• 한국분말재료학회지
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• 제21권5호
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• pp.349-354
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• 2014

This study is a basic research for repair material production which manufactured a Cu repair coating layer on the base material of a Cu plate using kinetic spray process. Furthermore, the manufactured material underwent an annealing heat treatment, and the changes of microstructure and macroscopic properties in the Cu repair coating layer and base material were examined. The powder feedstocks were sphere-shaped pure Cu powders with an average size of $27.7{\mu}m$. The produced repair coating material featured $600{\mu}m$ thickness and 0.8% porosity, and it had an identical ${\alpha}$-Cu single phase as the early powder. The produced Cu repair coating material and base material displayed extremely high adhesion characteristics that produced a boundary difficult to identify. Composition analysis confirmed that the impurities in the base material and repair coating material had no significant differences. Microstructure observation after a $500^{\circ}C/1hr$. heat treatment (vacuum condition) identified recovery, recrystallization and grain growth in the repair coating material and featured a more homogeneous microstructure. The hardness difference (${\Delta}H_v$) between the repair coating material and base material significantly reduced from 87 to 34 after undergoing heat treatment.

• 한국분말재료학회지
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• 제21권3호
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• pp.229-234
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• 2014

This study manufactured a CIG-based composite coating layer utilizing a new warm spray process, and a mixed powder of Cu-20at.%Ga and Cu-20at.%In. In order to obtain the mixed powder with desired composition, the Cu-20at.%Ga and Cu-20at.%In powders were mixed with a 7:1 ratio. The mixed powder had an average particle size of $35.4{\mu}m$. Through the utilization of a warm spray process, a CIG-based composite coating layer of $180{\mu}m$ thickness could be manufactured on a pure Al matrix. To analyze the microstructure and phase, the warm sprayed coating layer underwent XRD, SEM/EDS and EMPA analyses. In addition, to improve the physical properties of the coating layer, an annealing heat treatment was conducted at temperatures of $200^{\circ}C$, $400^{\circ}C$ and $600^{\circ}C$ for 1 hour each. The microstructure analysis identified ${\alpha}$-Cu, $Cu_4In$ and $Cu_3Ga$ phases in the early mixed powder, while $Cu_4In$ disappeared, and additional $Cu_9In_4$ and $Cu_9Ga_4$ phases were identified in the warm sprayed coating layer. Porosity after annealing heat treatment reduced from 0.75% (warm sprayed coating layer) to 0.6% (after $600^{\circ}C/1hr$. heat treatment), and hardness reduced from 288 Hv to 190 Hv. No significant phase changes were found after annealing heat treatment.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1996년도 추계학술대회 논문집
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• pp.964-968
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• 1996

The demands of size and quality of large steel shaft forgings for ship building, power plant, steel plant, etc. are rapidly increasing, and some of these productions are manufactured from ingot weighing more than 300 tons. For use as rotating components. shafts require toughness, strength and homogeneity, and therefore are produced through a variety of heat treatments. According to the increase of ingot size, micro- and macrosegregation and also mass effect of the product increase. Thus, special care should be paid to the heat treatment of such large shaft forgings. In this paper, the heat treatment of large shaft forgings such as rotor and back-up roll is calculated using the commercial finite element code SYSWELD. Calculated distributions of temperature and phase are compared with experimental data. The continuous cooling transformation diagram, thermal and mechanical properites of each phase are used. The phase proportion, hardness and residual stress during water quenching are discussed.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 춘계학술대회 논문집
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• pp.215-218
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• 2005

For the production of cold forged parts with near-net-shape attributes, the quality of the tool system is responsible for an essential portion of costs fer the finished components. Therefore, a tool lift is one of the important issues on cold forging industry. There are many complicated variables related with tool life, such as material, heat-treatment, coating, lubricant, process design. In this study, heat-treatment of tool material and lubricant are investigated to improve the tool life. Deep cryogenic treatment of tool steel is very efficient to improve the wear resistance due to the fine carbide. And, friction factor of lubricants for cold forging are measured by the ring compression test. Zinc-Phosphate and $MoS_2$ lubricant is effective to sustain the friction factor under 0.1.

• 대한기계학회논문집A
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• 제35권12호
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• pp.1663-1668
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• 2011

자동차 차체를 제작하는 프레스 금형의 가공공정 중 제품의 형태를 완성하는 드로잉 공정 및 불필요한 부분을 절단하는 트리밍 공정은 그 공정의 특성상 금형의 마모가 심하기 때문에 금형의 내마모성을 향상시키기 위한 표면경화처리가 요구되고 있다. 따라서 본 연구에서는 프레스 금형에 레이저 표면처리기술을 적용하기 위한 실험을 실시하였다. 드로잉 공정 및 트리밍 공정에 적합한 표면경화처리를 위해 다이오드 레이저를 이용하여 시험편의 평면부 및 모서리부를 열처리하였으며, 각각의 적정 열처리 조건을 도출하였다. 또한 시험편의 재료에 따른 열처리 특성을 비교하기 위해 구상흑연 및 편상흑연 주철을 사용하여 실험을 진행하였다. 실험 결과, 재료에 따른 열처리 특성에 차이가 있다는 것을 확인하였으며, 적정 열처리된 조건에서의 경화부는 모재에 비하여 약 3배 정도의 경도상승을 나타내었다.

• 열처리공학회지
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• 제25권4호
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• pp.190-195
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• 2012

This study aims to investigate and compare the microstructures and room temperature tensile properties for AZ91 and ECO-AZ91 (AZ91+0.3%CaO) alloys in as-cast, T4 and T6 states, respectively. In as-cast state, the ECO-AZ91 alloy has finer microstructure than the AZ91 alloy. The AZ91 alloy exhibits greater ductility, while YS and UTS are inferior to those of the ECO-AZ91 alloy. After T4 treatment, most of ${\beta}$ compounds disappear in the AZ91 alloy, whereas ${\beta}$ phase is still observed in the ECO-AZ91 alloy due to its enhanced thermal stability, resulting in lower values of ductility and UTS. In T6 state, YS and UTS are better in the ECO-AZ91 alloy.

• 한국분말재료학회지
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• 제20권4호
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• pp.245-252
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• 2013

This study attempted to manufacture a Cu-Ga coating layer via the cold spray process and to investigate the applicability of the layer as a sputtering target material. In addition, changes made to the microstructure and properties of the layer due to annealing heat treatment were evaluated, compared, and analyzed. The results showed that coating layers with a thickness of 520 mm could be manufactured via the cold spray process under optimal conditions. With the Cu-Ga coating layer, the ${\alpha}$-Cu and $Cu_3Ga$ were found to exist inside the layer regardless of annealing heat treatment. The microstructure that was minute and inhomogeneous prior to thermal treatment changed to homogeneous and dense with a more clear division of phases. A sputtering test was actually conducted using the sputtering target Cu-Ga coating layer (~2 mm thickness) that was additionally manufactured via the cold-spray coating process. Consequently, this test result confirmed that the cold sprayed Cu-Ga coating layer may be applied as a sputtering target material.

• KSBB Journal
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• 제20권1호
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• pp.50-54
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• 2005

셀룰로오스의 탄화과정에서는 셀룰로오스의 pyrolysis에 의 해 생산된 타르에 의해 탄화 후, 셀룰로오스 탄화물의 섬유구조를 저해시키는 문제점이 존재한다. 이와 같은 결과는 $800^{\circ}C$이상의 탄화온도와 건조 셀룰로오스를 toluene에 침지하고 초음파 처리 후 탄화한 탄화물에서 감소되지만, 섬유구조만의 탄화물을 얻을 수 없었다. 그러나 셀룰로오스의 탄화에서 타르의 생산을 감소시키는 HCI vapor flow 조건에서의 열처리 과정의 적용과 탄화과정 중 생성된 타르의 제거를 통해서 탄화 후, 대부분의 영역에서 섬유 구조를 갖는 탄화물을 얻을 수 있었다.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2003년도 추계학술대회논문집
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• pp.68-71
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• 2003

Heat treatment is one of the critical manufacturing processes that determine the quality of a product. This paper presents experimental and analytical results for the quench of a ring gear in stagnant oil. The goal of this study is to develop heat transfer predicting model in an overall analysis of the quenching process. Thermal conductivities which are dependant on temperatures and convection coefficients which are obtained by inverse method are used to develop the accurate heat transfer model. The results of heat transfer model have a good agreement with experimental results.

• 소성∙가공
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• 제13권5호
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• pp.441-448
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• 2004

Heat treatment is one of the critical manufacturing processes that determine the quality of a product. This paper presents experimental and analytical results for the quench of a ring gear in stagnant oil. The goal of this study is to develop heat transfer predicting model in an overall analysis of the quenching process, Thermal conductivities which are dependant on temperatures and convection coefficients which are obtained by inverse method are used to develop the accurate heat transfer model. The results of heat transfer model have a good agreement with experimental results.