic bias appear at the sensor of DFM-06 and RS92-SGP in case of temperature and RS80-15L and DFM-06 in case of relative humidity. The systematic warm and dry biases at all sensors tend to increase during daytime than nighttime because air temperature around sensor increases from the solar heating during daytime. Systematic biases of radiosonde are affected by the sensor type and the height of the sun but random errors are more correlated with the moisture conditions at each observation station.

Effect of urbanization on the light precipitation in the mid-Korean peninsula (한반도 중부지역에서 약한 강수에 미치는 도시화 효과)

  • Eun, Seung-Hee;Chae, Sang-Hee;Kim, Byung-Gon;Chang, Ki-Ho
    • Atmosphere
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    • v.21 no.3
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    • pp.229-241
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    • 2011
  • The continuous urbanizations by a rapid economic growth and a steady increase in population are expected to have a possible impact on meteorology in the downwind region. Long-term (1972~2007) trends of precipitation have been examined in the mid-Korean peninsula for the westerly condition only, along with the sensitivity simulations for a golden day (11 February 2009). During the long-term period, both precipitation amount (PA) and frequency (PF) in the downwind region (Chuncheon, Wonju, Hongcheon) of urban area significantly increased for the westerly and light precipitation ($PA{\leq}1mm\;d^{-1}$) cases, whereas PA and PF in the mountainous region (Daegwallyeong) decreased. The enhancement ratio of PA and PF for the downwind region vs. urban region remarkably increased, which implies a possible urbanization effect on downwind precipitation. In addition, the WRF simulation applied for one golden day demonstrates enhanced updraft and its associated convergence in the downwind area (about 60 km), leading to an increase in the cloud mixing ratio. The sensitivity experiments with the change in surface roughness demonstrates a slight increase in cloud water mixing ratio but a negligible effect on precipitation in the upwind region, whereas those with the change in heat source represents the distinctive convergence and its associated updraft in the downwind region but a decrease in liquid water, which may be attributable to the evaporation of cloud droplet by atmospheric heating induced by an increase in an anthropogenic heat. In spite of limitations in the observation-based analysis and one-day simulation, the current result could provide an evidence of the effect of urbanization on the light precipitation in the downwind region.

Exothermic Curing System with Hot Wire in Cold Weather (열선을 사용하는 동절기 발열양생 평가시스템 개발)

  • Lee, Tae-Gyu;Lee, Jin-Sun
    • The Journal of the Korea Contents Association
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    • v.16 no.1
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    • pp.52-59
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    • 2016
  • For almost of concrete structures by placing in cold weather, it is very important that the selection of curing method at early aged construction stage. The Exothermic curing method with hot wire and rapid hardening cement is used mostly to prevent the initial cracks and the strength decrease. Most of the construction sites, however, have not been applied to the optimal curing method caused by the simple approaches and the empirical judgements. Therefore, this paper has proposed a evaluation algorithm of the exothermic curing method for representing heating temperature, period, position of hot wire by analyzing the transient heat transfer solution. This has been implemented, moreover, using an object oriented programming language to develop structural analysis system taking account risk parameters. This system is composed of input module, database module, database store module, analysis module, and result generation module. Linkage interface between the central database and each of the related module is implemented by the visual c# concept. Graphic user interface and the relational database table are supported for user's convenience.

A Study on the Short-Term Plan of Structural Reinforcing and the Temporary Housing Supply Strategy through the Analysis of the Status of North Korean Standard Housing

  • Kim, Seong Eun;Kim, Seung Hun;Lee, Yong Taeg
    • Architectural research
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    • v.20 no.3
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    • pp.83-92
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    • 2018
  • Recently, there has been inter-Korean exchanges are active, in company with an assertive international activity with North Korea and inter-Korean Summits. Thus, there is a growing possibility of Korean reunification. However, when the unification situation occurs, population inflow by North Korean residents will be expected, and it will be necessary to prepare a housing supply strategy. In addition, even if North Koreans are prevented from entering, a plan is necessary to ensure structural safety since most buildings in North Korea are aging and a recent natural disaster occurs frequently. In this research, we will try to present a temporary housing supply strategy and a short-term structural reinforcement plan based on analysis of the standard housing conditions in North Korea. In this research, we represent the analysis result of the existing construction level, supply status and structural performance of North Korea. When we consider the reinforcement period and social costs, a short-term reinforcement plan is recommended rather than the full reinforcement of the aged housing in North Korea. Furthermore, we examine the ways to secure the residential safety of North Koreans through a case study of domestic and overseas temporary residential facilities, until the permanent residential facilities were supplied. According to the analysis, the tent houses were used as a form of relief housing in overseas frequently. However, the tent house is difficult to apply for domestic country with clear seasons due to insulation and heating problems. Therefore, it is appropriate to develop a residential supply strategy as focusing on the temporary housing facilities in assembled or container from, in preparation for the future population inflow.

A Case Study on the Economic Analysis for an Advanced Technology-Based HYAC System Using LCC Technique (LCC 기법을 이용한 신기술 냉 $\cdot$ 난방 공조설비 시스템의 경제성 분석에 관한 사례연구)

  • Kim Yong-Su;Hwang Seong-Su
    • Korean Journal of Construction Engineering and Management
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    • v.6 no.2 s.24
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    • pp.129-138
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    • 2005
  • The purpose of this study is to assess economic effects for an advanced technology-based HVAC system. The study has been performed using LCC technique for the economic analysis. Data for LCC analysis are collected from estimation and interview of estimators and maintenance experts of buildings. Based on the LCC analysis, the economic effect of a new HVAC system has been predicted as follows : for the investment during 15 years of study period, (1) $21.6\%$ of LCC saving is predicted, (2) return rate for the investment is 4.8 times in case of new construction, and 14.4 times in case of building remodelling.