• 제목/요약/키워드: Grain sizes

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EBSD측정에 의한 반복겹침접합압연된 무산소동의 두께방향으로의 미세조직 변화 분석 (Microstructural Evolution Analysis in Thickness Direction of An Oxygen Free Copper Processed by Accumulative Roll-Bonding Using EBSD Measurement)

  • 이성희;임차용
    • 한국재료학회지
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    • 제24권11호
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    • pp.585-590
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    • 2014
  • Microstructural evolution in the thickness direction of an oxygen free copper processed by accumulative rollbonding (ARB) is investigated by electron back scatter diffraction (EBSD) measurement. For the ARB, two copper alloy sheets 1 mm thick, 30 mm wide and 300 mm long are first degreased and wire-brushed for sound bonding. The sheets are then stacked and roll-bonded by about 50% reduction rolling without lubrication at an ambient temperature. The bonded sheet is then cut to the two pieces of the same dimensions and the same procedure was repeated on the sheets up to eight cycles. The specimen after 1 cycle showed inhomogeneous microstructure in the thickness direction so that the grains near the surface were finer than those near the center. This inhomogeneity decreased with an increasing number of ARB cycles, and the grain sizes of the specimens after 3 cycles were almost identical. In addition, the aspect ratio of the grains decreased with an increasing number of ARB cycles due to the subdivision of the grains by shear deformation. The fraction of grains with high angle grain boundaries also increased with continuing process of the ARB so that it was higher than that of the low angle grain boundaries in specimens after 3 cycles. A discontinuous dynamic recrystallization occurred partially in specimens after 5 cycles.

기계적합금화한 (Al +12.5%Cu)3Zr 초미립 금속간화합물의 CIP 성형 및 소결 거동 (Cold Isostatic Pressing and Sintering Behavior of (Al +12.5%Cu)3Zr Nanocrystalline Intermetallic Compound Synthesized by Mechanical Alloying)

  • 문환균;홍경태;김선진
    • 한국재료학회지
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    • 제12권8호
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    • pp.634-640
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    • 2002
  • To improve the ductility of mTEX>$(Al +12.5%Cu)<_3$Zr intermetallics, which are the potential high temperature structural materials, the mechanical alloying behavior, the effect of pressure and temperature on the $Ll_2$, phase formation and the behavior of the cold isostatic press and sintering were investigated. However mechanically alloyed A1$_3$Zr alloy have been known to have high mechanical strength even at high temperature, its workability was poor. A method of solution is refined grain size and phase transformation from $DO_{23}$ to $Ll_2$.$ Ll_2$ structure TEX>$(Al+12.5%Cu)<_3$Zr with nanocrystalline microstructure intermetallic powders where were prepared by mechanical alloying of elemental powders. Grain sizes of the as milled powders were less than 10nm (from transmission electron microscopy, TEM). Thermal analyses showed that $Ll_2$ structure was stable up to$ 800^{\circ}C$ for 1hour $(Al+ 12.5%Cu)<_3$Zr. $(Al+12.5%Cu)<_3$Zr has been consolidated by cold isostatic pressing (CIP 138, 207, 276, 414MPa) at room temperature and subsequent heat treatment at high temperatures where $Ll_2$ structure was stable under vacuum atmosphere. The results showed that 94.2% density of Ll$_2$ compacts was obtained for the (Al +12.5%Cu)$_3$Zr by sintering at 80$0^{\circ}C$ for 1hour (under CIPed 207MPa). This compact of the grain size was 40nm.

800 MPa급 고강도강 용접금속의 미세조직 특성 비교 연구 (Microstructural Characteristics of 800 MPa Grade High Strength Steel Weld Metals)

  • 이재희;김상훈;윤병현;김환태;길상철;이창희
    • Journal of Welding and Joining
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    • 제29권1호
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    • pp.65-73
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    • 2011
  • Microstructural characteristics of two high strength (600 MPa & 800 MPa) weld metals produced by flux-cored arc welding process (FCAW) were evaluated. The 600 MPa grade weld metal was consisted of 75% acicular ferrite and 25% ferrite which was formed at relatively high temperature (grain boundary ferrite, widmanstatten ferrite, polygonal ferrite). However, the 800 MPa grade weld metal was composed of about 85% acicular ferrite and 15% low temperature forming phases (bainite, martensite). The prior austenite grain size of 800 MPa grade weld metal was decreased by solute drag force. The compositions and sizes of inclusions which are the dominant factors for the formation of acicular ferrite were analyzed by a transmission electron microscopy (TEM). In both 600 MPa and 800MPa grade weld metals, the inclusions were mainly consisted of Ti-oxide and Mn-oxide, and the average size of inclusions was $0.7{\mu}m$. The 800 MPa grade weld metal exhibited higher tensile strength and similar toughness compared with the 600 MPa grade weld metal. This result is mainly due to a higher fraction of low temperature products and a lower fraction of grain boundary ferrite in the 800 MPa grade weld metal.

제어압연한 베이나이트계 고강도강의 인장 및 충격 성질 (Tensile and Charpy Impact Properties of High-Strength Bainitic Steels Fabricated by Controlled Rolling Process)

  • 성효경;신상용;황병철;이창길;김낙준;이성학
    • 대한금속재료학회지
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    • 제48권7호
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    • pp.615-624
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    • 2010
  • This study is concerned with tensile and Charpy impact properties of high-strength bainitic steels fabricated by controlled rolling process. Six kinds of steels were fabricated by varying finish rolling temperature, start cooling temperature, and cooling rate, and their microstructures and tensile and Charpy impact properties were investigated. Their effective grain sizes were also characterized by the electron backscatter diffraction analysis. The microstructures of the steels rolled in the single phase region were most similar to those of the steels rolled in the two phase region. The steels cooled from $700{^{\circ}C}$ were composed mainly of granular bainites, while those cooled from $600{^{\circ}C}$ contained a number of bainitic ferrites, which resulted in the decrease in ductility and upper shelf energy in spite of the increase in strength. In the steels cooling from $600^{\circ}C$, fine acicular ferrites were well formed when the cooling rate was slow, which led to the best combination of high ductility, high upper shelf energy, and low energy transition temperature according to the decrease in the overall effective grain size due to the presence of acicular ferrites having smaller effective grain size.

급속소결에 의한 Ti와 TiH2로부터 나노구조의 Ti 제조 및 기계적 특성 (Fabrication of Nanostructured Ti from Ti and TiH2 by Rapid Sintering and Its Mechanical Properties)

  • 김나리;조성욱;김원백;손인진
    • 대한금속재료학회지
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    • 제50권1호
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    • pp.34-38
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    • 2012
  • Titanium has good deformability, high hardness, high biocompatibility, excellent corrosion resistance and low density. Due to these attractive properties, it has been used in many industrial applications. Dense nanostructured Ti was sintered from mechanically activated Ti and $TiH_2$ powders by high frequency induction heating under pressure of 80 MPa. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition of grain growth. $TiH_2$ powder was decomposed to Ti during sintering. The hardness of Ti increased and the average grain size of Ti decreased with increasing milling time. The average grain sizes of Ti samples sintered from Ti and $TiH_2$ powder milled for 5 hrs were about 26 nm, 44 nm, respectively. The hardness of Ti sintered from Ti and $TiH_2$ powder milled for 5 h was $504kg/mm^2$ and $567kg/mm^2$, respectively.

Superfine-Nanocomposite Mo - Cu Powders Obtained by Using Planetary Ball Milling

  • Lee, Han-Chan;Moon, Kyoung-Il;Shin, Paik-Kyun;Lee, Boong-Joo
    • Journal of the Korean Physical Society
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    • 제73권9호
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    • pp.1340-1345
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    • 2018
  • Mo-10 at.% Cu nanocomposite powders were fabricated by using planetary ball-milling (PBM), a mechanical alloying technique for preparing nanocomposite alloy powders of metals with mutual insolubility, and the variations in the physical and the chemical characteristics with the process conditions were investigated. We observed that Mo-10 at.% Cu was an appropriate composition to ensure a good alloying grade and minimal welding between particles. The influences of the temperature and the milling conditions on the mechanical alloying process and the phase change of Mo-10 at.% Cu composite powders were investigated, and the particle and the grain sizes of the powders after mechanical alloying were confirmed. The Mo-10 at.% Cu powders showed homogeneous elemental distributions and no phase changes up to $1200^{\circ}C$; their compositions were retained after the mechanical alloying process. The finest grain size obtained was about 5 nm for powders processed using optimum PBM processing conditions: ball-to-powder weight ratio of 5 : 1, ambient air atmosphere, a milling time of 20 h, a rotation speed of 200 rpm, and a stearic acid content of 4 wt.% produced superfine-grained Mo-10 at.% Cu nanocomposite powders with an average grain size of 5 nm (which is smaller than that of other similar materials reported in the literature). The analytical results confirmed that the PBM technique presented here is a promising method for preparing superfine-grained Mo-10 at.% Cu powders with improved properties.

Grain Growth Revealed by Multi-wavelength Analysis of Non-axisymmetric Substructures in the Protostellar Disk WL 17

  • Han, Ilseung;Kwon, Woojin;Aso, Yusuke
    • 천문학회보
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    • 제45권1호
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    • pp.59.2-59.2
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    • 2020
  • Disks around protostars are the birthplace of planets. The first step toward planet formation is grain growth from ㎛-sized grains to mm/cm-sized grains in a disk, particularly in dense regions. In order to study whether grains grow and segregate at the protostellar stage, we investigate the ALMA Band 3 (3.1 mm) and 7 (0.87 mm) dust continuum observations of the protostellar disk WL 17 in ρ Ophiuchus L1688 cloud. As reported in a previous study, the Band 3 image shows substructures: a narrow ring and a large central hole. On the other hand, the Band 7 image shows different substructures: a non-axisymmetric ring and an off-center hole. The two-band observations provide a mean spectral index of 2.3, which suggests the presence of mm/cm-sized large grains. Its non-axisymmetric distribution may imply dust segregation between small and large grains. We perform radiative transfer modeling to examine the size and spatial distributions of dust grains in the WL 17 disk. The best-fit model suggests that large grains (>1 cm) exist in the disk, settling down toward the midplane, whereas small grains (~10 ㎛) well mixed with gas are distributed off-center and non-axisymmetrically in a thick layer. The low spectral index and the modeling results suggest that grains rapidly grow at the protostellar stage and that grains differently distribute depending on sizes, resulting in substructures varying with observed wavelengths. To understand the differential grain distributions and substructures, we discuss the effects of the protoplanet(s) expected inside the large hole and the possibility of gravitational instability.

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공릉천 감조구간에 나타나는 표층퇴적물의 공간적 분포 특성 (Spatial distribution patterns of the surficial sediments in the tidal river, Gongneungcheon)

  • 최영선
    • 한국지형학회지
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    • 제18권4호
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    • pp.203-212
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    • 2011
  • 감조하천이 발달한 경기도 파주시 탄현면 일대의 공릉천 감조구간을 연구지역으로 하여 표층퇴적물의 공간적 분포 특성을 조사하였다. 연구 결과는 다음과 같다. 첫째, 공릉천 감조구간의 표층퇴적물은 주로 실트로 구성되어 있다. 둘째, 종단축의 경우 겨울과 여름 모두 감조구간의 하류보다 상류에서 평균입도가 세립해지는 경향이 나타났으며, 여름이 겨울보다 평균입도가 작고 분급이 양호한 것으로 나타났다. 감조구간 종단축의 입도 분포를 볼 때 부유물질이 퇴적되는 데에는 조류의 작용, 특히 밀물의 영향을 많이 받는 것으로 보이며 이러한 경향은 겨울에 더 우세한 것으로 판단된다. 셋째, 횡단축의 경우 하도로부터 거리가 멀어질수록 평균입도가 세립해지는 경향이 나타났다. 넷째, 갑문과 같은 인공 시설 역시 유속을 정체시킴으로써 입도 분포에 영향을 미친다고 판단된다.

서해 중부 태안반도 북부 해역의 장안사퇴 표층퇴적물 분포 특성 (Distribution Patterns of Surface Sediments of the Jangan Linear Sand Ridge off the Northern Taean Peninsula, in the Mid-west Coast of Korea)

  • 장태수;이은일;변도성;이화영;백승균
    • 한국해양학회지:바다
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    • 제29권1호
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    • pp.14-27
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    • 2024
  • 빈사 상태의 대륙붕 사퇴와는 달리, 연안 사퇴는 활동성이 높으며 주변 해양환경변화에 민감하게 반응하기 때문에 해저지형변화의 관점에서 관심의 대상이다. 대산항에서 불과 5 km 떨어진 장안사퇴는 지난 20여 년 동안 격심한 해저지형변화를 겪어오고 있다. 이러한 해저지형변화의 원인을 밝히기 위해서는 사퇴의 특성을 이해하는 것이 중요하다. 이러한 맥락에서 이 연구는 장안사퇴와 주변해역의 퇴적물 분포 양상을 이해하고자, 그랩식 채니기를 사용하여 총 227점의 퇴적물을 획득하고 체질-피펫방식의 입도분석을 수행하였다. 또한 1997년의 입도자료와 비교를 통해 지난 25년 동안의 퇴적물 입도 변화를 조사하였다. 장안사퇴의 중심부는 평균 입도 2-3∅의 중립사 내지는 세립사로 이루어졌으며, 사퇴의 골은 -2-6∅의 자갈과 니사질역으로 구성된다. 사퇴의 능선 퇴적물은 양호한 분급의 정규분포를 보인 반면에 사퇴의 기저 퇴적물은 불량한 분급과 주로 자갈퇴적물에 소량의 세립 퇴적물이 혼합된 양(+)의 왜도를 나타낸다. 사퇴의 중심부 퇴적물은 소량의 잔자갈의 혼합된 음(-)의 왜도를 보인다. 1997-2021년 동안 장안사퇴의 퇴적물은 전반적으로 0.5∅정도 조립해진 것으로 보이며, 겨울철 고파랑의 영향으로 세립질 퇴적물이 제거되었거나 해사채취 시 부유사의 제거로 설명할 수 있다. 표층퇴적물의 공간분포 양상을 미루어 볼 때 잔류 자갈 위에 30 m에 달하는 사퇴 본체가 놓인 것으로 추정된다. 사퇴 비대칭성, 기저면의 노출과 재동이 심한 잔류 자갈의 존재는 장안사퇴가 퇴적물 공급이 충분하지 않음을, 따라서 침식 상태에 놓여 있음을 시사한다.

바인더 볏단의 크기가 자동탈곡기(自動脱糓機)의 탈곡성능(脱糓性能) 및 부하특성(負荷特性)에 미치는 영향(影響) (Effects of Binder-Sheaf Size on Threshing Performance and Load Characteristics of an Auto Feed Thresher)

  • 유수남;류관희
    • Journal of Biosystems Engineering
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    • 제6권1호
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    • pp.60-72
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    • 1981
  • This study was carried out to find out the effects of the sheaf size of paddy harvested by the binders on the threshing performance, load characteristics and power requirement of an auto-feed thresher. The results of the study are summarized as follows: 1. The seperating performance of the thresher appeared to be satisfactory for all the sheaf sizes although the amount of rubbishes and empty grains slightly increased with the sheaf size of paddy. 2. There was no significant difference in grain output quality of the thresher among the three sheaf sizes. However, the amount of grains left unthreshed increased with the sheaf size. In the case of the largest sheaf size with the feed rate of 780kg/h, it exceeded the limit set by the national inspection regulations. 3. The position of the feed-chain rail gave a significant effect on the power requirement of the thresher. At the feed rate of 780kg/h, the net power required to convey sheafs through the feed chain was in the range of 0.37 to 0.50 PS for the middle and lowest position of feed-chain rail, and there was no significant difference among the sheaf sizes. At the highest position, however, it appeared that the smallest sheaf required more power than the others. The net power requirements at this position were 1.03, 0.59. 0.65 PS for the smallest, medium and largest sheafs respectively. 4. The torques of both the thresher and the engine shaft increased with the feed rate and were not affected by the sheaf size for the lower two feed rates of 520 and 780kg/h. At the highest feed rate of 1,040 kg/h, however, they were affected by the sheaf size. In this case, the medium sheaf size gave lower values than the others. 5. The variations in the thresher and the engine torque increased with the feed rate and were not affected by the sheaf size for the feed rate of 520kg/h. At the feed rate of 780kg/h, however, they increased with sheaf size. And at the feed rate of 1,040 kg/h, the torque variations increased greatly for all the sheaf sizes due to an over-load operating condition. 6. It appeared that the average and maximum power requirements of the thresher increased with the feed rate. But, there was no significant difference in power requirement among the sheaf sizes for the lower two feed rates. 7. The threshing efficiency of the thresher was in the range of 214-249 kg/ps.h with the feed rates of 520 and 780 kg/h, and it was not affected by both the sheaf size and the feed rate. At the feed rate of 1,040 kg/h, however, it decreased to as low as 171-174 kg/ps.h because of a sudden increase in power requirement. 8. The average power requirements of the engine were slightly higher than those of the thresher due to the slippage of flat belt between the thresher and engine. It appeared that power transmission from the engine to the thresher was maintained properly since slippages were moderately low with the range of 2.78 to 6.51% throughout the tests. 9. The specific fuel consumption of the engine (diesel 8PS) decreased as the feed rate increased. However, there was no significant reduction in specific fuel consumption as the feed rate increased above 780 kg/h.

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