• 한국재료학회지
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• 제2권4호
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• pp.306-310
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• 1992

Effects of hafnium, boron and zirconium on the ductility of Ni$_3$(Al, Fe) intermetallic compounds were studied using tensile test and SIMS analysis. Ni$_3$(Al, Fe) alloy with 0.1 at.% Hf, 0.05 at.% B and 0.1 at.% Zr additions showed maximum elongations of about 30% at 300K, 10% at 300K and 14% at 473K, respectively. The fracture mode of the alloy without the additive was the mixture of intergranular and transgranular fractures, but the addition of Hf, Zr or B changed the fracture mode to transgranular only. SIMS analysis showed that the beneficial effects of Hf, Zr or B segregation on the grain boundary strength are consistent with the grain boundary cohesion theory.

• Interaction and multiscale mechanics
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• 제4권3호
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• pp.207-217
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• 2011

International efforts have focused recently on the development of tungsten surfaces that can intercept energetic ionized and neutral atoms, and heat fluxes in the divertor region of magnetic fusion confinement devices. The combination of transient heating and local swelling due to implanted helium and hydrogen atoms has been experimentally shown to lead to severe surface and sub-surface damage. We present here a computational model to determine the relationship between the thermo-mechanical loading conditions, and the onset of damage and failure of tungsten surfaces. The model is based on thermo-elasticity, coupled with a grain boundary damage mode that includes contact cohesive elements for grain boundary sliding and fracture. This mechanics model is also coupled with a transient heat conduction model for temperature distributions following rapid thermal pulses. Results of the computational model are compared to experiments on tungsten bombarded with energetic helium and deuterium particle fluxes.

• 한국재료학회지
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• 제2권6호
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• pp.468-476
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• 1992

초기 결정입 크기 15${\mu}$m인 W-0.2wt%Ni, 1시간 30분과 W-0.4wt%Ni, 1시간 소결체의 응력 파단 성질 및 파괴 양상을 조사하기 위해서 direct load creep tester를 사용, 100$0^{\circ}C$~120$0^{\circ}C$, 수소분위기에서 응력 파단 시험을 행하였다. 100시간 응력 파단 강도는 W-0.4wt%Ni이 W-0.2wt% Ni보다 23% 크게 나타났다. 이것은 시험 중 결정입 성장에 따른 영향 때문으로 생각된다. W-0.2wt%NI에서 크리프 속도와 초기 결정입 크기와의 관계는 반비례하는 경향을 보였다. 활성 소결체에서 Ni 첨가량이 증가함에 따라, 단위 면적당 기공의 밀도 및 크기는 작아지고, 형태는 구형화 되어 미세균열로의 전이가 어려워 응력 파단 성질이 향상되었다. 응력 파란 시험 후, 각단면은 전형적인 입계파괴 양상을 나타내었다. 이는 소결 과정 중 생성된 기공들이 결정입계를 따라 전파하였기 때문으로 생각된다.

• 열처리공학회지
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• 제9권3호
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• pp.212-218
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• 1996

To clarify the influence of precipitation microstructure and inclusion on the monotonic tensile fracture behaviors in 2090 alloy aged at $180^{\circ}C$, the detailed measurement of hardness, tensile strength, elongation and the observation of scanning electron micrography, transmision electron micrography have been carried out. The transgranular shear ductile fracture has been observed in specimen quenched after solution treatment at $500^{\circ}C$ for 45min. While the under-aged specimen was fractured in both transgranular shear ductile and intergranular fracture mode, the fracture mode of peak-aged and over-aged alloy was predominantly intergranular fracture. The fracture behavior of each ageing condition was influenced by the change of precipitation microstructural features. In the case of peak-aged and over-aged alloys, the coarse and heterogeneous slip band caused by both shearable nature of the ${\delta}^{\prime}(Al_3Li)$ precipitates and PFZ along the high angle grain boundary aid the localization of deformation, resulting in low energy intergranular fracture. It was also estimated that the fractured T-type intermetallic phases (inclusion) and the equilibrium ${\delta}$(AlLi) phases which were formed at grain boundaries palyed an important role in promoting intergranular fracture mode.

• 소성∙가공
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• 제17권4호
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• pp.240-248
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• 2008

The effect of alloying elements(Mn, S, Mo, B) on the high temperature deformation behavior of Fe-29%Ni-17%Co (Kovar) alloy were investigated. And the effect of high temperature oxidation on the hot ductility was also studied. The hot ductility of Kovar alloy was drastically increased with the addition of Mn and lowering of S content. It has been found that the brittle intergranular fracture at high temperature cracking is closely associated with the FeS sulfide along the grain boundary. When Mn was added, the type of sulfide was changed to MnS from FeS and ductile intergranular fracture and transgranular fracture were promoted. The formation of oxide layer was found to have minimized the hot ductility of the Kovar alloy significantly. Grain boundary micro-cracks in the internal oxide region were noted following deformation due to high temperature, one of which acting as a notch that caused the poor hot workability of the oxidized specimen. The addition of Mo to the Kovar alloy could also retard the decrease in the hot ductility of the oxidized specimen through the prevention of notching due to internal oxidation. Hot ductility was remarkably improved by the addition of Boron. The improvement of hot ductility results from the grain boundary migration mainly due to the dynamic recrystallization at lower temperature range ($900{\sim}1000^{\circ}C$).

• 터널과지하공간
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• 제31권6호
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• pp.593-609
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• 2021

본 연구에서는 입자기반 개별요소모델(grain-based distinct element model, GBDEM)을 이용하여 결정질 암석 내 포함된 균열의 열-역학적 거동을 평가할 수 있는 수치해석기법을 제시하고 열에 의한 균열의 미끄러짐 거동을 해석하였다. 이는 DECOVALEX-2023 프로젝트 Task G의 일환으로 수행된 벤치마크 모델링 연구로, Task G는 결정질 암반 내 균열의 열-수리-역학적 복합거동을 해석하기 위한 수치해석기법을 개발하는 데에 목표가 있다. 여기에서는 Voronoi diagram을 이용하여 다면체 개별입자의 집합체로서 해석모델을 생성하고, 입자 및 입자간 접촉에서 발생하는 열-역학적 거동을 개별요소프로그램인 3DEC을 통해 해석하였다. 암석 시험편의 탄성거동을 재현하기 위하여 등가연속체 개념을 적용하여 입자와 접촉의 미시물성을 산정하였으며, 균열에 상응하는 접촉에는 Coulomb slip model을 부여하여 인장강도와 전단강도를 갖는 불연속면을 모사하였다. 경계응력과 열응력에 의한 균열의 거동을 수치적으로 모델링하였으며, 경계조건에 따라 균열의 미끄러짐이 발생하는 열-역학적 메커니즘을 정량적으로 분석하였다. 해석 결과, 본 연구에서 제시한 해석모델이 암석 내 열팽창과 열응력의 증가, 균열 응력과 변위, 경계조건의 영향 등을 합리적으로 재현하고 있음을 확인하였다. 본 연구의 해석모델은 Task G에 참여하는 국외 연구팀들과의 의견 교류와 워크숍을 통해 지속적으로 개선하는 한편, 향후 실내실험에 적용하여 타당성을 검증할 예정이다.

• 대한금속재료학회지
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• 제50권1호
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• pp.52-58
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• 2012

Hydrogen-delayed fracture (HDF) was analyzed from the deposited weld metals of 600-MPa and 800-MPa flux-cored arc (FCA) welding wires, and then from the diffusible hydrogen behavior of the weld zone. Two types of deposited weld metal, that is, rutile weld metal and alkali weld metal, were used for each strength level. Constant loading test (CLT) and thermal desorption spectrometry (TDS) analysis were conducted on the hydrogen pre-charged specimens electrochemically for 72 h. The effects of microstructures such as acicular ferrite, grain-boundary ferrite, and low-temperature-transformation phase on the time-to-failure and amount of diffusible hydrogen were analyzed. The fracture time for hydrogen-purged specimens in the constant loading tests decreased as the grain size of acicular ferrite decreased. The major trapping site for diffusible hydrogen was the grain boundary, as determined by calculating the activation energies for hydrogen detrapping. As the strength was increased and alkali weld metal was used, the resistance to HDF decreased.

• 마이크로전자및패키징학회지
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• 제8권4호
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• pp.25-33
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• 2001

Bi(0, 2.5, 4.8, 7.5, 10 wt%)가 첨가된 Sn-3.5Ag-xBi 합금을 주조 및 압연을 거쳐 준비하였다. 그 후, dog-bone형상의 시편의 안정한 미세 조직을 위해 열처리를 거친 후, 일정하중에 크리프 실험을 수행하였다. 2.5%Bi 첨가 합금의 경우, 크리프 저항성이 가장 우수하였으며, Bi가 더 첨가됨에 따라 크리프 저항성은 감소하였다. 합금의 응력 지수는 전형전인 전위 크리프에 의한 4를 나타내었으며, 10%Bi 시편의 경우, 입계 미끄러짐에 의한 2를 나타내었다. 0%Bi 합금의 경우, 연성 파괴 양상을 보인 반면, Bi 첨가 합금의 경우, 약간의 단면적 감소를 보이는 취성 파괴 양상을 보여주었다. 파단 시편의 미세 조직 관찰 결과, 응력축에 수직한 방향으로 기공이 관찰되었으며, 상당량의 입계 미끄러짐이 관찰되었다.

• International Journal of Safety
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• 제8권1호
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• pp.6-9
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• 2009

The crack in a J85 engine V.G. actuator arm shaft for a bell crank on the engine compressor was investigated. The crack was observed in twenty two shafts during the inspection of 238 shafts. The failure analysis of shaft cracks was performed by chemical composition analysis using ICP(Inductively Coupled Plasma) and by fracture surface and microstructure analysis using FE-SEM and optical microscope. The crack initiated from the top and bottom and propagated to the center along the grain boundaries. From the chemical composition analysis, the fractography of the fracture surface and the microstructure, it was found that the failure mechanism of the shafts is the inclusion-related intergranular decohesion crack. The inclusion was found out from MnS particle by EDS(Energy Dispersive Spectroscopy). The crack initiated MnS inclusion in the grain boundary and propagated with the increase of applied shear stress during long operation. In order to prevent the fracture, NDI(Nondestructive inspection) is needed periodically as recommended.

• The Korean Journal of Ceramics
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• 제1권4호
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• pp.197-203
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• 1995

Nearly fully dense PZT samples both with tetragonal and with morphotropic phase boundary compositions were prepared by the conventional powder processing and sintering. A micro-indentation technique was used to evaluate the dependence of fracture toughness on remanent polarization, crack length and the direction of crack propagation. The result shows that the toughness increases with the remanent polarization along the poling direction and decreases in the transverse direction. The dependence of toughness on the remanent polarization is neither symmetric nor linear but rather shown to be saturated quickly with the increase in remanent polariztion. R-curve behaviors are observed in both poled and unpoled samples. Sequential SEM and XRD studies on annealed, poled, ground, fractured and etched samples show that domain switching is evident as a viable toughening mechanism but might depend upon the rate of crack propagation. Grain bridging is also observed as one of the active toughening mechanisms.