• Title/Summary/Keyword: Grain Boundary Crack

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Electron Beam Weld ability of Alloy 718 Nozzle for Jet Propulsion Component (고속 추진체용 Alloy 718 노즐 단조품의 전자빔 용접성 평가)

  • Lee, C.H.;Kim, J.H.;Hong, J.K.;Yeom, J.T.;Yoon, J.W.;Park, N.K.
    • Transactions of Materials Processing
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    • v.17 no.7
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    • pp.523-527
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    • 2008
  • In this study, mechanical properties of Alloy 718 welded after forgings for jet propulsion component was investigated. Hot-forged and machined work-pieces($230mm\times70mm\times15mm$) which have different grain sizes are welded by electron beam welding technique. After welding, the components were solution heat-treated and aged. Samples were sectioned to analyze the microstructural evolution and formation of micro-crack. It was found that HAZ grain boundary liquation crack generally initiates in the coarse grains rather than the fine grains. Needle-like phases with high Nb contents were found at the outer part near the base metal. Vickers hardness and tensile tests were carried out at room temperature and at $649^{\circ}C$. The tensile properties of electron beam welding specimens exhibited around 100MPa and 10% decrease in strength and elongation, respectively.

Effect of a Matrix Structure on the Initiation of Fatigue Crack and Fatigue Strength in Nodular Graphite Cast Iron (구상흑연 주철재의 피로크랙 발생 및 피로강도에 미치는 기지조직의 영향)

  • Yoon, Myung-Jin;Lee, Kyoung-Mo
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.7 no.5
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    • pp.66-71
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    • 1998
  • It is required the superior materials for the parts of machines or structures, which could be endurable in severe load and environment. According to advancement of casting technology, nodular graphite cast iron is used as suitable for such condition. But nodular graphite cast iron is scattering of fatigue strength and low reliability. Therefore in this study, the effect of matrix structure and number of nodular graphite on the initiation of fatigue crack and fatigue strength. It was found that the material which has relatively high ferrite volume fraction was more easily cracked than other materials and fatigue limit was low. The material which has not found pinhole on the surface, the crack was initiated in graphite went through ferrite and propagated into through graphite, but separated graphite and ferrite grain boundary and combined with other cracks to fro large one.

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A Study on Fatigue strength by hardenability of Boron Addition Steel (보론 첨가강의 경화기구에 따른 기계적 성질에 관한 연구)

  • Lee, Jong-Hyung;Yoo, Duck-Sang;Park, Shin-Kyu
    • Journal of the Korean Society of Industry Convergence
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    • v.6 no.4
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    • pp.299-305
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    • 2003
  • This research is for the relationship with heat treatment cooling temprature and the characteristic of Mechanical properties of Boron-Addition-Steel, the main material and SM25C steel, the sub material, structure viewing fractography, hardness test, tensite test and are carried out after the manufacturing small-specimen treated with heat of $750^{\circ}C$, $850^{\circ}C$, $1050^{\circ}C$. The influence to the Mechanical properties accompanied by AISI51B20, Boron-Addition-steel shows the following result. 1. The influenc of heat treatment by the content of cabon-steel is dominant. Addition of boron result is Strengthening structure effectively by segregation and improving over all mechanical characters such as good. it results from the increase of temacity by the stability of inter granular with improvement of harden-ability. 2. Boron-Addition-Steel exist in the from of martensite structure accompanied by the ferrite precipitition centering around grain boundary, and is improved to Hv 200. 3. The height of harden-ability and fatigue stress the influence of heat results from crystal structure of martensite by difference of strength level in the structure of ferrite and doesn't have am effect on sensibility of temperature, and turns out to defend on production and growth of Matrix-structure-factor.

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Effect of Cd addition on the Fatigue Properties of Al-Cu-Mn cast alloy (Al-Cu-Mn 주조합금의 피로성질에 미치는 Cd 첨가의 영향)

  • Kim, Gyeong-Hyeon;Lee, Byeong-Hun;Kim, In-Bae
    • Korean Journal of Materials Research
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    • v.11 no.4
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    • pp.300-304
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    • 2001
  • Effect of Cd addition on the fatigue properties of Al-Cu-Mn cast alloy was investigated by low and high cycle fatigue tests. With increasing Cd content, fatigue life and tensile strength were increased. It was found that the fatigue strength was 115MPa and the fatigue ratio was 0.31. Metallographic observation revealed that the fatigue crack initiated at the surface and propagated along the grain boundary. This propagation path was attributed to the presence of PFZ along the grain boundary. The tensile strength increased from 330MPa in the Cd-free Al-Cu- Mn cast alloy to 401MPa in the 0.15%Cd-containing alloy.

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Effect of Sn Addition on the Fatigue Properties of Al-Cu-Mn Cast Alloy (Al-Cu-Mu 주조합금의 피로성질에 미치는 Sn 첨가의 영향)

  • Kim, Kyung-Hyun;Kim, Jeung-Dae;Kim, In-Bae
    • Korean Journal of Materials Research
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    • v.12 no.4
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    • pp.248-253
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    • 2002
  • Effect of Sn addition on the fatigue properties of Al-Cu-Mn cast alloy was investigated by low and high cycle fatigue tests. Fatigue life showed the maximum value of 5450cycles in the Al-Cu-Mn alloy containing 0.10%Sn, but decreased rapidly beyond 0.20% of Sn additions. It was found that the fatigue strength was 132MPa and fatigue ratio was 0.31 in the alloy containing 0.10%Sn. Metallographic observation revealed that the fatigue crack initiated at the surface and propagated along the grain boundary. This propagation path was attributed to the presence of PFZ along the grain boundary. The tensile strength increased from 330MPa in 7he Sn-free Al-Cu-Mn cast alloy to 429MPa in the alloy containing 0.10%Sn. But above 0.20%Sn additions, tensile strength was decreased by the segregation of Sn.

Consideration of Methods Evaluating the Growing Process of Stress Corrosion Cracking of the Sensitized 18-8 Austenitic Stainless Steel in High Temperature Water Based on Electric Circuit Theory: The Effects of Stress Factors

  • Tsukaue, Yasoji
    • Corrosion Science and Technology
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    • v.6 no.3
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    • pp.103-111
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    • 2007
  • The effect of stress factors on the growing process of stress corrosion cracking (SCC) of the sensitized 18-8 stainless steel in high temperature water was investigated using equations of crack growth rate derived from applying electric circuits to SCC corrosion paths. Three kinds of cross sections have to be considered when electric circuit is constructed using total current. The first is ion flow passage area, $S_{sol}$, of solution in crack, the second is total dissolving surface area, $S_{dis}$, of metal on electrode of crack tip and the third is dissolving cross section, $S_{met}$, of metal on grain boundary or in base metal or in welding metal. Stress may affect each area. $S_{sol}$ may depend on applied stress, $\sigma_{\infty}$, related with crack depth. $S_{dis}$ is expressed using a factor of $\varepsilon(K)$ and may depend on stress intensity factor, K only. SCC crack growth rate is ordinarily estimated using a variable of K only as stress factor. However it may be expected that SCC crack growth rate depends on both applied stress $\sigma_{\infty}$ and K or both crack depth and K from this consideration.$\varepsilon(K)$ is expressed as ${\varepsilon}(K)=h_2{\cdot}K^2+h_3{\cdot}K^3$ when $h_{2}$ and $h_{3}$ are coefficients. Also, relationships between SCC crack growth rate, da/dt and K were simulated and compared with the literature data of JBWR-VIP-04, NRC NUREG-0313 Rev.2 and SKIFS Draft. It was pointed out in CT test that the difference of distance between a point of application of force and the end of starter notch (starting point of fatigue crack) may be important to estimate SCC crack growth rate. An anode dissolution current density was quantitatively evaluated using a derived equation.

Effect of internal Stress on the Strength of PZT Cermics (PZT 세라믹스의 강도에 미치는 내부응력의 영향)

  • 태원필;윤여범;김송희
    • Journal of the Korean Ceramic Society
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    • v.33 no.1
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    • pp.49-55
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    • 1996
  • The aim of this study is to investigate the change of bending strength and fatigue strength in the unpoled and poled Pb(Zr, Ti)O3 ferroelectrics of tetragonal morphotropic phase boundary (MPM) and rhombohedral com-position in terms of internal stress which is measured by XRD method. Before poling treatment the highest bending strength was found in rhombohedral composition. After poling treatment the bending strength decreas-ed in all compositions but it decreased most remarkably in tetragonal composition. The most prominent de-crease of bending strength after poling treatment in tetragonal was attributed to the occurrence of microcracks due to highanisotropic internal stress around grain boundary which was induced of bending strength after poling in MPB and rhombohedral composition was not due to the occurrence of microcracks but to the increase in tensile internal stress perpendicular to the direction of crack propagation by domain alignment. Fatigue strength was higher before poling treatment than after poling treatment for various compositions.

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Changes of Lamellar Structure of TiAl Intermetallic Compound Heat Treatment (열처리에 따른 TiAl금속간화합물의 층상조직 변화)

  • Shin, Jae-Kwan;Chung, In-Sang;Park, Kyuong-Chae
    • Journal of the Korean Society for Heat Treatment
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    • v.6 no.3
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    • pp.127-137
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    • 1993
  • The changes of lamellar(${\alpha}_2+{\gamma}$) structure of TiAl intermetallic compound which is a high potential, high temperature aerospace material was investigated by heat treatment. The lamellar structure was short and made subgrain in prior a grains after homogenizing at 1523 K. It became longer and finer, and the subgrain went out during subsequent isothermal heatteating at 1273 K. The yield, fracture strength and strain to fracture if the heat treated specimens was increased and the hardness of them was decreased a little in the finer lamellar structure, because fine lamellar interface, sugrain boundary and grain boundary may block initiation and propagation of crack.

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Fabrication of cube textured Au/Ni template using electoless-plating (무전해 도금법을 이용한 cube 집합조직을 가지는 Au/Ni template 제조)

  • Lim Jun Hyung;Kim Jung Ho;Jang Seok Hem;Kim Kyu Tae;Lee Jin Sung;Yoon Kyung Min;Joo Jinho;Kim Chan-Joong;Ha Hong-Soo;Park Chan
    • Progress in Superconductivity
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    • v.6 no.2
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    • pp.133-137
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    • 2005
  • We fabricated the Au/Ni template for YBCO coated conductors and evaluated texture formation and the microstructural evolution. The cube textured Ni substrate was fabricated by rolling and recrystallization annealing, and subsequently Au layer formed on the substrate by electroless-plating method. The texture was evaluated by pole-figure with x-ray goniometer with orientation distribution function (ODF) analysis. The surface roughness and grain boundary morphology of template were characterized by atomic force microscopy (AFM) We observed that Au layer deposited epitaxially on Ni substrate and formed a strong cube texture when plating time was optimized. The full-width at half-maximum (FWHM) was $8.4^{\circ}$ for out-of-plane and $9.98^{\circ}$ for in-plane texture for plating time of 30 min. Microstructural observation showed that the Au layer was homogeneous and dense without formation of crack/microcrack. In addition, we observed that root-mean-square (RMS) and depth of grain boundary were 14.6 nm and 160 $\AA$ for the Au layer, respectively, while those were 27.0 nm and 800 $\AA$ for the Ni substrate, indicating that the electoless-plated Au layer had relatively smooth surface and effectively mollified grain groove.

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Mechanism of Crack Formation in Pulse Nd YAG Laser Spot Welding of Al Alloys (Al합금 펄스 Nd:YAG 레이저 점 용접부의 균열 발생기구)

  • Ha, Yong Su;Jo, Chang Hyeon;Gang, Jeong Yun;Kim, Jong Do;Park, Hwa Sun
    • Journal of Welding and Joining
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    • v.18 no.2
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    • pp.213-213
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    • 2000
  • This study was performed to investigate types and formation mechanism of cracks in two Al alloy welds, A5083 and A7NO1 spot-welded by pulse Nd: YAG laser, using SEM, EPMA and Micro-XRD. In the weld zone, three types of crack were observed: center line crack($C_{C}$), diagonal crack($C_{D}$), and U shape crack($C_{U}$). Also, HAZ crack($C_{H}$), was observed in the HAZ region, furthermore, mixing crack($C_{M}$), consisting of diagonal crack and HAZ crack was observed.White film was formed at the hot crack region in the fractured surface after it was immersed to 10%NaOH water. In the case of A5083 alloy, white films in C crack and $C_D crack region were composed of low melting phases, Fe₂Si$Al_8$ and eutectic phases, Mg₂Al₃ and Mg₂Si. Such films observed near HAZ crack were also consist of eutectic Mg₂Al₃. In the case of A7N01 alloy, eutectic phases of CuAl₂, $Mg_{32}$ (Al,Zn) ₃, MgZn₂, Al₂CuMg and Mg₂Si were observed in the whitely etched films near $C_{C}$ crack and $C_{D}$ crack regions. The formation of liquid films was due to the segregation of Mg, Si, Fe in the case of A5083 alloy and Zn, Mg, Cu, Si in the case of A7N01 aooly, respectively.The $C_{D}$ and $C_{C}$ cracks were regarded as a result of the occurrence of tensile strain during the welding process. The formation of $C_{M}$ crack is likely to be due to the presence of liquid film at the grain boundary near the fusion line in the base metal as well as in the weld fusion zone during solidification. The $C_{U}$ crack is considered a result of the collapsed keyhole through incomplete closure during rapid solidification. (Received October 7, 1999)