• 제목/요약/키워드: Heat-setting

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A Fundamental Experiment on Preventing Frost Damage at Early Age of Mortar in Low Temperature using Reduction Slag (환원슬래그를 사용한 모르타르의 저온에서의 초기동해 방지에 관한 기초적 실험)

  • Min, Tae-Beom;Mun, Young-Bum;Kim, Hyeong-Cheol;Choi, Hyun-Kuk;Kim, Jae-Young;Lee, Han-Seung
    • Journal of the Korea Institute of Building Construction
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    • v.16 no.1
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    • pp.1-7
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    • 2016
  • In this research, it used cement powder and reduction slag, which generates high hydration heat in hydration reaction without heat cure below $-5^{\circ}C$ degree. Purpose of final research is preventing freezing and thawing by making the compressive strength 5MPa in 3days below zero temperature due to own heat of concrete. and it is the result of physical characteristic and thermal property evaluation of reduction slag. Because reduction slag generates high hydration heat, compressive strength development is excellent. By generating highly hydration heat by $C_{12}A_7$ and $C_3A$ in reduction slag, compressive strength is developed in low temperature. In case of displacing only reduction slag without $SO_3$, it is indicated that quick-setting occurs by shortage of $SO_3$. For preventing quick-setting, gypsum is used essentially. According to this research result, in case of using reduction slag and gypsum as a ternary system, compressive strength developed 5MPa in 3 days below zero temperature. It is identified to prevent early frost damage of concrete below zero temperature.

Phase Changes of Soil-Cement Mixture Using Fall Cone and Heat of Hydration (Fall cone과 수화열을 이용한 흙-시멘트 혼합물의 상 변화 연구)

  • Kim Jae-Hyung;Won Jeong-Yun;Kim Sung-Pil;Chang Pyoung-Wuck
    • Journal of the Korean Geotechnical Society
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    • v.20 no.9
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    • pp.25-32
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    • 2004
  • Some amount of cements can be added into the soil with high water content to improve the engineering properties. In such a case, it is difficult to predict and figure out the phase changes of the soil-cement mixture which is closely associated with workability of the soil-cement mixture. Changes in heat of hydration and hardness of the cement pastes are known to provide the useful information about the phase changes of the soil-cement mixtures. In this study, heat of hydration and cone penetration depth were measured from the specimens of cement paste and 3 soil-cement mixtures. From the experimental results, it was found that the phase changes of the soil-cement mixtures are the same as those of cement paste, and that shear strength of the mixtures abruptly increases when the heat of hydration is minimum. Initial setting time of the mixtures coincides with the state when fall cone penetration depth was 1.0 mm and it is defined as plastic limit of the mixtures. Initial setting time of the mixtures is retarded as soil/cement ratio is increased. Measurements of heat of hydration and fall cone apparatus could be the useful tools to predict the phase changes of tile soil-cement mixtures.

Comparison of Strength-Maturity Models Accounting for Hydration Heat in Massive Walls

  • Yang, Keun-Hyeok;Mun, Jae-Sung;Kim, Do-Gyeum;Cho, Myung-Sug
    • International Journal of Concrete Structures and Materials
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    • v.10 no.1
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    • pp.47-60
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    • 2016
  • The objective of this study was to evaluate the capability of different strength-maturity models to account for the effect of the hydration heat on the in-place strength development of high-strength concrete specifically developed for nuclear facility structures under various ambient curing temperatures. To simulate the primary containment-vessel of a nuclear reactor, three 1200-mm-thick wall specimens were prepared and stored under isothermal conditions of approximately $5^{\circ}C$ (cold temperature), $20^{\circ}C$ (reference temperature), and $35^{\circ}C$ (hot temperature). The in situ compressive strengths of the mock-up walls were measured using cores drilled from the walls and compared with strengths estimated from various strength-maturity models considering the internal temperature rise owing to the hydration heat. The test results showed the initial apparent activation energies at the hardening phase were approximately 2 times higher than the apparent activation energies until the final setting. The differences between core strengths and field-cured cylinder strengths became more notable at early ages and with the decrease in the ambient curing temperature. The strength-maturity model proposed by Yang provides better reliability in estimating in situ strength of concrete than that of Kim et al. and Pinto and Schindler.

A Study on the Development of the Console with LCD Panel for Exterior Advertizing (LCD 패널을 탑재한 옥외 광고용 콘솔 개발에 관한 연구)

  • Choi, Kab-Yong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.1
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    • pp.13-20
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    • 2010
  • The development of the console for exterior advertizing LCD Panel(LCD Console) is the purpose of this study with regard to importance of display industry. In this study, the most important point is to develop the cooling system for LCD Console. It is developed by using systematic application techniques and statistical tests and analysis to integrate commercial components, cooling fan, heat sink, thermo electronic modules etc, of it. This study, at first, shows design/manufacturing process of the cooling system and the setting process of control factors to control through experimentation. Next, after constructing the complete console, 46 inch LCD Panel and the cooling system are built in, the performance test of it is shown through experimentation.

Ice Slurry Formation of a Solution in a Pressurized Plate Heat Exchanger (가압 판형 열교환기에 의한 수용액의 아이스슬러리 생성)

  • Lee Dong-Gyu;Kim Byung-Seon;Peck Jong-Hyeon;Hong Hi-Ki;Kang Chae-Dong
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.18 no.7
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    • pp.596-602
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    • 2006
  • Ice adhesion and blockage problems have been issued in continuous ice slurry making process. So we composed continuous ice slurry making device using a commercial small plate heat exchanger (PHX), and investigated character of ice formation. An experiment of ice formation was peformed with an aqueous solution of ethylene glycol 7 mass%. In the experiment, the effect of the pressurization on ice slurry formation during the cooling process was investigated. The pressurization test for the aqueous solution was performed by setting valves at the PHX inlet and outlet. At the results, the time of continuous ice formation increased as the pressure of the plate heat exchanger increased for cooling temperature of $-5^{\circ}C$. Also continuous ice formation at the cooling temperature of $-7^{\circ}C$ showed a possibility. It was found that the pressurization may contribute to suppress the dissolution of supercooled aqueous solution in the PHX.

Effects of steam heat treatment conditions on the swelling and physical properties of PBS (polybutylene succinate) copolymer monofilament gill net (습식 열처리 조건이 PBS 공중합체 모노필라멘트 그물감의 부풀음 및 물성변화에 미치는 영향)

  • Park, Seongwook;Kim, Seonghun;Do, Choonho;Lim, Jihyun;Choi, Haesun
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.50 no.3
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    • pp.274-283
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    • 2014
  • Swelling of the heat-treated netting for gillnet was estimated through the netting height in square acrylic tank. Experimental Nylon netting and PBSAT netting were heat-treated by using the high-degree vacuum method in hot water after net making. Heat-treatment temperatures were conducted with Nylon netting $105^{\circ}C$ and PBSAT netting $62^{\circ}C$, $65^{\circ}C$, $66^{\circ}C$, $67^{\circ}C$. The swelling measurement method of a netting using the square tank was capable of the reduction measurement errors comparing with measurement methods of a mesh inner angle and the shortening rate of a mesh size. In addition, this method was available to comparison evaluation for each netting more easily. Wet type heat-treatment apparatus with high-degree vacuum was shown higher $7{\sim}8^{\circ}C$ inner side temperature than a setting temperature. The tensile strength and elongation of Nylon netting and PBSAT netting were shown higher wet condition than dry condition. The tensile strengths of PBSAT monofilaments in dry and wet condition were sharply decreased at heat-treatment temp. $75^{\circ}C$ than heat-treatment temp. $74^{\circ}C$.

THERMAL ANALYSIS OF THE DUAL CURED RESIN CEMENTS ACCORDING TO CURING CONDITION (중합조건에 따른 dual cured resin cement의 열분석적 연구)

  • Lee, In-Bog;Chung, Kwan-Hee;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.24 no.2
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    • pp.265-285
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    • 1999
  • The purposes of this investigation were to observe the reaction kinetics of five commercial dual cured resin cements (Bistite, Dual, Scotchbond, Duolink and Duo) when cured under varying thicknesses of porcelain inlays by chemical or light activation and to evaluate the effect of the porcelain disc on the rate of polymerization of dual cured resin cement during light exposure by using thermal analysis. Thermogravimetric analysis(TGA) was used to evaluate the weight change as a function of temperature during a thermal program from $25{\sim}800^{\circ}C$ at rate of $10^{\circ}C$/min and to measure inorganic filler weight %. Differential scanning calorimetry(DSC) was used to evaluate the heat of cure(${\Delta}H$), maximum rate of heat output and peak heat flow time in dual cured resin cement systems when the polymerization reaction occured by chemical cure only or by light exposure through 0mm, 1mm, 2mm and 4mm thickness of porcelain discs. In 4mm thickness of porcelain disc, the exposure time was varied from 40s to 60s to investigate the effect of the exposure time on polymerization reaction. To investigate the effect on the setting of dual cured resin cements of absorption of polymerizing light by porcelain materials used as inlays and onlays, the change of the intensity of the light attenuated by 1mm, 2mm and 4mm thickness of porcelain discs was measured using curing radiometer. The results were as follows 1. The heat of cure of resin cements was 34~60J/gm and significant differences were observed between brands (P<0.001). Inverse relationship was present between the heat of reaction and filler weight % the heat of cure decreased with increasing filler content (R=-0.967). The heat of reaction by light cure was greater than by chemical cure in Bistite, Scotchbond and Duolink(P<0.05), but there was no statistically significant difference in Dual and Duo(P>0.05). 2. The polymerization rate of chemical cure and light cure of five commercially available dual cured resin cements was found to vary greatly with brand. Setting time based on peak heat flow time was shortest in Duo during chemical cure, and shortest in Dual during light cure. Cure speed by light exposure was 5~20 times faster than by chemical cure in dual cured resin cements. The dual cured resin cements differed markedly in the ratio of light and chemical activated catalysts. 3. The peak heat flow time increased by 1.51, 1.87, and 3.24 times as light cure was done through 1mm, 2mm and 4mm thick porcelain discs. Exposure times recommended by the manufacturers were insufficient to compensate for the attenuation of light by the 4mm thick porcelain disc. 4. A strong inverse relationship was observed between peak heat flow and peak time in chemical cure(R=0.951), and a strong positive correlations hip was observed between peak heat flow and the heat of cure in light cure(R=0.928). There was no correlationship present between filler weight % or heat of cure and peak time. 5. The thermal decomposition of resin cements occured primarily between $300^{\circ}C$ and $480^{\circ}C$ with maximum decomposition rates at $335^{\circ}C$ and $440^{\circ}C$.

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Burning Tests for Interior Flooring Materials (건축용 바닥재의 연소성능 시험)

  • Lee, Bong-Woo;Lee, Jang-Won;SaKong, Seong-Ho;Kim, Hee-Soo;Lee, Byoung-Ho;Kim, Hyun-Joong
    • Fire Science and Engineering
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    • v.22 no.2
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    • pp.30-37
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    • 2008
  • We have performed the inflammability test for various flooring materials through a radiant heat panel tester by using the specification KSISO 9239-1 (an examination method of flooring materials) that has been set as an international standard for the fire prevention means of interior flooring materials. We have measured the flame spread distance, critical heat flux and smoke density generated by the fire of various flooring materials while using the radiant heat panel tester. The measurement result has shown the burning characteristics different from each other by the respective flooring materials and we could see that the surface materials and construction elements influence greatly on the heat release and smoke generation. We could see that the evaluation method above is an important test method in evaluating the critical heat flux, smoke generation and flame spread distance that are Important factors in studying for fire risks and it is judged that setting and applying a fire evaluation method of flooring materials suitable for the domestic construction use would be relevant.

A study of Experimental on Construction of Concrete Filled in Steel Tube Column under a Low Temperature (저온하에서의 CFT 시공을 위한 실험적 연구)

  • 강용학;이민경;정근호;백민수;김진호;정상진
    • Proceedings of the Korea Concrete Institute Conference
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    • 2002.10a
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    • pp.489-494
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    • 2002
  • The basic Physical properties, Slump, Slump Flow, Air content, Bleeding, and Settlement of concrete was investigated to test Characteristic of Setting and to evaluate the relation between Model Specimen and Heat of Hydration for construction under Low Temperature (CFT). The objective of this study is to take the partial core after the cementation of Model Specimen, test the compression intensity and analyze the relation to Test Piece.

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Influences of Sodium Gluconate on the Physical Properties of Portland Cement Pastes and Mortars (포틀랜드 시멘트 페이스트 및 몰탈의 물성에 미치는 글루콘산 나트륨의 영향)

  • 김창은;이승헌;김원기;이경원
    • Journal of the Korean Ceramic Society
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    • v.24 no.3
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    • pp.289-295
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    • 1987
  • The changes of physical properties of portland cement pastes and mortars were investigated by addition of sodium gluconate. Flow table experiment and viscosity measurement were took in order to find dispersing effect, and time-dependent changesof viscosity and rates of hydration heat evolution were carried out for the sake of finding retardation effect of hydration. And changes of physical properties of cement pastes and mortars were discussed by setting time, compressive strength and porosity.

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