• International Journal of Korean Welding Society
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• 제1권1호
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• pp.58-62
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• 2001

The surface of AC8A Ah alloy was modified by adding the Cu powder using a Plasma Transferred Arc (PTA) welding process. Under the optimum fabricating conditions, the modified surface of AC8A Ah alloy was observed to possess the sound microstructure with a minimum porosity. Hardness and wear resistance properties of the as-fabricated alloy were compared with those of the 76 heat-treated one. In case of the as-fabricated alloy, the hardness of the modified layer was twice that of the matrix region. Although significant increase in the hardness of the matrix region was observed after T6 heat treatment, the hardness of the modified layer was not observed to change. The wear resistance of the modified layer was significantly increased compared to that of the matrix region. The microstructure of a weld zone and the matrix region were investigated using the optical microscope, scanning electron microscope (SEM), electron probe microanalysis (EPMA), and transmission electron microscope (TEM). The primary and eutectic silicon in the weld zone were finer and more curved than in the matrix region, while some precipitates has had been found therein. According to the TEM observation, the predominant precipitate present in the weld zone was the $\theta$'phase, which is precipitated during cooling by rapid solidification in PTA welding process. Improvement of hardness and wear properties in the weld zone in the as-fabricated condition can be explained based on the presence of $\theta$’precipitates and fine primary and eutectic silicon distribution.

• Journal of Welding and Joining
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• 제33권1호
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• pp.61-71
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• 2015

The effect of welding condition on microstructure and mechanical property of Plasma-MIG Hybrid Weld between Al 5083 plates(thickness : 10mm) was investigated. 1 pass weld without any defects such as puckering, undercut, and lack of fusion was obtained by 150~200A of plasma current and 5~7mm of welding speed. Gas porosities and shrinkage porosities were existed in the weld near fusion line. As welding speed and plasma current were decreasing, the area fraction of porosity was increasing. The hardness of the weld is increasing as welding speed. On the basis of microstructural analysis, Mg segregated region near dendrite boundaries tends to increase with the welding speed. In the result of hardness test, Distribution of hardness in fusion zone showed little change with the plasma current. However, when the welding speed increased, hardness in weld metal markdly increased. It could be considered that effect of heat input to growth of the dendritic solidification structures. Based on tensile test, tensile properties of weld metal was predominated by area fraction of porosities. Consequently, tensile properties can be controlled by formation site and area fraction of porosity.

• 한국기계가공학회지
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• 제10권6호
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• pp.128-133
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• 2011

In this study, the steel material for shipbuilding(LR-A class) was used, and FCAW was taken advantage of 3G attitude and they are welded by different welding ways. As a result of analyzing wave with welding monitoring system, the stable values are obtained which are the first floor(electronic current 164~182 A, voltage 24 V), the second floor(electronic current 174~190 A, voltage 22~25 V), the third floor(electronic current 158~188 A, voltage 22~25 V), and fourth floor(electronic current 172~184 A, voltage 22~25 V), at this time, the stable wave standard deviation and changing coefficient could be obtained. When the welding testing through nondestructive inspection was analyzed know defect of welding, there was no defect of welding in A, D, E, but some porosities in B, and slag conclusion near the surface in C, because the length of arc was not accurate, and the electronic current and voltage was not stable. After observing the change of heat affect zone through micro testing, each organization of floor formed as Grain Refinement, so welding part was fine, the distance of heat affect zone is getting wider up to change the values of the electronic current and voltage. As a result of degree of hardness testing, the hardness orders were the heat affect zone(HAZ), Welding Zone(WZ), and Base Metal(BM). When the distribution of degree of hardness is observed. B is the highest degree of hardness The reason why heat effect zone is higher than welding zone and base metal, welding zone is boiled over melting point($1539^{\circ}C$) and it starts to melt after the result of analysis through metal microscope, so we can know that delicate tissue is created at the welding zone. Therefore, in order to get the optimal conditions of the welding, the proper current of the welding and voltage is needed. Furthermore the precise work of welding is required.

• 한국표면공학회지
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• 제45권3호
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• pp.130-135
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• 2012

Hydrogen charging was electrochemically conducted at high strength DP steels and TRIP steel with varying charging time. The penetration depths and the mechanical properties with charging conditions were investigated through the distribution of micro-hardness and the microstructural observation of the subsurface zone. The micro-Vickers hardness was measured to evaluate the hydrogen embrittlement of subsurface zone in addition to the microscope investigation. It was shown that the hydrogen amounts decreased in DP steels and TRIP steel with increasing hydrogen charging time. As shown by micro-Vickers hardness test and small punch test results, micro-Vickers hardness and SP energy for DP steels and TRIP steel decreased with increasing hydrogen charging time, for constant value of charging current density. SEM investigation results for the hydrogen contained samples showed that the major fracture behavior was brittle fracture which results in dimples on fractured surface and the size of dimples were decreased with increasing hydrogen charging time. These results indicate that hydrogen embrittlement is the major cause for the fracture of high strength steels and also micro-Vickers hardness test and small punch test is a valuable test method for hydrogen embrittlement of high strength sheet steels.

• The Journal of Advanced Prosthodontics
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• 제16권2호
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• pp.115-125
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• 2024

PURPOSE. The purpose of this in vitro study was to investigate the fracture resistance, surface hardness, and color stain of 3D printed, CAD-CAM milled, and conventional interim materials. MATERIALS AND METHODS. A total of 80 specimens were fabricated from auto polymerizing polymethyl methacrylate (PMMA), bis-acryl composite resin, CAD-CAM polymethyl methacrylate resin (milled), and 3D printed composite resin (printed) (n = 20). Forty of them were crown-shaped, on which fracture strength test was performed (n = 10). The others were disc-shaped specimens (10 mm × 2 mm) and divided into two groups for surface hardness and color stainability tests before and after thermal cycling in coffee solution (n = 10). Color parameters were measured with a spectrophotometer before and after each storage period, and color differences (CIEDE2000 [DE00]) were calculated. The distribution of variables was measured with the Kolmogorov Smirnov test, and one-way analysis of variance (ANOVA), Tukey HSD, Kruskal-Wallis, Mann-Whitney U tests were used in the analysis of quantitative independent data. Paired sample t-test was used in the analysis of dependent quantitative data (P < .05). RESULTS. The highest crown fracture resistance values were determined for the 3D printed composite resin (P < .05), and the lowest were observed in the bis-acryl composite resin (P < .05). Before and after thermal cycling, increase in mean hardness values were observed only in 3D printed composite resin (P < .05) and the highest ΔE₀₀ value were observed in PMMA resin for all materials (P < .05). CONCLUSION. 3D printing and CAD-CAM milled interim materials showed better fracture strength. After the coffee thermal cycle, the highest surface hardness value was again found in 3D printing and CAD-CAM milled interim samples and the color change of the bis-acryl resin-based samples and the additive production technique was higher than the PMMA resin and CAD-CAM milled resin samples.

• Journal of Welding and Joining
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• 제4권2호
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• pp.21-29
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• 1986

The influence of welding heat input variation(600-900J/cm) and heat-treatment condition after welding on tensile strength of butt welded joint in $175Kg/mm^2$ strength level Maraging steel(Co-free and Co-containing) sheets was investigated on the basis of hardness distribution, microstructure of weld metal and fracture surface. The obtained main results are as follows; 1. The strength of weldment (UTS, NTS), joint efficiency showed a little decreasing tendency with the increase in welding heat input, and the elongation showed a little increasing tendency with the increase in the width of weld metal. It was considered because of the plastic constraint of the high strength base metal. 2. The strength of weldment was better in the solution treatment and aging than the aging only after welding due to the disappearance of almost denverite in weld metal. 3. The hardness distribution in weldment after welding and heat-treatment was almost similar to both Co containing and Co free Maraging steel with change in welding heat input. 4. The fracture was occurred at weld metal, and the fracture surface showed a relatively shallow dimples in both Co containing and Co free Maraging steel.

• 한국재료학회지
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• 제20권11호
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• pp.581-585
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• 2010

High strength sheet steels for automobile are seriously compromised by hydrogen embrittlement. This issue has been continuously studied, but the field of interest, which lies between microstructural characteristics and hydrogen behavior with hydrogen charging, has not yet been thoroughly investigated. This study was done to investigate the behavior of hydrogen according to the hydrogen volume fraction on 590MPa grade DP steels, which are developed under hydrogen charging conditions as high strength sheet steels for automobiles. The penetration depths and the mechanical properties, according to charging conditions, were investigated through the distribution of micro-hardness and the microstructural observation of the subsurface zone. It was found that the amount of hydrogen trapping in 590MPa DP steels was related to the austenite volume fraction. It was confirmed that the distribution of micro-hardnesses according to the depth of the subsurface zone under the free surface showed the relationship of the depth of the hydrogen saturation between the charging conditions.

• 대한기계학회논문집
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• 제8권3호
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• pp.224-231
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• 1984

본 연구에서는 이상과 같은 점을 고려하고, 인장시험을 통해 최대용접강도를 나타내는 최적용접조건을 구한 다음, 최적조건하에서 박강판을 1점 점용접한 재료의 너깃주위에 관찰되는 파괴거동을 광탄성 응력분포거동과 관련시켜 고찰하였다.

• 한국주조공학회지
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• 제4권1호
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• pp.5-11
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• 1984

Green compressive strength, permeability, deformation, flowability, compactability and green hardness values at room temperature are dependable on the grain distribution and grain shape. The results obtained under constant moisture (4% for sand) and bentonite (8% for sand) were as follows; 1. With decreasing grain size, surface area of sand grain was increased. 2. With decreasing grain size, coefficient of angularity was increased. 3. As surface area increased from $8926.43cm^2$ to $21211.16cm^2$ , green compressive strength was increased from $210.93\;g/cm^2$ to $449.98\;g/cm^2$, hardness was increased from 76.7 to 82.3, but permeability was decreased from $411.7\;{\frac{\;cc\;{\cdot}\;cm\;}{atm\;{\cdot}\;cm^2\;{\cdot}\;min.}}$ to $113.7\;{\frac{\;cc\;{\cdot}\;mm\;}{atm\;{\cdot}\;cm^2\;{\cdot}\;min.}}$ 4. As surface area increased from $8926.43\;cm^2$ to $21211.16\;cm^2$, flowability was decreased from 82.3% to 80.8%, deformation was decreased from $67.1\;cm\;{\times}\;10^{-3}$ to $54.6\;cm\;{\times}\;10^{-3}$, but compactability was increased from 44.8% to 54.3%. 5. Room temperature properties of molding sand were affected by variation of surface area.

• 한국재료학회지
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• 제13권2호
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• pp.120-125
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• 2003

A low melting borosilicate glass frit was used as an adhesion promoter, which enables $MnWO_4$to be sintered with in a reasonable sintering temperature range ($800∼1000^{\circ}C$). The glass was evaluated for glass transition temperature ($Τ_{g}$ X) and thermal expansion coefficient($\alpha$). Mechanical property (Vickers hardness), grain growth, the comparison of lattice parameter and pore distribution of sintered $MnWO_4$ with the frit were methodically discussed. As sintering temperature increased, a typical liquid phase sintering showed the rapid grain growth and high densification of X$MnWO_4$grain, improvement of hardness (until $920^{\circ}C$) and different pore size distribution. Resistance of sintered $MnWO_4$varied from 450k$\Omega$ to 8.8M$\Omega$ under the measuring humidify ranging from 30 to 90%. Thus, the results will contribute to the application of glass frit containing sensor materials and their future use.