• Title/Summary/Keyword: Green body density

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FE Analysis of Alumina Green Body Density for Pressure Compaction Process (압축성형공정에 대한 알루미나 성형체 밀도분포의 FE 분석)

  • Im, Jong-In;Yook, Young-Jin
    • Journal of the Korean Ceramic Society
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    • v.43 no.12 s.295
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    • pp.859-864
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    • 2006
  • For the pressure compaction process of the ceramic powder, the green density is very different with both the ceramic body shape and the processing conditions. The density difference cause non-uniform shrinkages and deformations, and make cracks in the sintered ceramics. In this paper, Material properties of the alumina powder mixed with binder and the friction coefficient between the powder and the tool set were determined through the simple compaction experiments: Also the powder flow characteristics were simulated and the green density was analyzed during the powder compaction process with Finite Element Method (FEM). The results show that the density distributions of the green body were improved at the optimized processing condition and both the possibility of the farming crack generation and rho deformation of the sintered Alumina body were reduced.

Fabrication of Light Aggregates Using the Fly Ash-Clay Slurry

  • Seunggu Kang;Lee, Kigang;Kim, Jungwan
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.06a
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    • pp.81-86
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    • 1998
  • The light aggregates were fabricated by sintering green bodies made form the fly ash-clay alip. The content of fly ashes in the slip could be increased up to 70wt.% due to controlled rheological behavior of the slip, and the green body of uniform microstructure could be obtained by DCC(Direct Coagulation Casting)method. The apparent density, microstructure and compressive strength for sintered bodies fired at 1100∼1200$^{\circ}C$ were evaluated. The properties of light aggregates fabricated depend on slip density, particle behavior in the slip and sintering conditions. The sintered body prepared by firing a green body made from slip of density 1.60 at 1150$^{\circ}C$/2hr satisfied conditions of a light aggregate as apparent density of 1.49${\pm}$0.02 and compressive strength of 584${\pm}$62kg/$\textrm{cm}^2$.

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Correlation of the Green Microstructure of ZrO2 with the Colloid/Interface Variables (Zirconia성형체의 미세구조와 콜로이드/계면변수와의 상관관계에 대한 분석)

  • 장현명;한규호;이기강;정한남
    • Journal of the Korean Ceramic Society
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    • v.27 no.1
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    • pp.91-101
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    • 1990
  • The green microstructure and sintering behavior of ZrO2 were analyzed in terms of kinetic stability (measured by the stability ratio ; W) and interfacial characteristics of colloidal suspension. Green density and the most frequent pore radius(MFPR) of green body were directly correlated with the stability ratio. These observations were explained using a concept of the critical stability ratio(Wc) and the potential energy of two interacting particles in colloidal suspension. Analysis of the data also indicates that the potential energy barrier between two interacting colloid particles should be higher than its critical value for a fabrication of ZrO2 green body with dense and uniform microstructure. Besides, we have successfully applied a concept of the donoracceptor interaction to increase the kinetic stability of ZrO2 slip and density of green body.

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Comparison of the Finite Element Analysis and Experimental Result for Green Body Density of Alumina Ceramics (알루미나 압축성형체의 성형밀도와 유한요소 시뮬레이션 결과의 비교)

  • Yook, Young-Jin;Im, Jong-In
    • Journal of the Korean Ceramic Society
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    • v.44 no.4 s.299
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    • pp.235-239
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    • 2007
  • For the pressure compaction process of the ceramic powder, the density distribution is very important for the uniform shrinkages at the sintered body. In this paper, we fabricated alumina green body using compaction process and simulated about same condition. Then comparison of simulation and experimental result confirmed that accuracy of simulation. On the average density of top and lower part was each $2.41g/cm^3,\;2.27g/cm^3$ and deviation at final step was calculated with 0.06 in simulation. Also, experiments show that total density of top and lower part was each $2.59g/cm^3,\;2.36g/cm^3$, and deviation was 0.09. Conclusion, that was not a difference to the simulation and experimental result. The application using the finite element simulation method is possible optimization of the compressing process, predict generated part of cracks and there is a possibility of getting result of more fast, more accurate then existing experience method.

Effect of Polymeric Binders on Green body Properties of WC-Co Cemented Carbides (초경합금 성형체 특성 변화에 미치는 유기물 결합제의 영향)

  • Lim, Young-Soo;Ahn, Sun-Yong;Lim, Jae-Suk;Paek, Yeong-Kyeun;Chung, Tai-Joo
    • Journal of Powder Materials
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    • v.29 no.4
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    • pp.291-296
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    • 2022
  • The green body of WC-Co cemented carbides containing polymeric binders such as paraffin, polyethylene glycol (PEG), and polyvinyl acetate (PVA) are prepared. The green density of the WC-Co cemented carbides increases with the addition of binders, with the exception of PVA, which is known to be a polar polymeric substance. The green strength of the WC-Co cemented carbides improves with the addition of paraffin and a mixture of PEG400 and PEG4000. In contrast, the green strength of the WC-Co does not increase when PEG400 and PEG4000 is added individually. The compressive strength of the green body increases to 14 MPa, and the machinability of the green body improves when more than 4-6 wt% paraffin and a mixture of PEG400 and PEG4000 is used. Simultaneously, the sintered density of WC-Co is as high as 99% relative density, similar to a low binder addition of 1-2 wt%.

Preparation of Alumina Ceramics by Pressureless Powder Packing Forming Method: (I) Development of Pressureless Powders Packing Forming Method and Characterization of Green Body (무가압 분말 충전 성형법을 이용한 알루미나 세라믹스의 제조: (I) 무가압 분말 충전 성형법 개발 및 성형체 특성 관찰)

  • 박정현;성재석;이상진
    • Journal of the Korean Ceramic Society
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    • v.31 no.1
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    • pp.31-38
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    • 1994
  • To overcome the demerit of conventional forming method, new forming method, pressureless powder packing forming method, was investigated. This technique is performed by powder packing followed by the infiltration of binder solution. Various alumina powders were used as starting materials and the powders showing good packing condition through powder packing experiment were chosen. The green densities prepared by this new forming method with these powders were lower than those of specimens by pressing method, but, nearly same density was obtained in case of green body prepared with the powders having high packing density. The distribution of binder in a green body was homogeneous and it was possible to a complex shape form by this forming method.

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Microstructures and Drying of the Alumina Green Body by the Gel-Casting Method (Gel-Casting으로 제조한 알루미나 성형체의 건조와 미세구조)

  • 오창준;이홍림
    • Journal of the Korean Ceramic Society
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    • v.31 no.12
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    • pp.1467-1474
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    • 1994
  • The effects of the dispersion, drying, and binder burning-out on the green-microstructures of gelcasted alumina were studied. The slip consisting of 55 vol% alumina powder and 5 wt% organic materials was well-dispersed by adding 0.28 wt% polyelectrolyte polymer. Green bodies were dried at >85% relative humidity at room temperature. Green-microstructures were observed to be depended on the heating rate during binder burnout. Constant drying rate was not observed in drying process of gelcasted alumina. Sintered body showed its relative density higher than 99% when it was sintered at 1$600^{\circ}C$ for 2 hours.

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Simulation of Sintering for the Complex Ceramic Bodies by NASTRAN

  • Lee, Sang-Ki;Kim, Hyung-Jong;Lee, June-Gunn
    • The Korean Journal of Ceramics
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    • v.5 no.3
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    • pp.235-238
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    • 1999
  • In a ceramic green body, some degree of nonuniformity in density always presents. These differences in green density will appear as nonuniform shrinkage after sintering takes place. For the complex ceramic bodies with various curves and angles, therefore, it is quite difficult to foresee the final dimensions precisely after sintering. This simulation study shows that, considering the sintering process as a thermal shrinkage phenomenon, the use of NASTRAN enables to predict the precise shape of a sintered body. Based on this result, 'the reverse engineering technique' has been developed that can unfold the exact dimensions of a green body to have the desired shape after sintering. This approach will provide a simple and useful tool for ceramic engineers to fabricate complicate bodies with tight dimensional tolerances.

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Effects of green tea or $Sasa$ $quelpaertensis$ bamboo leaves on plasma and liver lipids, erythrocyte Na efflux, and platelet aggregation in ovariectomized rats

  • Ryou, Sung-Hee;Kang, Min-Sook;Kim, Kyu-Il;Kang, Young-Hee;Kang, Jung-Sook
    • Nutrition Research and Practice
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    • v.6 no.2
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    • pp.106-112
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    • 2012
  • This study was conducted to investigate the effects of $Sasa$ $quelpaertensis$ bamboo and green tea on plasma and liver lipids, platelet aggregation, and erythrocyte membrane Na channels in ovariectomized (OVX) rats. Thirty female rats were OVX, and ten female rats were sham-operated at the age of 6 weeks. The rats were divided into four groups at the age of 10 weeks and fed the experiment diets: sham-control, OVX-control, OVX-bamboo leaves (10%), or OVX-green tea leaves (10%) for four weeks. Final body weight increased significantly in the OVX groups compared with that in the sham-control, whereas body weight in the OVX-green tea group decreased significantly compared with that in the OVX-control ($P$ < 0.01). High density lipoprotein (HDL)-cholesterol level decreased in all OVX groups compared with that in the sham-control rats ($P$ < 0.05) but without a difference in plasma total cholesterol. Plasma triglycerides in the OVX-green tea group were significantly lower than those in the sham-control or OVX-control group ($P$ < 0.05). Liver triglycerides increased significantly in the OVX-control compared with those in the sham-control ($P$ < 0.01) but decreased significantly in the OVX-green tea group compared with those in the OVX-control or OVX-bamboo group ($P$ < 0.01). Platelet aggregation in both maximum and initial slope tended to be lower in all OVX rats compared with that in the sham-control rats but was not significantly different. Na-K ATPase tended to increase and Na-K cotransport tended to decrease following ovariectomy. Na-K ATPase decreased significantly in the OVX-green tea group compared with that in the OVX-control group ($P$ < 0.01), and Na-K cotransport increased significantly in the OVX-bamboo and OVX-green tea groups compared with that in the OVX-control ($P$ < 0.05). Femoral bone mineral density tended to be lower in OVX rats than that in the sham-control, whereas the green tea and bamboo leaves groups recovered bone density to some extent. The results show that ovariectomy caused an increase in body weight and liver triglycerides, and that green tea was effective for lowering body weight and triglycerides in OVX rats. Ovariectomy induced an increase in Na efflux via Na-K ATPase and a decrease in Na efflux via Na-K cotransport. Furthermore, consumption of green tea and bamboo leaves affected Na efflux channels, controlling electrolyte and body water balance.

The Hypocholesterolemic Effect of Green Tea EGCG Was Not Mediated Via the Stimulation of the Low-Density Lipoprotein Receptor Gene Expression in Cholesterol-Fed Rats

  • Moon Hee-Jung;Kim Yangha
    • Nutritional Sciences
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    • v.8 no.3
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    • pp.175-180
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    • 2005
  • Green tea, which has high polyphenols amount, is thought to have hypocholesterolemic effects. The present study was performed to further examine the hypocholesterolemic action of green tea, especially (-) epigallocatechin gallate (EGCG) for its effect on diet-induced hypercholesterolemia in rats. Male Sprague-Dawley rats (n=15) were fed a green tea-free diet (control), $1.0\%$ green tea catechin (catechin) or $0.5\%$ green tea catechin EGCG for seven weeks. Hypercholesterolemia was induced by adding $1\%$ cholesterol and $0.5\%$ cholic acid to all diets. There was no difference in food intake and body weight gain among the groups. The green tea EGCG treatment led to a significant improvement in plasma levels of total cholesterol, low density lipoprotein (LDL)-cholesterol and high density lipoprotein (HDL)/LDL ratio (p<0.05). There was no significant effect on the plasma HDL-cholesterol level. The catechin treatment led to a 4.19-fold increase in the LDL-receptor mRNA level compared to the control, but the EGCG treatment did not affect the hepatic LDL-receptor mRNA level. Our results suggest that when blood cholesterol level is down-regulated by green tea EGCG, the LDL receptor gene-independent pathway may dominate the hypocholesterolemic action of EGCG.