• Proceedings of the Korean Society for Food Science of Animal Resources Conference
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• 2004.05a
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• pp.283-286
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• 2004

본 연구는 노계육의 화염처리 조건에 따른 pH, 드립발생, 육색, 도체특성 변화를 살펴보기 위하여 실시되었다. pH는 저장 3일에서도 화염 중처리와 강처리구에서 5.76, 5.96으로 무처리구보다 높은 경향을 나타냈으나, 저장 5일에서는 처리별 비슷한 경향을 나타냈다. 드립 발생율은 저장기간이 증가할수록 처리구와 상관없이 증가하는 경향을 나타냈으며, 저장 5일에 화염을 80PSI으로 처리한 구에서 0.55%으로 무처리보다 2.7배 정도 드립발생율이 저하되었다. 노계육의 황색도($b^{\ast}$)는 저장 1일의 가슴살 경우 화염처리를 하지 않는 구에서 6.07를 나타냈으며, 중처리 및 강처리로 높일수록 9.77, 11.77으로 점차 증가하는 경향을 나타냈다. 깃털유무는 화염처리 하지 않는 처리구에서 평균 5.7개를 나타냈으나 화염이 강도 80PSI로 증가하였을 때 2.3개로 현저히 저하되었다. 잔모는 화염을 처리하지 않는 처리구에서는 잔모가 약간 분포되어있는 수준이 55,6%이었으나 강처리구에서는 5.6%까지 저하되는것을 확인할 수 있었다. 종합적으로 판단하여 볼 때 노계육의 화염 처리는 80PSI 수준까지 올려도 가능할 것으로 사료된다.

• Proceedings of the KOSOMBE Conference
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• v.1996 no.05
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• pp.283-287
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• 1996

This paper described the estimator and eliminator far three kinds of artifacts in electrocardiogram. The most efficient estimation of baseline drift could be obtain in the cubic spline interpolation method with the PQ and TP segment which are considered to be isoelectric, from the experimental results obtained from the applied 4 types of algorithms. The time loss and distortion could be avoided with the aid of detection criteria by checking if baseline drifts exist or not. The AIEF proposed in this paper was verified as having the best removal performance with less distortion in the QRS complex through the comparison of 5 proposed algorithms. furthermore, the AIEF are most suitable far the ECG analyzer which was only needed relatively short time data due to the fast conversion into the stable state. The proposed parabolic filter with 11 points width was identified as having the best performance for the elimination of muscle artifacts. Also we could obtain 99.7% detection accuracy of spike component and minimize the error identifying QRS complex as spike.

• The Journal of Asian Finance, Economics and Business
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• v.9 no.2
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• pp.283-294
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• 2022

This holistic research focused on the interactive relationship of different factors with a unique relationship with the dependent variable. The first research objective of the study was to identify the most significant factor that has an impact on Job performance while being mediated. The second objective was to see the moderating effect of gender on the relationship between transformation leadership and innovation on job performance. This research followed a purely quantitative research paradigm with a structured questionnaire to quantify the information collected from 96 respondents for the empirical analysis. For testing the research hypotheses, IBM SPSS version 24 and SmartPLS version 3.2.8 softwares were used to run the structural equation modeling to establish the causal relationship between the study variables. Most of the variables were found with a significant impact on job performance. Further, the hypotheses H³, H⁶, and H¹⁰ were rejected as these contributed insignificant towards the research model. This research was limited to specific educational institutions and businesses, and the timeframe was restrictive. The findings of this research can benefit policymakers and the operational side of various industries. Future research may consider the difference in gender in predicting employee engagement through leadership and innovation.

• Journal of the Korean Chemical Society
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• v.21 no.4
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• pp.276-283
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• 1977

Reduction of dichromate at a platinum cathode in acid solution was studied by cyclic voltammetry and controlled potential electrolysis. Cathodic polarization curve consisted of three waves in unbuffered solution of potassium dichromate having initial pH ranges 1.5∼4.0, with sodium sulfate as the supporting electrolyte. Relative heights of the first and the second waves were, respectively, a function of chromium (Ⅵ) concentration and activity of hydrogen ion, but that of the third wave was not proportional to both of them. The current of the first two peaks were proportional to the sweep rate of potential (${\nu}$), while that of the last peak vs. ${\nu}^{1/2}$ was linear at the sweep rate of less than 50mV/sec. By the controlled potential electrolysis, the reduction of chromium (Ⅵ) was almost completely suppressed at potentials more negative than the last peak and at initial pH's above ca. 2.3 of unbuffered solution. Therefore, these peaks represented, respectively, $Cr_2O_7^{2-}{\to}Cr^{3+},\;2H^+{\to}H_2$ and the formation of a cathodic film.

• Journal of the Korean Chemical Society
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• v.7 no.4
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• pp.283-287
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• 1963

The distribution ratio of hydrogen cupferrate in $H_2O-CHCl_3$ system was considered as a function of pH ($HClO_4$), ionic strength ($NaClO_4$), and cupferron concentration in perchloric acid media, respectively. The values were independent upon pH (1.50∼3.00 range) and ionic strength (0.1∼2.00 range), but they increased as increasing the cupferron concentration in the acidic media. At the infinite dilution, the thermodynamic distribution ratio between chloroform and aqueous phase was 120. 0. The activity coefficients of hydrogen cupferrate in chloroform solution were determined by the distribution ratio. This activity coefficient may be calculated by using the empirical equation, $-log\;f_{CHCl3}=0.1285C_{CHCl3}+{7.775C^2}_{CHCl3}$ which represents the experimental data quite well for the solution in 0.1 mole/l order of hydrogen cupferrate concentration.

• Journal of Powder Materials
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• v.12 no.4 s.51
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• pp.279-283
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• 2005

In this study, the ZnS composite powders for host material in phosphor was synthesized in situ by mechanical alloying. As the mechanical alloying time increases, particle size of ZnS decreases. ZnS powders of $1.85\;\mu{m}$ in a mean size was fabricated by mechanical alloying for 10h. The crystal structures of ZnS powders were investigated by X-ray diffraction and the photo-luminescence properties was evaluated with the optical spectra analyzer. The steady state condition of mechanically alloyed ZnS was obtained as a mean particle size of $2\;\mu{m}$ in 5h milling. The sphalerite and wurtize structures coexist in the ZnS mechanically alloyed for 5h. The ZnS powder mechanically alloyed for 10h grows to the sphalerite structure. And the strong emission peaks of ZnS are observed at 480 nm wave length at the powders of mechanically alloyed for 10h, but the sphalerite and wurtize structures in ZnS coexist and emission peaks are not appeared at the powders of mechanically alloyed for 10h.

• Journal of Hydrogen and New Energy
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• v.22 no.4
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• pp.424-431
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• 2011

The Sulfur-Iodine(SI) thermochemical hydrogen production process consists of three sections, which are so called the Bunsen reaction section, the $H_2SO_4$ decomposition section and the HI decomposition section. In order to identify the phase separation characteristics in the reaction conditions with the high solubility of $SO_2$, we conducted the Bunsen reaction at the low temperatures, ranging from 283 to 298K, with the $I_2/H_2O$ molar ratios of 2.5/16.0 and 3.5/16.0. The molar ratios of HI/$H_2SO_4$ products obtained from low temperature Bunsen reactions were ca. 2, indicating that there were no side reactions. The amount of reacted $SO_2$ was increased with decreasing the temperature, while the amounts of unreacted $I_2$ and $H_2O$ were decreased. In the phase separation of the products, the amount of a $H_2SO_4$ impurity in $HI_x$ phase was increased with decreasing the temperature, though the temperature has little affected on HI and $I_2$ impurities in $H_2SO_4$ phase.

• Journal of the Korean Chemical Society
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• v.58 no.3
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• pp.283-288
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• 2014

A column solid phase extraction procedure based on modified polyurethane foam (PUF) by a newly synthesized Schiff base ionophore, named 2,2'-{iminobis[propane-3,1-diylnitrilo(1E)prop-1-yl-1-ylidene]}diphenol, was developed for preconcentration step of trace amounts determination of copper ions in water samples by atomic absorption flame spectroscopy. The influence of parameters on the adsorption process such as sample pH, amount of modified PUF packed in the column, type and volume of stripping reagent and its flow rate were investigated and optimized. Under optimum experimental conditions, the calibration graph was linear in a relatively wide range ($0.005-210{\mu}g/ml$) with a limit of detection $0.002{\mu}g/ml$ of copper. The proposed method allows achieving to a concentration factor of >133. The capacity of a column (1.6 cm i.d.) packed by 6 g of PUF modified by 12 mg of the Schiff base was found to be $247.7({\pm}2.1){\mu}g$ of copper. It was found that the adsorption process was highly selective towards copper ions with respect to some associated metal ions. The presented procedure was successfully applied for determination of copper in some water samples.

• Journal of Food Hygiene and Safety
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• v.13 no.3
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• pp.206-212
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• 1998

An improved antibody-coated sensor system based on quartz crystal microbalance was developed for the detection of Salmonella spp. An antibody against Salmonella common structural antigen was immobilized onto one gold electrode of the piezoelectric quartz crystal surface by various immobilization procedures. The best results in sensitivity and stability were obtained with the thin layers of protein A and 3,3'-dithiopropionimidate.2HCI(DTBP), a homobifunctional thiol-cleavable crosslinker. After the addition of a S. typhimurium suspension into a reaction cell with 0.1 M sodium phosphate buffer, pH 7.2, the resonant frequency owing to S. typhimurium adsorption decreased conspicuously. The antibody-immobilized crystals prepared by the gold-protein A complex formation and DTBP thiolation showed the frequency shifts of 80 and 283 Hz, respectively. The time required for maximum frequency shift was about 30~60 min. The antibody-coated crystal could be reused for 6~8 consecutive assays.

• Proceedings of the Korean Vacuum Society Conference
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• 2014.02a
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• pp.283.2-283.2
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• 2014

열필라멘트 화학증착공정(Hot Wire Chemical Vapor Deposition)에서 기상 에서 생성되는 하전된 실리콘 나노입자와 저온결정성 실리콘박막 증착의 연관성을 압력의 변화에 따른 상호비교를 통해 조사하였다. 필라멘트 온도는 $1800^{\circ}C$로 고정시키고 0.3~2 torr의 범위에서 공정 압력을 변화시키면서 증착하였다. 압력이 증가함에 따라 증착된 실리콘 박막의 결정화도는 증가하였으며, 증착속도는 감소하였다. 반응기 압력에 따른 기상에서 생성되는 나노입자의 크기분포의 변화를 조사하기 위하여 탄소막이 코팅된 투과전자현미경(Transmission Electron Microscopy) 그리드 위에 실리콘 나노입자를 포획하고 관찰하였다. 포획된 실리콘 나노입자의 크기분포와 개수농도는 압력이 증가함에 따라 감소하였다. 투과전자현미경을 이용하여 분석한 결과, 나노입자는 결정성 구조를 보였다. 압력이 증가함에 따라 나노입자의 크기가 감소하고 개수농도가 감소하는 것은 증착속도의 감소와 관련됨을 알 수 있다. 한편, 공정압력 증가에 따른 나노입자의 크기분포 및 개수농도 감소와 증착속도의 감소는 일반적으로 알려진 기상에서 석출하는 고상의 평형석출량(equilibrium amount of precipitation)이 압력의 증가함에 따라 증가한다는 사실과 일치하지 않는다. 이러한 압력경향성은 Si-H 시스템이 0.3~2 torr의 압력 영역에서 retrograde solubility를 갖는 것을 의미한다. 나노입자의 하전여부, 크기분포 및 개수농도를 측정하기 위하여 입자빔질량분석장비(Particle Beam Mass Spectroscopy)를 이용하였다. 그 결과, 실리콘 나노입자는 양 또는 음의 극성을 가진 하전된 상태임을 확인하였고, 투과전자현미경(TEM) grid에 포획한 실리콘 나노입자의 크기와 경향성이 일치하였다. 이는 나노입자가 저온의 기판에서 핵생성되어 성장하여 생성된 것이 아니라 열필라멘트 주위의 고온영역에서 생성된 것을 의미한다.