• Title/Summary/Keyword: Grain Size Analysis

Search Result 776, Processing Time 0.024 seconds

Fabrication and mdchanical properties of $AC4A/SiC_p$ composites by mechanical alloying (기계적합금화에 의한 $AC4A/SiC_p$복합재료의 제조 및 기계적 특성)

  • Lee, Byung-Hun;Cho, Hyung-Jun;Lim, Young-Ho;Lee, Jun-Hee
    • Korean Journal of Materials Research
    • /
    • v.4 no.6
    • /
    • pp.651-661
    • /
    • 1994
  • Utilizing Mechanical Alloy Process, that were obt,ained the results from investigated formation process of AC4A/$SiC_p$. composite material powders and mechanical properties of their extrusion materials. The obtained results are as follow conclusions. AC4A-lOwt.% $SiC_p$ powders which were mechanically alloyed at 150rpm for 420min have been obtained finely and uniformly rounded powder particals that were reached the steady state which was saturated micro hardness about tlv 230 in the range size of 1 0 ~ 2 0$\mu \textrm{m}$. EDAX analysis tests have been resulted in a little amount of I'e conrents increasing with MA times, the artifical aging of AC4A/S$SiC_p$ composite materials was obtained the hardness with solution treated at $525^{\circ}C$ for lOhrs the maximum value of Hv 230 with aging at. $170^{\circ}C$ for 1000min. The Intensity and width of X-ray diffraction pattern were decreasing and widening because of grain boundary refinement and heterogeneous strain during mechanical alloying. Tensile tests at room temperature were carried out the maximum value of 37 Kgf/$\mu \textrm{mm}^2$ with ext,rused materials, 27 Kgf/$\mu \textrm{mm}^2$ with heat treated them at $500^{\circ}C$.

  • PDF

Characteristics of Core Sedimentary Facies at the Ulleung Basin in the East Sea of Korea (한국 동해 울릉분지 코어 퇴적상 특성)

  • Lee, Byoung-Kwan;Lee, Su-Woong;Kim, Hong-Tae;Kim, Seok-Yun
    • Journal of Environmental Science International
    • /
    • v.20 no.7
    • /
    • pp.829-837
    • /
    • 2011
  • A study on the grain size change, sedimentary facies and age indicator of volcanic tephra was analysis through four cores (P1 ~ P4) at the Ulleung Basin in the East Sea of Korea. The two cores (P1 and P2) were collected in the northeastern side of the Ulleung Basin (about 2,000 m in water depth), while the other two cores (P3 and P4) with the water depth of about 1,500 m and 1,700 m, respectively, were collected from the continental slope of the southwestern and western side of the Ulleung Basin. Four sedimentary facies and eight sedimentary subfacies were identified. The four facies were massive sand, bioturbated mud, homogeneous mud, and laminated mud. The eight subfacies were further divided as pumiceous ash massive sand, scorieaous massive sand, plain bioturbated mud, pyrite filamented bioturbated mud, distinctly laminated mud, indistinctly laminated mud, thinly laminated mud and homogeneous mud. The homogeneous mud was not found in the core of P3 which is located in the western side of Ulleung Basin (close to the Korean coast). In the case of laminated mud facies, the thinly laminated mud facies was dominated in the lower part of core sequences of the Ulleung Basin (P1 and P2), while the indistinctly laminated mud were overally distributed in the core sequences from the continental slope of Ulleung Basin. The Tephra layers from the core sequences of central Ulleung Basin were more dominated and distinctive than those from the core sequences of continental slope. This is related to the distance from the volcanic source and the amount of sediment supply. The core locations of Ulleung-Oki Tephra layers in the central Ulleung Basin were in the upper part of core sequences, while those in the continental slope were in the lower part of core sequences. This is indicated that the amounts of sediment supply in the continental slope after the Ulleung-Oki eruption were very high and different sedimentary environment between upper and lower of Tephra layer.

The Distribution and Habitation Characteristics of Zostera marina L. along the Southern Coast of Korea (남해안에서 자생하는 거머리말(Zostera marina L.)식물의 분포와 생육지 환경)

  • Lee, Sang-Yong;Lee, Sung-Mi;Jee, Hae-Geun;Choi, Chung-Il
    • Korean Journal of Environmental Biology
    • /
    • v.19 no.4
    • /
    • pp.313-320
    • /
    • 2001
  • An ecological study was conducted to determine the geographic distribution, community structure, and habitat characteristics of eelgrass, Zostera marina L. beds along the southern coast of Korea. Plants and sediment samples were collected during June 2000 and December 2000 on twenty-eight locations, including two Cheju Island stations, which were used to compare morphological characteristics with habitat types. Z. marina populations existed from the intertidal to subtidal zone, mainly in the bays along the coast and the island, the barrier reef, and the estuary where the water depth was 0.5${\sim}$8.0m. Salinity range in Z. marina beds ranged 18.2 to 34.5%$_o$. Sediments of Z. marina beds contained 49.7${\sim}$99.1% of sand and were classified into sand, muddy sand, and sandy mud. Mean grain size varied from 1.5 to 4.4 phi. Height of vegetation shoots varied from 54.7 to 171.4 cm, depending on water depth, location, substrata and habitat types. quantitative morphological features that enabled recognition of the two phonetic groups were short-narrow leaf type and long-broad leaf type. Statistical analysis indicated that biomass of individual plants and their quantitative morphological characteristics were significantly correlated.

  • PDF

Electrical Properties in $Pt/SrTiO_3/Pb_x(Zr_{0.52}, Ti_{0.48})O_3/SrTiO_3/Si$ Structure and the Role of $SrTiO_3$ Film as a Buffer Layer ($Pt/SrTiO_3/Pb_x(Zr_{0.52}, Ti_{0.48})O_3/SrTiO_3/Si$ 구조의 전기적 특성 분석 및 $SrTiO_3$박막의 완충층 역할에 관한 연구)

  • 김형찬;신동석;최인훈
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.11 no.6
    • /
    • pp.436-441
    • /
    • 1998
  • $Pt/SrTiO_3/Pb_x(Zr_{0.52}, Ti_{0.48})O_3/SrTiO_3/Si$ structure was prepared by rf-magnetron sputtering method for use in nondestructive read out ferroelectric RAM(NDRO-FEAM). PBx(Zr_{0.52}Ti_{0.48})O_3}$(PZT) and $SrTiO_3$(STO) films were deposited respectively at the temperatures of $300^{\circ}C and 500^{\circ}C$on p-Si(100) substrate. The role of the STO film as a buffer layer between the PZT film and the Si substrate was studied using X-ray diffraction (XRD), Auger electron spectroscopy (ASE), and scanning electron microscope(SEM). Structural analysis on the interfaces was carried out using a cross sectional transmission electron microscope(TEM). For PZT/Si structure, mostly Pb deficient pyrochlore phase was formed due to the serious diffusion of Pb into the Si substrate. On the other hand, for STO/PZT/STO/Si structure, the PZT film had perovskite phase and larger grain size with a little Pb interdiffusion. the interfaces of the PZT and the STO film, of the STO film and the interface layer and $SiO_2$, and of the $SiO_2$ and the Si substate had a good flatness. Across sectional TEM image showed the existence of an amorphous layer and $SiO_2$ with 7nm thickness between the STO film and the Si substrate. The electrical properties of MIFIS structure was characterized by C-V and I-V measurements. By 1MHz C-V characteristics Pt/STO(25nm)/PZT(160nm)/STO(25nm)/Si structure, memory window was about 1.2 V for and applied voltage of 5 V. Memory window increased by increasing the applied voltage and maximum voltage of memory window was 2 V for V applied. Memory window decreased by decreasing PZT film thickness to 110nm. Typical leakage current was abour $10{-8}$ A/cm for an applied voltage of 5 V.

  • PDF

Effect of Annealing in a Nitrogen Atmosphere on the Properties of In2O3 Films Deposited with RF Magnetron Sputtering (RF 마그네트론 스퍼터로 증착된 In2O3 박막의 질소분위기 열처리에 따른 특성변화)

  • Kong, Young-Min;Lee, Young-Jin;Heo, Sung-Bo;Lee, Hak-Min;Seo, Min-Su;Kim, Yu-Sung;Kim, Dae-Il
    • Korean Journal of Materials Research
    • /
    • v.22 no.1
    • /
    • pp.24-28
    • /
    • 2012
  • $In_2O_3$ films were deposited by RF magnetron sputtering on a glass substrate and then the effect of post deposition annealing in nitrogen atmosphere on the structural, optical and electrical properties of the films was investigated. After deposition, the annealing process was conducted for 30 minutes at 200 and $400^{\circ}C$. XRD pattern analysis showed that the as deposited films were amorphous. When the annealing temperature reached 200-$400^{\circ}C$, the intensities of the $In_2O_3$ (222) major peak increased and the full width at half maximum (FWHM) of the $In_2O_3$ (222) peak decreased due to the crystallization. The films annealed at $400^{\circ}C$ showed a grain size of 28 nm, which was larger than that of the as deposited amorphous films. The optical transmittance in the visible wavelength region also increased, while the electrical sheet resistance decreased. In this study, the films annealed at $400^{\circ}C$ showed the highest optical transmittance of 76% and also showed the lowest sheet resistance of $89{\Omega}/\Box$. The figure of merit reached a maximum of $7.2{\times}10^{-4}{\Omega}^{-1}$ for the films annealed at $400^{\circ}C$. The effect of the annealing on the work-function of $In_2O_3$ films was considered. The work-function obtained from annealed films at $400^{\circ}C$ was 7.0eV. Thus, the annealed $In_2O_3$ films are an alternative to ITO films for use as transparent anodes in OLEDs.

Structural characteristics of the Yecheon Shear Zone in the Pukhumyeon-Pyeongeunmyeon area, Gyeongsangbukdo, Korea (경상북도 북후면-평은면 지역에 발달된 예천전단대의 구조적 특성)

The Study of Low Carbon Microalloyed Forging Steels by Direct Quenching Method with Mo Additions (몰리브덴을 첨가한 직접 소입 저탄소 비조질강에 관한 연구)

  • Wee, Kyoum-Bok;Lee, Kyung-Sub
    • Korean Journal of Materials Research
    • /
    • v.2 no.6
    • /
    • pp.452-460
    • /
    • 1992
  • Effects of the microalloyed elements, temperatures and cooling rates on the strength and toughness of the medium carbon microalloyed hot forging steels obtained by air cooling(A.C.) method and the low carbon microalloyed forging steels by direct quenching(D.Q.) method were investigated. Combined additions of V+Nb produced the optimum combination of strength and toughness with ferrite-pearlite structure of the medium carbon steel by the A.C. method. 831MPa in UTS and 52.1J in toughness were obtained for 0.40c+0.12V+0.07Nb. It was martensite structure for the low carbon steel by the D.Q. method. The highest UTS and toughness obtained by Mo additions were 855MPa and 108j by 0.12C+0.10V+0.03Nb+1.13Mo respectively. Especially, the toughness of the low carbon steel was twice better than that of the medium carbon steel. 110$0^{\circ}C$was more appropriate than 120$0^{\circ}C$ for the reheating and forging temperature and 1.$2^{\circ}C$ /s was the best cooling rate from the viewpoint of the strength and toughness. Multiple regression analysis was used to quantify the influence of the microalloyed elements, temperatures and cooling rates on the strength, toughness, austenite grain size, and the pearlite interlamellar spacing.

  • PDF

Electrochemical Study of Nanoparticle Li4Ti5O12 as Negative Electrode Material for Lithium Secondary Battery (리튬이차전지 음극재용 나노입자 Li4Ti5O12의 전기화학적 연구)

  • Oh Mi-Hyun;Kim Han-Joo;Kim Young-Jae;Son Won-Keun;Lim Kee-Joe;Park Soo-Gil
    • Journal of the Korean Electrochemical Society
    • /
    • v.9 no.1
    • /
    • pp.1-5
    • /
    • 2006
  • Lithium titanium oxide $(Li_4Ti_5O_{12})$ with spinel-framework structures as anode material for lithium-ion battery was prepared by sol-gel and high energy ball milling (HEBH) method. According to the X-ray diffraction (XRD), Particle Size Analyses(PSA) and scanning electron microscopy (SEM) analysis, uniformly distributed $Li_4Ti_5O_{12}$ particles with grain sizes of 100 nm were observed. Half cells, consisting of $Li_4Ti_5O_{12}$ as working electrode and lithium foil as both counter and reference electrodes showed the high performance of high rate discharge capacity and 173 mAh/g at 0.2C in the range of $1.0\sim2.5 V$. Furthermore, the crystalline structure of $Li_4Ti_5O_{12}$ didn't transform during the lithium intercalation and deintercalation process.

The effects of the microstructure of the feed rod of $SrTiO_{3}$ on the melting stability ($SrTiO_{3}$ 원료봉의 미세구조가 용융대 안정에 미치는 영향)

  • Cho, Hyun;Shim, Kwang-Bo;Auh, Keun-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.6 no.2
    • /
    • pp.247-253
    • /
    • 1996
  • Microscopic analysis has been performed in order to investigate effects of the microstructure of the starting feed rods on the morphology of the S-L interface and the stability of the molten zone during single crystal growth of $SrTiO_{3}$ using a floating zone method. Undoped and $Fe_{2}O_{3}$ doped $SrTiO_{3}$ doped $SrTiO_{3}$ specimens, sintered at the different temperatures have been used. In the case of the feed rods sintered at the lower temperature($1400^{\circ}C$), the poor densification made the stability of the molten zone difficult to maintain. The feed rods sintered at the higher temperature ($1600^{\circ}C$) exhibited the higher density but their molten zone was difficult to maintain due to the presence of the abnormally grown grains. It is concluded that the uniform grain size distribution of the feed rod is the critical factor to maintain the stable molten zone and therefore to give optimum growth condition during FZ single crystal growth.

  • PDF

Distribution patterns of macrobenthos in the sandy shore of Hakampo, Korea (학암포 사질조간대 대형저서동물의 분포양상)

  • Nam, Ki-Ung;Ma, Chae-Woo;Son, Dae-Sun;Kim, Jong-Chun
    • Korean Journal of Environment and Ecology
    • /
    • v.29 no.5
    • /
    • pp.729-735
    • /
    • 2015
  • This study was carried out to analyze the community structure and distribution of macrobenthos in Hakampo sandy shore. As for the environmental factors of sampling stations, the average grain size of the sediments from the sampling stations was $2.37{\phi}$ with the range of $1.90{\phi}{\sim}2.52{\phi}$, which represents the typical medium sand sedimentary facies of sandy beach. The average sediment organic content was 1.15% with the range of 0.90%~1.46%. Most stations had low sediment organic content which is typical of sandy beach. The number of species were total 59 from 6 taxa and the individuals was $668inds./m^2$ in the 10 stations of the study area. Based on the Bray-Curtis similarity analysis, the 10 stations of the study area were broadly divided into 3 groups. The highest part of intertidal zone was St. 2~St. 4, the middle part of intertidal zone was St. 5~St. 8, and the lower part of intertidal zone was St. 9~St. 10. A spatial community structure was observed which is divided into the highest, middle, and lower parts.