• Journal of the Korean Ceramic Society
• /
• v.54 no.6
• /
• pp.506-510
• /
• 2017

One of the characteristics of polycrystalline graphene that determines its material properties is grain size. Mechanical properties such as Young's modulus, yield strain and tensile strength depend on the grain size and show a reverse Hall-Petch effect at small grain size limit for some properties under certain conditions. While there is agreement on the grain size effect for Young's modulus and yield strain, certain MD simulations have led to disagreement for tensile strength. Song et al. showed a decreasing behavior for tensile strength, that is, a pseudo Hall-Petch effect for the small grain size domain up to 5 nm. On the other hand, Sha et al. showed an increasing behavior, a reverse Hall-Petch effect, for grain size domain up to 10 nm. Mortazavi et al. also showed results similar to those of Sha et al. We suspect that the main difference of these two inconsistent results is due to the different modeling. The modeling of polycrystalline graphene with regular size and (hexagonal) shape shows the pseudo Hall-Petch effect, while the modeling with random size and shape shows the reverse Hall-Petch effect. Therefore, this study is conducted to confirm that different modeling is the main reason for the different behavior of tensile strength of the polycrystalline structures. We conducted MD simulations with models derived from the Voronoi tessellation for two types of grain size distributions. One type is grains of relatively similar sizes; the other is grains of random sizes. We found that the pseudo Hall-Petch effect and the reverse Hall-Petch effect of tensile strength were consistently shown for the two different models. We suspect that this result comes from the different crack paths, which are related to the grain patterns in the models.

• Korean journal of food and cookery science
• /
• v.23 no.3 s.99
• /
• pp.314-320
• /
• 2007

The objective of this study was to investigate the effect of grain size on the physicochemical properties of rice porridge. Here, the grain size of the rice was classified as whole grain, half grain, and flour by traditional Korean cooking methods. The viscosity of the rice flour porridge was highest for the among the three different grain size porridges. In the amylographs, the increase in viscosity for the whole grain porridge was higher than that of the rice flour porridge during cooling. The soluble solid and reducing sugar contents of the rice porridges increased according to the rice grain size, while the blue value decreased. The SDI (starch digestion index) increased according to the rice grain size. The RDS (rapidly digestible starch) was highest while the SDS (slowly digestible starch) the lowest in the rice flour porridge. The morphologies of the rice porridges were examined by SEM and showed a smoother surface and more exudated gelatinized granules in the rice flour than in the whole grain rice porridge. In conclusion, rice porridges made from the smallest possible grain size such as flour may be helpful for people with weaker digestive systems such as infants, the elderly, and hospital patients.

• Journal of Powder Materials
• /
• v.13 no.5 s.58
• /
• pp.360-365
• /
• 2006

The phase stability of tetragonal phase in Y-TZP was investigated in terms of the distribution of grain sizes and heat-treating atmosphere. Y-TZP with various grain sizes were prepared using duration time at $1600^{\circ}C$ as experimental parameter. Accumulated grain size distributions were built from the SEM micrographs and the amount of tetragonal phase were measured using XRD. Both results were compared to determine the critical grain size before and after heat-treatment in vacuum. The critical grain size drastically decreased compared with the small increase of average grain size due to the autocatalytic effect which critically affects the tetragonal to monoclinic phase transformation. After heat-treatment in reductive atmosphere critical grain size relatively increased due to the stabilization of tetragonal phase. The formation of oxygen vacancies during heat-treatment was ascribed to the increase of stability.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2006.06a
• /
• pp.46-46
• /
• 2006

$SrTiO_3$ was annealed at two different annealing times (1 h and 16 h) to investigate the annealing effect on the grain size and orientation distribution. Electron backscattered diffraction (EBSD) was used to analyze the grain size and grain orientation distributions of the $SrTiO_3$. It is possible to understand the annealing effect on the microstructure evolution, by comparing the grain size and orientation distribution of the $SrTiO_3$ as a function of annealing time.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.14 no.10
• /
• pp.815-820
• /
• 2001

The piezoelectric properties of the PT-PZ-PNN system ceramics were investigated depending on the variati on of the grain size. The grain size was varied by sintering temperature, and additive. The effect of the grain size on the electrical, dielectric, and piezoelectric properties was studied with respect to the feasibility of the application for the piezoelectric transformer. Grain size increased as the PMW contents increased. The smaller the particle size used, the smaller the grain size obtained. Specimens are densily sintered. Dielectric and piezoelectric properties are not always improved in proportion to the grain sizes. When he particle size are fine and the grain size are increased properly with the optimum additives, the piezoelectric preperties have good values. the specimen sintered at 1200$\^{C}$ with PMW 2 mol% and MnO$\_$2/ 0.5wt% contents exhibited good piezoelectric properties for a piezoelectric transformer.

• 한국기계연구소 소보
• /
• s.20
• /
• pp.71-78
• /
• 1990

This investigation was undertaken to establish the technologies of grain refinement and modification, and to characterize material properties, essential for high quality aluminum alloy castings. Grain refinement seldom changed DAS and eutectic Si size, but largely decrease grain size. The variations of grain size induced by grain refinement had a great influence on the elongation without changes in the tensile strength or yield strength. The optimum Ti level lies between 0.1% and 0.16% to achieve the best possible mechanical properties. DAS and grain size were little affected, but eutectic Si size was greatly refined by modification. The variation of eutectic Si size had a great effect on the elongation, impact value, fracture toughness and fatigue crack propagation rate without changes in the tensile strength or yield strength. The Sr content of 0.015% is optimum to modification.

• Korean Journal of Materials Research
• /
• v.32 no.10
• /
• pp.414-418
• /
• 2022

Magnesium alloy is the lightest practical metal. It has excellent specific strength and recyclability as well as abundant reserves, and is expected to be a next-generation structural metal material following aluminum alloy. This paper investigated the possibility of thin plate fabrication by applying a overheating treatment to the melt drag method, and investigating the surface shape of the thin plate, grain size, grain size distribution, and Vickers hardness. When the overheating treatment was applied to magnesium alloy, the grains were refined, so it is expected that further refinement of grains can be realized if the overheating treatment is applied to the melt drag method. By applying overheating treatment, it was possible to fabricate a thin plate of magnesium alloy using the melt drag method, and a microstructure with a minimum grain size of around 12 ㎛ was obtained. As the overheating treatment temperature increased, void defects increased on the roll surface of the thin plate, and holding time had no effect on the surface shape of the thin plate. The fabricated thin plate showed uniform grain size distribution. When the holding times were 0 and 30 min, the grain size was refined, and the effect of the holding time became smaller as the overheating treatment temperature increased. As the overheating temperature becomes higher, the grain size becomes finer, and the finer the grain size is, the higher the Vickers hardness.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2008.10a
• /
• pp.398-400
• /
• 2008

In this work, an air-bending test using magnesium alloy ZK60 sheet was carried out at the various temperatures from room temperature to $300^{\circ}C$ in order to investigate the effect of grain size on the spring-back characteristic. It was found out from experiments that the amount of spring-back was nearly zero at all temperature range when the specimens with grain sizes of 14.66 and $60.71{\mu}m$ were bent by $90^{\circ}$. On the other hand, the spring-back amount dramatically increased at room temperature and phenomenon of spring-go was observed at high temperature when the specimen with submicro grain size of $0.98{\mu}m$ was bent by $90^{\circ}$. From this kind of different spring-back characteristics according to the grain size, it was confirmed that the grain size of material is one of the important factors which have an effect on the spring-back.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.11 no.6
• /
• pp.867-876
• /
• 1987

Corrosion fatigue fracture with change in the grain size of M.E.F. dual phase steel is investigated in 3.5% NaCI aqueous solution at pH 2, 4, 6, 9, and 11. Generally speaking, decrease in corrosion fatigue life is strongly dependent on decrease in pH and slightly on the grain size. For the B material with the big grain size, the fatigue life is small due to its large reduction ratio of corrosion fatigue life. The influence of grain size on the reduction ratio of corrosion fatigue life is large at pH 11-6. Whi9le at pH 4-2 the reduction ratio of corrosion fatigue life only depends on the corrosion effect. The larger grain size and the lass pH result in the greater influence on corrosion fatigue crack propagation rate. As pH decreases, the plateau portion in the crack propagation rate curves of the B material are distinct. Crack propagation rate curves become slow down at high .DELTA.K range because crack closure effect by minute corrosion products inside crack causes the oxidation corrosion action less effective for a certain period of time. In A material with small grain size, fatigue life is increased in proportion with increase of martensite intergranular which brings forth restraining the crack propagation decreases crack propagation rate. Corrosion pit which is created in the surface of specimen is found at pH 6,4 and 2 which is noticeable and the unevenness of the surface of the specimen becomes severe as pH decreases. The unevenness of corrosion fatigue fracture surface is severe as the effect of pH increases i.e. as pH decreases. In proportion with increase in the grain size and decrease in pH, the aspect of brittle fracture becomes evident.

• 한국초전도학회:학술대회논문집
• /
• v.10
• /
• pp.285-288
• /
• 2000

The effect of the initial BSCCO 2212 grain size on the final gain size and the formation of the BSCCO 2223 was studied using a powder precursor synthesized by two-powder method. 2212 and CaCuO$_2$ tapes were prepared by dip coating and joined by pressing and then followed by the repeated thermo mechanical treatment. The samples were characterized by XRD and SEM analysis. The formation and grain size of the BSCCO 2223 depended on the initial BSCCO 2212 grain size.