• Membrane Journal
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• v.9 no.4
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• pp.215-220
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• 1999

The asymmetric polyimide [PI] membrane with good solvent-resisting and heat-resisting properties was prepared by using the phase inversion method from polyamic acid, and its pervaporation separation characteristics of water-acetic acid system were studied. It was appeared from the prepared membranes that the best non-solvent of polyamie acid for the phase inversion was toluene. The best heat-treatment condition for the imidization of polyamic acid was 1 hr heating at each of the temperatures, 373, 473, and 573 K The thermal durability and chemical stability during the pervaporation separation of water-acetic acid of the prepared PI membrane was superior. The pervaporation characteristics of prepared membrane were 180 of separation factor and 0.5 kg/$m^2$hr of total flux for 80 wt% acetic acid feed.

• Transactions of the Korean Society of Automotive Engineers
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• v.14 no.3
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• pp.133-141
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• 2006

The Low cycle fatigue behavior of 11.7Cr-1.1Mo heat-resisting steel has been investigated under strain-controlled conditions with mean stresses at room temperature and $300^{\circ}C$. For the tensile mean stress test, the initial high tensile mean stress generally relaxed to zero at room temperature, however, at $300^{\circ}C$ initial tensile mean stress relaxed to compressive mean stress. Low cycle fatigue lives under mean stress conditions are usually correlated using modifications to the strain-life approach. Based on the fatigue test results from different stain ratio of -1, 0, 0.5, and 0.75 at room temperature and $300^{\circ}C$, the fatigue damage of the steel was represented by using cyclic strain energy density. Total strain energy density considering mean stress indicated well better than not considering mean stress at $300^{\circ}C$. Predicted fatigue life using Smith-Watson-Topper's parameter correlated fairly well with the experimental life at $300^{\circ}C$.

• Journal of Korea Foundry Society
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• v.33 no.3
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• pp.122-126
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• 2013

Recently, heat-resistant aluminum alloy has been re-focused as a downsizing materials for the internal combustion engines. Heat-resistant Al alloy development and many researches are still ongoing for the purpose of improving thermal stability, high-temperature mechanical strength and fatigue properties. The conventional principle of heat-resistant Al alloy is the precipitation of intermetallic compounds by adding a variety of elements is generally used to improve the mechanical properties of Al alloys. Heat resistant aluminum alloys have been produced by CrW homogeneous solid solution to overcome the limit of conventional heat resistant aluminum alloy. From EPMA, it is found that CrW homogeneous soild solution phases with the size of $50-100{\mu}m$ have been dispersed uniformly, and there is no reaction between aluminum and CrW alloy. In addition, after maintaining at high temperature of 573 K, there is no growth of hardening phase, nor desolved, but CrW still exists as a homogeneous solid solution.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1996.10a
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• pp.99-104
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• 1996

A proform for engine valve was designed by finite element method. In the preform design of engine valve, various initial billets are simulated for better preform to get sound final product. Here a preform is design to get desirable metal flow in the forming so that the final product has more uniform strain distribution. after forming. The analysis of the micro-structure of the value formed through the designed process was also performed and result was compared with that of simulation.

• Journal of Power System Engineering
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• v.6 no.1
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• pp.68-73
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• 2002

An opportunity to use the elevated temperature has been recently increasing in various elements of heat facilities or machines such as heat exchanger tubes, pressure vessels, engines of aircraft, boilers and turbines in power plants, and nuclear reactor components, etc. as machinery industry develops. Thus, the development of such elevated-temperature heat-resisting materials and the studies on their elevated-temperature materials friction welding, creep design and analysis have been considered as an important and needful fact. In this paper, friction welding optimization for 1Cr0.5Mo to STS304 and AE applications for the weld quality evaluation were investigated. The important results of this study are as follows : The techniques for dissimilar friction welding optimization of the elevated temperature materials 1Cr0.5Mo and STS304 and its real-time weld quality evaluation by AE were developed, considering on both strength and toughness. Quantitative relationship was identified among welding condition, weld quality and cumulative AE counts.

• Journal of Welding and Joining
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• v.20 no.6
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• pp.823-829
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• 2002

In order to evaluate the proper fracture strength of microstructures in a steel weldment, smaller size loading ball than used for a conventional small punch(CSP) testing is required due to regional limitation on constitutive structures. In this study, the minimized loading ball(${\varphi}1.5mm$) and bore diameter of lower die(${\varphi}3mm$) were designed for an advanced small punch(ASP) test. The results obtained from the ASP test were compared with those from a CSP testing for a X20CrMoV121 steel weldment. It was found that the ASP test clearly showed the microstructural dependance on fracture strength and ductile-brittle transition behavior of the weldment. In the ASP test, especially, the cracks tend to initiate for various directions within hemispherical indentation region of an objective structure in SP test. This indicates that the evaluation of more proper fracture strength for F.L+CGHAZ, FGHAZ and ICHAZ can be performed by means of the ASP test in a steel weldment.

• Transactions of the Korean Society of Automotive Engineers
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• v.3 no.1
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• pp.1-12
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• 1995

Isothermal and thermal-mechanical fatigue characteristics of 12Cr heat resisting steel used for high temperature applications were investigated including hold time effects. Isothermal low cycle fatigue test at $600^{\circ}C$ and in-phase, out-of-phase thermal-mechanical fatigue test at 350 to $600^{\circ}C$ were conducted using smooth cylindrical hollow specimen under strain-control with total strain ranges from 0.006 to 0.015. Regardless of thermal-mechanical and isothermal fatigue tests, cyclic softening behavior was observed and much more pronounced in the thermal-mechanical fatigue tests with hold times due to the stress relaxation during the hold time. The phase difference between temperature and strain in thermal-mechanical fatigue tests resulted in significantly shorter fatigue life for out-of-phase compared to in-phase. The differences in fatigue lives were dependent upon the magnitudes of plastic strain ranges and mean stresses. During the hold time in the strain-controlled fatigue tests, the increase in the plastic strain range and the stress relaxation were observed. It appeared that the increase in plastic strain range per cycle and the introduction of creep damage made important contributions to the reduction of thermal-mechanical fatigue life with hold time, and the life reduction tendency was more remarkable in the in-phase than in the out-of-phase thermal-mechanical fatigue. Isothermal fatigue tests performed under the combination of fast and slow strain rates at $600^{\circ}C$ showed that the fatigue life decreased as the strain rate and frequency decreased,especially for the low strain ranges.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2011.03a
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• pp.97-97
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• 2011

현대사회에서 화재에 의한 물적 피해는 물론 인적피해가 현저하게 증가하고 있으며 희생자의 사망원인이 종래에는 화재시 발생한 열에 의한 화상을 중심으로 하는 소사였지만, 최근에는 화염보다 독성가스로 인하여 사망하는 경우가 많아졌고, 희생자는 거의 화상을 확인할 수 없거나 화상자이더라도 혈액 중에서 일산화탄소를 중심으로 한 유독가스가 확인되기 때문에 이들 유독가스의 흡입으로 인하여 행동불능상태 이후 열의 영향으로 사망한 것으로 추정되는 사례가 증가하는 추세이다. 따라서 대규모 건축물에 있어서는 화재발생시 유독가스가 건물 전체로 연소 확대되는 것을 방지하기 위하여 넓은 면적을 일정한 면적으로 구획하거나 계단실 등과 다른 부분 또는 층별 등으로 구획하고 있으며, 국내의 방화구획은 크게 다른 층으로 화재전파를 막기 위한 층간 방화구획, 연소면적을 제한하기 위한 면적별 방화구획, 다른 용도로 인한 화재 위험성 감소를 위해 용도별 방화구획으로 3가지를 법에서 채택하고 있다. 방화구획은 방화문 또는 자동방화셔터를 이용하거나, 내부구조의 바닥, 벽, 각종 방화문으로 구획할 것을 정하고 있다.(피난방화규칙 제14조) 본 연구에서는 철제방화셔터 대체용으로 직물방화셔터용의 실리카 소재를 이용하여 제직한 직물에 내열/차연 기능성 코팅의 공정 조건을 변화하여 최종 방화시험을 거치기 전 내열성 테스트중 하나인 불꽃열 통과량 실험을 실행하여 방화 직물의 내열성을 비교 분석하였다. 이러한 결과를 토대로 본 연구는 고내열/차연성 방화 제품 기술을 개발하는데 필요한 연구를 수행하는데 목적이 있다.

• Journal of the Korean Society for Nondestructive Testing
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• v.27 no.5
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• pp.417-425
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• 2007

The ferritic 9Cr-1Mo-V-Nb heat-resisting steel was experimentally studied in order to characterize its microstructural evolution during creep-fatigue by coercivity measurement. The creep-fatigue test was conducted at $550\;^{\circ}C$ with the tensile holding time of 60s and 600s, respectively. The coercivity decreased until the failure and the hardness monotonously decreased for the whole fatigue life. As the life fraction of creep-fatigue increased, the $M_{23}C_6$ carbide coarsened following the Ostwald ripening mechanism. However, the MX carbonitrides did not grow during creep-fatigue due to so stable at $550\;^{\circ}C$. The width of martensite lath increased because of the dislocation recovery at the lath boundaries. The magnetic coercivity has an influence on the microstructural properties such as dislocation, precipitates and martensite lath boundaries, which interpreted in relation to microstructural changes. Consequently, this study proposes a magnetic coercivity to quantify the level of damage and microstructural change during the creep-fatigue of ferritic 9Cr-1Mo-V-Nb steel.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.27 no.11
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• pp.1979-1985
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• 2003

Fretting is a kind of surface degradation mechanism observed in mechanical components and structures. The fretting damage decreases in 50-70% of the plain fatigue strength. This may be observed in the fossil power plant and the nuclear power plant used in special environments and various loading conditions. The thermal degradation of material is observed when the heat resisting steel is exposed for long period time at the high temperature. In the present study, the degraded 1Cr-0.5Mo steel used for long period time at high temperature (about 515$^{\circ}C$) and artificially reheat-treated materials are prepared. These materials are used for evaluating an effect of thermal aging on the fretting fatigue behavior. Through the experiment, it is found that the fretting fatigue endurance limit of the reheat-treated 1Cr-0.5Mo steel decreased about 46% from the non-fretting fatigue endurance limit, while the fretting fatigue endurance limit of the degraded 1Cr-0.5Mo steel decreased about 53% from the non-fretting fatigue endurance limit. The maximum value of fatigue endurance limit difference is observed as 57%(244 MPa) between the fretting fatigue of degraded material and non-fretting fatigue of reheat-treated material. These results can be a basic data to a structural integrity evaluation of heat resisting steel considered to thermal degradation effect.