• 대한치과교정학회지
• /
• 제36권5호
• /
• pp.349-359
• /
• 2006

니켈-티타늄 합금은 높은 spring-back성질, 초탄성 효과, 형상기억 효과 등의 장점을 가지고 있으나 성형이 어렵다는 단점을 가지고 있다. 본 연구에서는 니켈-티타늄 와이어의 굴곡을 위한 열처리 시에 나타나는 부하-변위 곡선의 변화 및 상전이 온도 변화와 같은 물성 변화 양상을 조사하고자 하였다. 수종의 니켈-티타늄 와이어를 열처리를 시행하지 않은 군, 전기저항 열처리 장치를 이용하여 와이어 단면적에 따라 제조회사에서 권장하는 전류를 기초로 하여 $00.016"\;{\times}\;00.022"$ (5 A, 7 sec), $0.018"\;{\times}\;0.025"$ (6 A, 7 sec) 그리고 $0.0215"\;{\times}\;0.028"$ (7 A, 8 sec) 와이어를 열처리만 시행한 실험군, 열처리를 시행하여 굴곡을 부여한 실험군 그리고 열처리 시간을 1초 증가시켜 굴곡을 부여한 실험군으로 분류하여 3점 굴곡 실험과 시차주사열량측정을 하여 다음과 같은 결과를 얻었다. $0.016"\;{\times}\;0.022"$, $0.018"\;{\times}\;0.025"$ 그리고 $0.0215"\;{\times}\;0.028"$ 니켈-티타늄 와이어에서 굴곡을 부여하지 않고 열처리만 시행한 실험군이 열처리를 시행하지 않은 대조군에 비해 부하-변위 곡선이 상방 이동되어 초탄성 현상에 의한 평탄역(loading and unloading plateau)의 힘이 더 증가되었다. $0.016"\;{\times}\;0.022"$, $0.018"\;{\times}\;0.025"$ 그리고 $0.0215"\;{\times}\;0.028"$ 와이어에서 열처리만 시행한 실험군이 열처리를 시행하지 않은 군보다 더 낮은 austenite finish ($A_f$) 온도를 보였다. $0.018"\;{\times}\;0.025"$ 및 $0.0215"0.028"$ 와이어에서 열처리를 시행하여 굴곡을 부여한 실험군은 열처리만 시행한 실험군과 열처리를 시행하지 않은 대조군에 비해 부하-변위 곡선이 상방 이동되었으며, 열처리 시간을 1초 증가시켜 굴곡을 부여한 실험군에서 가장 높은 부하-변위 곡선을 나타냈다. $0.018"\;{\times}\;0.025"$ 그리고 $0.0215"\;{\times}\;0.028"$ 와이어에서 $A_f$ 온도는 열처리 시간을 1초 증가시켜 굴곡을 부여한 실험군에서 가장 낮게 관찰되었고 열처리를 시행하여 굴곡을 부여한 실험군, 열처리만 시행한 실험군 그리고 열처리를 시행하지 않은 대조군 순으로 높게 관찰되었다. 이상의 결과를 종합할 때, 임상에서 니켈-티타늄 합금 와이어에 굴곡을 부여하기 위해 열처리하는 경우 초탄성 특성은 유지될 수 있으나, 부하-변위 곡선의 상방 증가가 나타나므로, 와이어에 의한 교정력이 증가될 수 있음에 유의하여야 한다.

• 열처리공학회지
• /
• 제32권2호
• /
• pp.57-60
• /
• 2019

The impact of two-step treatment on the mechanical properties of the 6061 Al alloy was investigated by testing the hardness and electrical conductance values. After two-step aging treatment, the hardness and electrical conductivity of the alloy was increased, and if the first aging treatment temperature was lower than the secondary aging treatment temperature, both the hardness and the electrical conductivity were not increased. The higher the temperature of the first aging treatment, the higher the hardness. The temperature of the first aging treatment is $175^{\circ}C$, $150^{\circ}C$, $120^{\circ}C$, and the second is $175^{\circ}C$ and $120^{\circ}C$.

• 열처리공학회지
• /
• 제22권1호
• /
• pp.3-7
• /
• 2009

Variation in oxidation behavior with heat treatment temperature is investigated for a Ni-Ti alloy using X-ray diffraction, DSC (differential scanning calorimetry) and Auger electron spectroscopy. And the effect of oxidation on transformation behavior and superelasticity is characterized. A cold-worked 50.6Ni-Ti alloy is oxidized at 300-$700^{\circ}C$ for 1 hr in the air atmosphere. With an increase in heating temperature, the structure of $TiO_2$ changes from amorphous (300 and $400^{\circ}C$) to anatase ($500^{\circ}C$), and to rutile ($700^{\circ}C$). Activation energy of oxidation for NiTi is measured to be 51 Kcal/mol when heating temperature is $500^{\circ}C$ or above. Since Ti reacts preferably with oxygen, Ni content increases between matrix and oxide, forming $Ni_{3}Ti$ compounds. The resultant of oxidation decreases significantly $M_s$ and $A_s$ temperature in the specimen oxidized at $900^{\circ}C$ with $B_2{\rightarrow}M$ transformation path. An extra is found on cooling between two peaks in the specimen with $B_2{\rightarrow}R{\rightarrow}M$ one which is oxidized at $900^{\circ}C$ and aged at $500^{\circ}C$. Oxidation deteriorates superelasticity due to formation of Ni-rich compound.

• Journal of Forest and Environmental Science
• /
• 제29권2호
• /
• pp.109-115
• /
• 2013

Fast-grown wood generally contains a high proportion of juvenile wood that results in inferior dimensional stability and durability against biological deteriorations. In the present research, the Acacia mangium wood from plantation forests in Vietnam was treated with high temperature in air. The effects of heat treatment on physical properties of Acacia mangium wood, including mass loss (ML), water absorption (WA), water-repellent effectiveness (WRE) and anti-swelling efficiency (ASE) were examined. The results showed that the dimensional stability and the water-repellent effectiveness are increased by about 15-46% and 8-18%, respectively. However, the mass and dimension of wood are decreased. The results also indicated that both treatment temperature and treatment duration significantly affect the wood properties of Acacia mangium. It is thus concluded that heat treatment demonstrates an interesting potential to improve the wood quality of Acacia mangium for solid timber products. This technology provides an environmentally safe method of protecting sustainable common woods to give a new generation of value-added biomaterials with increased stability without the use of toxic chemicals.

• 열처리공학회지
• /
• 제16권5호
• /
• pp.281-284
• /
• 2003

• 대한기계학회논문집A
• /
• 제23권7호
• /
• pp.1215-1222
• /
• 1999

It is advantageous to use an NDE method to assess the mechanical properties of materials since the conventional method is time-consuming and sometimes requires cutting of sample from the material/component. This paper shows that the ultrasonic and the Barkhausen noise(BHN) methods can be used to accurately characterize forged reactor vessels. The attenuation coefficient of the ultrasonic wave was changed with heat treatment temperature and condition[as-quenched, tempered, PWHT]. The RMS[root mean square] voltage of Barkhausen noise depended on heat treatment temperature and conditions. The fracture appearance transition temperature(FATT) can be predicted using nondestructive evaluation methods.

• 한국세라믹학회지
• /
• 제34권10호
• /
• pp.1045-1052
• /
• 1997

Barium ferrites (BaFe12O19) were synthesized at the various temperature by the coprecipitation-oxidation method. X-ray diffraction Rietveld analysis for barium ferrites were performed, their microstructures were observed and their magnetic properties were measured, in order to analyze the crystal structures and determine the optimal temperature of heat-treatment. The barium ferrite, its average particle size 80 nm, was formed at 600℃ through the hematite (α-Fe2O3), but the site occupations of the Fe's in tetrahedral and bipyramidal sites and of the Ba relatively low. Increasing the heating temperature, these occupations and the magnetization increased, and the crystal c-axis decreased. These changes were very small at the heat treatment of above 800℃, but the particles were rapidly grown. It is suggested that the optimal temperature of heat-treatment is 800℃, at which temperature crystal structure is relatively stable and the particles hardly ever grow.

• Nuclear Engineering and Technology
• /
• 제45권6호
• /
• pp.821-826
• /
• 2013

In the present study, the effects of various heat treatments on the microstructure and mechanical properties of dual phase ODS steels were investigated to enhance the high strength at elevated temperature. Dual phase ODS steels have been designed by the control of ferrite and austenite formers, i.e., Cr, W and Ni, C in Fe-based alloys. The ODS steels were fabricated by mechanical alloying and a hot isostatic pressing process. Heat treatments, including hot rolling-tempering and normalizing-tempering with air- and furnace-cooling, were carefully carried out. It was revealed that the grain size and oxide distributions of the ODS steels can be changed by heat treatment, which significantly affected the strengths at elevated temperature. Therefore, the high temperature strength of dual phase ODS steel can be enhanced by a proper heat treatment process with a good combination of ferrite grains, nano-oxide particles, and grain boundary sliding.

• Food Science and Biotechnology
• /
• 제17권5호
• /
• pp.1010-1015
• /
• 2008

The effects of heat treatment on the physicochemical properties and mineral composition of sun-dried salt were investigated. The salts parched at high temperature were appeared the higher alkalinity and the lower oxidation-reduction potential (ORP) than the samples without heat treatment. The commercial salts (bamboo salt and yellow loess salt) and the sun-dried salt parched at high temperature had relatively higher sodium ion content (418-450 ppm) compared to that (418.0 ppm) of refined salt. The increase of calcium ion occurred in the salts parched at high temperature compared to the sun-dried salt without heat treatment, but the magnesium ion was vice versa. The commercial salt, yellow loess salt had highest turbidity (0.973) whereas sun-dried salt showed lowest level (0.097) among the tested samples. Turbidity of heat treatment samples decreased as solubility increased. The maximum concentration of dialyzed salt was reached after 4 hr regardless of various processed salts, but those had no difference significantly among the tested samples. The X-ray diffraction patterns of the parched sun-dried salts showed different peak intensity with common salts, and they were similar to the patterns of oxide salts, especially MgO. The maximum value (2.56%) of MgO appeared in the sun-dried salt parched at $1,400^{\circ}C$.

• Journal of Mechanical Science and Technology
• /
• 제18권12호
• /
• pp.2204-2208
• /
• 2004

Ti-8Ta-3Nb has been developed as a new biomaterial. The experimental specimens are as-cast and forged Ti-8Ta-3Nb alloys. Treatment in a solution, ranging from 760 to 960$^{\circ}C$ has carried out. The microstructural research has carried out after the solution treatment and the hardness was measured. The specific heat and the length variations of Ti-8Ta-3Nb were also measured. The optimum temperature for the solution heat treatment of Ti-8Ta-3Nb was found to be 880$^{\circ}C$. This was based on the mechanical properties and the volume fraction of ${\alpha}$ phase and their phases shown from the results of the solution heat treatment. From the results, the ${\beta}$ transition temperature of Ti-8Ta-3Nb was found to be between 860$^{\circ}C$ and 880$^{\circ}C$.