• The Korean Journal of Ceramics
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• v.3 no.3
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• pp.191-194
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• 1997

Epitaxial Pb(Zr, Ti)O3(PZT) thin films were prepared on MgO(100) substrates by dipping-pyrolysis (DP) process using metal naphthenates as starting materials, and effects of pyrolysis and final heat-treatment conditions on the film's orientation were investigated. Solid-state epitaxial growth of PZT proceeds at lower temperature around 650℃ from the precursor pyrolyzed at 350 and 500℃. The in-plane alignment of the PZT films depends not only on the final heat-treatment temperature but on the pyrolysis conditions; the films, pyrolyzed at a higher temperature for a short time, i.e., at 500℃ for 10 min, exhibited stronger orientation after the same final heat treatment at 650°∼750℃. The PZT films with the strongest orientation were prepared by pyrolysis under the above conditions followed by final heat treatment at 750℃.

• Journal of the Korean Wood Science and Technology
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• v.43 no.2
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• pp.168-176
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• 2015

This study was performed to investigate the effects of heat treatment the on mechanical properties of two species of wood under different heating conditions including at $180^{\circ}C$ for 12 h and 24 h, and at $210^{\circ}C$ for 3 h and 6 h. Two species of wood, Pinus densiflora and Larix kaempferi, were exposed to different heat treatments to assess the effects on the volume change, bending properties in static and dynamic mode and compressive strength. The results showed heat treatment caused significant changes in mechanical properties such as the static and dynamic moduli of elasticity ($MOE_d$ and $MOE_s$), and the modulus of rupture (MOR). The volume of the wood after heat treatment decreased as the heating temperature and time were increased. The bending strength performance of the wood after heat treatment decreased as the heating temperature and time were increased. The effect of heat treatment at a high temperature on the bending MOR was greater in both species than that for a long time. However, the compressive strengths of all the heat-treated samples were higher than the control sample. Furthermore, highly significant correlations between $MOE_d$ and MOR, and $MOE_s$ and MOR were found for all heating conditions.

• Journal of the Korean institute of surface engineering
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• v.48 no.6
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• pp.329-334
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• 2015

The aim of this paper is to determine the proper heat treatment temperature for SDSS tube production without ${\sigma}$-phase precipitation. When Mother steel tube was heat treated at $800^{\circ}C$ temperature, relatively a large amount of ${\sigma}$-phase precipitated and grain refinement of ferrite phase occurred simultaneously. However, in Pilgered and Drawn steel tubes, grain refinement of the ferrite phase did not occur and a small amount of ${\sigma}$-phase precipitated. For all three types of steel tubes, the pitting potential was reduced to 2/5 or less compared with the untreated one and corrosion also occurred in the salt spray test due to the precipitation of ${\sigma}$-phase. When heat treatment temperature was $900^{\circ}C$, grain refinement of the ferrite phase occurred and very little ${\sigma}$-phase precipitated in Pilgered and Drawn steel tubes. But when heat treatment was done at $1,000^{\circ}C$ temperature, all three types of steel tubes had a similar corrosion properties of that of untreated one and also corrosion did not occur in the salt spray test, as ${\sigma}$-phase did not precipitate. Therefore, the optimum heat treatment temperature range is determined to be more than $1000^{\circ}C$ for the SDSS at which corrosion does not occur.

• Journal of the Korean Society for Heat Treatment
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• v.32 no.6
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• pp.263-269
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• 2019

The mechanism of microstructure and hardness changes during mill annealing of Ti-6Al-4V alloy was investigated. The annealing heat treatments were performed at $675{\sim}795^{\circ}C$ in vacuum for 2 hours, followed by air cooling. The microstructure was observed by using an optical microscope and X-ray diffraction, and hardness was measured by using a Rockwell hardness tester and micro Vickers hardness tester. The average grain size becomes smaller at $675^{\circ}C$ to $735^{\circ}C$ due to the formation of new grains rather than grain growth, but becomes larger at $735^{\circ}C$ to $795^{\circ}C$ due to growth of the already-formed grains rather than formation of new grains. The mill annealing temperature becomes higher, the ${\beta}$ phase fraction decreases and ${\alpha}$ phase fraction increases at room temperature. This is because the higher annealing temperature, the smaller amount of V present in the ${\beta}$ phase, and thus the ${\beta}$ to ${\alpha}$ transformation occurs more easily when cooled to room temperature. As the mill annealing temperature increases, the hardness value tends to decrease, mainly due to resolution of defects such as dislocations from $675^{\circ}C$ to $735^{\circ}C$ and due to grain growth from $735^{\circ}C$ to $795^{\circ}C$, respectively.

• Corrosion Science and Technology
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• v.14 no.6
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• pp.296-300
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• 2015

ALDC8 (Al-Si-Cu) alloy has been often corroded with pattern of intergranular corrosion in corrosive environments. Thus, in order to improve its corrosion resistance, the effect of annealing heat treatment to corrosion resistance and hardness was investigated with parameters of heating temperatures such as $100^{\circ}C$, $200^{\circ}C$, $300^{\circ}C$, $400^{\circ}C$ and $500^{\circ}C$ for 1hr. The hardness was varied with annealing temperature and slightly decreased with annealing heat treatment. However, the relation between annealing temperature and hardness agreed not well each other. Corrosion potential was shifted to noble direction and corrosion current density was also decreased with increasing annealing temperature. Moreover, both AC impedance at 10 mHz and polarization resistance on the cyclic voltammogram curve were also increased with increasing annealing temperature. Furthermore, intergranular corrosion was somewhat observed in non heat treatment as well as annealing temperatures at $100^{\circ}C$, $200^{\circ}C$ and $300^{\circ}C$, while, intergranular corrosion was not nearly observed at annealing temperature of $400^{\circ}C$, $500^{\circ}C$. Consequently, it is considered that the annealing heat treatment of ALDC8 alloy may be an available method not only to inhibit its intergranular corrosion but also to improve its corrosion resistance.

• Carbon letters
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• v.13 no.3
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• pp.151-156
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• 2012

This study considered the effect of the heat treatment temperature on the compressive strength of coal powder compacts affected by density, porosity, and crystallinity. Coal powder compacts were made by pressing of milled coal powder and were heat treated at 200, 400, 600, 800, and $1000^{\circ}C$. The density and porosity of the heat treated specimens at each temperature were measured using the Archimedes method and changes in crystallinity were analyzed using Raman spectroscopy. Increases in compressive strength at $600^{\circ}C$ or higher temperatures were proportionally related to increases in the density and the degree of crystallinity.

• Journal of the Korea Furniture Society
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• v.23 no.2
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• pp.163-168
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• 2012

Specimens of seven hardwood species were heat-treated at three temperature levels of 170, 190 and $210^{\circ}C$. Their FSP's were measured by the volumetric swelling method and compared with the control's. Within a species the FSP decreases as the temperature of heat treatment increases. The FSP's of the controls range from 26.1 to 29.6%, while those of the specimens heat-treated at $210^{\circ}C$ from 16.9 to 21.8%. There were no difference of basic density between the heat-treated and control specimens. The color indexes of ash and beech specimens were measured using a colorimeter. It was revealed that the temperature of heat treatment affected on the color more than the treatment time.

• Journal of Advanced Marine Engineering and Technology
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• v.26 no.1
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• pp.90-98
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• 2002

In this paper, the annealing heat treatments for the best corrosion resistant of Ti(Grade 2) were studied in a 3.5% NaCl solution by electrochemical methods. The annealing heat treatments were accomplished at 650, 700 and $750^{\circ}C$ with different time of 30min., 1hour and 2 hours in a vacuum condition. The obtained results are: 1) in the case of solution heat treated $930^{\circ}C$ for 2 hours in a vacuum and air, the corrosion potentials were -348.7 and -567. 1mV, and current densities 2.32 and $22.62\mu\textrm{A}$, respectively, 2) as increase both annealing heat treatment temperature 650, 700, $750^{\circ}C$ and time 30min., 1 hour, 2 hours, the corrosion potential were decreased, whereas corrosion current density increased, 3) in the case of cyclic polarization, the measured charges were increased as increasing solution heat treatment temperature and time, 4) on the bases of corrosion potential, current density and charge, the best annealing temperature and time were measured as $700^{\circ}C$ and 30min. for Ti(Grade 2) material.

• Journal of the Korean Wood Science and Technology
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• v.23 no.4
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• pp.67-73
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• 1995

This study was undertaken to investigate the effect of heat treatment on the dynamic viscoelasticity of three species of Phyllostachys bambusoides, Phyllostachys nigra var. henonis and Phyllostachys pubescens, grown in southern Korea. The bamboo was treated for 3~24 hours at $60{\sim}180^{\circ}C$, and then was treated in a climatic chamber for 3~48 hours at $40^{\circ}C$ and 95% relative humidity. The results obtained are summarized as follows : 1. Dynamic Young's modulus decreased with increasing temperature and duration of the heat treatment. 2. Internal friction decreased with increasing treatment duration. 3. Moisture absorption decreased with increasing temperature and duration of the heat treatment. 4. Dynamic viscoelasticity decreased, whereas internal friction slowly increased, with increasing moisture content.

• Journal of the Korean Wood Science and Technology
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• v.35 no.6
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• pp.50-56
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• 2007

FAO standard for heat sterilization of wood, International standards for phytosanitary measures (ISPM) No.15, must meet heat-treated wood core temperature to be higher than $56^{\circ}C$ and keep the temperature for more than 30 minutes. This study was carried out to analyze the heat treatment characteristics of domestic pinewood sterilized with the FAO standard. To enhance the effectiveness of heat treatment process in mountainous district energy consumption and time required to reach target temperature were evaluated at various temperature and relative humidity conditions and moisture contents of wood. Heat-treatment of high temperature and high humidity reduced the required heating time. Lower humidity levels at same temperature reduced energy consumption per unit time. However, lower humidity levels could not reduce total energy consumption greatly because longer treatment time was required at that condition. It is necessary to estimate energy consumption and predict treatment time in dynamic heating and cooling situations, because it frequently happens not to meet optimum treatment condition due to poor surrounding climates and operation performance of heat treatment facility in real field.