• 제목/요약/키워드: Gas-phase Analysis

검색결과 882건 처리시간 0.032초

Volatile Metabolic Markers for Monitoring Pectobacterium carotovorum subsp. carotovorum Using Headspace Solid-Phase Microextraction Coupled with Gas Chromatography-Mass Spectrometry

  • Yang, Ji-Su;Lee, Hae-Won;Song, Hyeyeon;Ha, Ji-Hyoung
    • Journal of Microbiology and Biotechnology
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    • 제31권1호
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    • pp.70-78
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    • 2021
  • Identifying the extracellular metabolites of microorganisms in fresh vegetables is industrially useful for assessing the quality of processed foods. Pectobacterium carotovorum subsp. carotovorum (PCC) is a plant pathogenic bacterium that causes soft rot disease in cabbages. This microbial species in plant tissues can emit specific volatile molecules with odors that are characteristic of the host cell tissues and PCC species. In this study, we used headspace solid-phase microextraction followed by gas chromatography coupled with mass spectrometry (HS-SPME-GC-MS) to identify volatile compounds (VCs) in PCC-inoculated cabbage at different storage temperatures. HS-SPME-GC-MS allowed for recognition of extracellular metabolites in PCC-infected cabbages by identifying specific volatile metabolic markers. We identified 4-ethyl-5-methylthiazole and 3-butenyl isothiocyanate as markers of fresh cabbages, whereas 2,3-butanediol and ethyl acetate were identified as markers of soft rot in PCC-infected cabbages. These analytical results demonstrate a suitable approach for establishing non-destructive plant pathogen-diagnosis techniques as alternatives to standard methods, within the framework of developing rapid and efficient analytical techniques for monitoring plant-borne bacterial pathogens. Moreover, our techniques could have promising applications in managing the freshness and quality control of cabbages.

지오빗을 이용한 동해 가스하이드레이트 탄성파 자료처리 매개변수 분석 (Parameter analysis for gas hydrate data of East sea using Geobit)

  • 김영완;장성형;김현태;윤왕중
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2006년도 춘계학술대회
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    • pp.377-381
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    • 2006
  • A seismic survey for gas hydrate have performed over the East sea by the KIGAM since 1997. General indicator of gas hydrate in seismic data is commonly inferred from the BSR(Bottom Simulating Reflector) that occurred parallel to the sea floor, amplitude decrease at the top of the BSR, amplitude blanking at the bottom of the BSR, decrease of the interval velocity and the reflection phase reversal at the BSR. In this paper we had analyzed optimum parameters of the field data to detect the 9as hydrate. Shot delay correction is applied 95ms, spherical divergence correction is applied velocity library 3, bandpass filter is applied 25-30-115-120Hz deconvolution operator length is applied 60ms, lag is 6ms and accurate velocity analysis NMO correction, stack is performed. Geobit 2.11.0 developed by the KIGAM was used for all data processing. Processing results say that the BSR occurred parallel to the sea floor were shown at 3,150m/s of two way travel time from the sea floor through shot point 5,000-5,610, and identified the interval velocity decrease around BSR and the reflection phase reversal corresponding to the reflection at the sea floor.

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증발디젤분무의 혼합기 형성과정에 대한 열역학적 접근 (Thermodynamic Approach to the Mixture Formation Process of Evaporative Diesel Spray)

  • 염정국
    • 대한기계학회논문집B
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    • 제33권3호
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    • pp.201-206
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    • 2009
  • The focus of this work is placed on the analysis of the mixture formation process under the evaporative diesel-free spray conditions. In order to examine homogeneity of mixture within the vapor phase region of the injected spray, image analysis was carried out based on the entropy of statistical thermodynamics. As an experimental parameter, the injection pressure and ambient gas density were selected, and effects of the injection pressure and density variation of ambient gas on the mixture formation process in the evaporative diesel spray were investigated. In the case of application of the thermodynamic entropy analysis to evaporative diesel spray, the value of the dimensionless entropy always increases with increase in time from injection start. Consequently, the dimensionless entropy in the case of the higher injection pressure is higher than that of lower injection pressure during initial injection period.

S-ALE를 이용한 다공질 매체 거동의 유한요소해석 (Finite Element Analysis for Behavior of Porous Media Using the S-ALE Method)

  • 박대효;탁문호
    • 한국전산구조공학회:학술대회논문집
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    • 한국전산구조공학회 2006년도 정기 학술대회 논문집
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    • pp.381-388
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    • 2006
  • A porous medium is composed of solids, fluids, and gas which have different physical and chemical properties. In addition, these constituents have a relative velocity between each other. So far, in order to analyze porous media using finite element method, Lagrangian or Eulerian method has been used. However, the numerical analyses for porous media have a defect that the methods do not describe the movements of constituents. In this paper, numerical analysis for unsaturated porous media was performed in frame of ALE method which has advantages of Lagrangian and Eulerian. Namely, the Lagrangian description was used in solid phase, and the Eulerian description was used in fluid or gas phase in a porous medium Then the relationship between each other was controlled by the convective term in ALE method. Finally, the numerical results of ALE were compared with tile results of Lagrangian analysis.

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액상으로 분사되는 기체의 불안정성 해석 (Instability analysis of gas injection into liquid)

  • 김형준;권세진
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2006년도 제26회 춘계학술대회논문집
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    • pp.57-60
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    • 2006
  • 액상의 환경으로 고속의 기체가 분사될 때 기체-액체 표면에서 일어나는 불안정성에 대해 점성전위 유동의 이론을 이용하여 분석하였다. 기체의 속도가 낮을 경우 액상으로 기포로 형성되지만 속도가 증가하면서 기체는 제트의 형태로 변하게 되는데, 천음속 구간에서 제트로 변하게 되는 것으로 알려져 있다. 본 연구에서는 주로 액체 제트를 해석하는데 사용된 점성전위유동이론을 기체 제트의 불안정성 해석에 응용하였다. 천음속 구간에서 기체 제트의 성장률이 변하는 것을 확인하였다. 초음속 구간으로 가면서 성장률이 감소하는 것을 확인하였다. 그리고 이를 레이놀즈수와 같은 무차원수에 대해 기체 제트의 성장률의 변화에 대해 알아보았다.

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차압유량계를 이용한 기액 2상유량 및 건도의 동시측정 가능성에 관한 연구 (A Feasibility Study of Simultaneous Measurement of Gas-Liquid Two-Phase Flowrate and Quality with a Sharp-Edged Orifice)

  • 이상천;오홍의;김중엽
    • 대한기계학회논문집
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    • 제10권3호
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    • pp.335-342
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    • 1986
  • 본 연구에서는 이러한 가능성을 알아 보기 위하여 오리피스판을 통하여 기액 2상흐름이 있을 때 각 상의 유량변화레 따른 순간압력강하치를 분석하고자 한다. 우선 평균압력강하치를 측정하여 식 (1)과 비교 분석하며, 교란치의 평균진폭과 교란 강도를 구하여 기공율의 변화에 따른 이러한 통계치들의 경향을 고찰한다. 그리고 순간압력강하 곡선에 대한 통계함수들, 확률밀도함수(probability density function) 와 자기상관함수(auto-correlation function)을 구하여 이 들의 통계적 성질을 구명 하고 2상 유동량의 결정에 대한 교란치의 할동도를 토의한다.

DISCRETE PARTICLE SIMULATION OF DENSE PHASE PARTICULATE FLOWS

  • Tsuji Y.
    • 한국전산유체공학회:학술대회논문집
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    • 한국전산유체공학회 2005년도 추계 학술대회논문집
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    • pp.11-19
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    • 2005
  • First, methods of numerical analysis of gas-particle flows is classified into micro, meso and macro scale approaches based on the concept of multi-scale mechanics. Next, the explanation moves on to discrete particle simulation where motion of individual particles is calculated numerically using the Newtonian equations of motion. The author focuses on the cases where particle-to-particle interaction has significant effects on the phenomena. Concerning the particle-to-particle interaction, two cases are considered: the one is collision-dominated flows and the other is the contact-dominated flows. To treat this interaction mathematically, techniques named DEM(Distinct Element Method) or DSMC (Direct Simulation Monte Carlo) have been developed DEM, which has been developed in the field of soil mechanics, is useful for the contact -dominated flows and DSMC method, developed in molecular gas flows, is for the collision-dominated flows. Combining DEM or DSMC with CFD (computer fluid dynamics), the discrete particle simulation becomes a more practical tool for industrial flows because not only the particle-particle interaction but particle-fluid interaction can be handled. As examples of simulations, various results are shown, such as hopper flows, particle segregation phenomena, particle mixing in a rotating drum, dense phase pneumatic conveying, spouted bed, dense phase fluidized bed, fast circulating fluidized bed and so on.

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SPME를 이용한 수용액중의 휘발성 유기화합물 분석 (Determination of Volatile Organic Compounds (VOCs) in Drinking Water using Solid Phase Microextraction (SPME))

  • 박교범;이석근
    • 분석과학
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    • 제13권3호
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    • pp.277-281
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    • 2000
  • 16종의 휘발성 유기화합물을 blank water에 첨가하고 고정상으로 $100{\mu}m$ polydimethyl siloxane을 입힌 solid phase microextraction(SPME) fiber를 사용하는 headspace SPME방법으로 추출하여 gas chromatography/mass spectrometry (GC/MS)로 분석하였다. 이 방법의 평균회수율은 97%, 평균상대표준편차는 4.7%, 그리고 검출한계는 $0.01-0.5{\mu}g/l$를 나타냈다. 즉 SPME 방법을 이용한 수용액 중의 휘발성 유기화합물의 결과는 현재 많이 사용되고 있는 기존의 다른 방법보다 우수하고 편리한 방법으로 나타났다.

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Ni5Y 합금상이 형성된 Ni계 산화물 분산강화 아토마이징 분말의 밀링 거동 분석 (Analysis on Milling Behavior of Oxide Dispersion Strengthened Ni-based Atomizing Powder with Ni5Y Intermetallic Phase)

  • 박천웅;변종민;최원준;김영도
    • 한국분말재료학회지
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    • 제26권2호
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    • pp.101-106
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    • 2019
  • Ni-based oxide dispersion strengthened (ODS) alloys have a higher usable temperature and better high-temperature mechanical properties than conventional superalloys. They are therefore being explored for applications in various fields such as those of aerospace and gas turbines. In general, ODS alloys are manufactured from alloy powders by mechanical alloying of element powders. However, our research team produces alloy powders in which the $Ni_5Y$ intermetallic phase is formed by an atomizing process. In this study, mechanical alloying was performed using a planetary mill to analyze the milling behavior of Ni-based oxide dispersions strengthened alloy powder in which the $Ni_5Y$ is the intermetallic phase. As the milling time increased, the $Ni_5Y$ intermetallic phase was refined. These results are confirmed by SEM and EPMA analysis on microstructure. In addition, it is confirmed that as the milling increased, the mechanical properties of Ni-based ODS alloy powder improve due to grain refinement by plastic deformation.

천연가스 생산기지 시설물의 내진성능평가 절차 (Procedure of Seismic Performance Evaluation of LNG Receiving Terminal Facilities)

  • 이태형;이은숙;박태규;홍성경;김준호
    • 한국안전학회지
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    • 제29권4호
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    • pp.110-115
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    • 2014
  • It is crucial for important facilities to withstand strong earthquakes because their damage may cause undesirable socio-economic effect. A liquefied natural gas (LNG) receiving terminal is one of the lifeline facilities whose seismic safety needs to be guaranteed. Even though all operating LNG receiving terminals in Korea were seismically designed, old design codes do not guarantee to comply with the current seismic design codes. In addition, if the constructional materials have been deteriorated, the seismic capacity of facilities may be also deteriorated. Therefore, it is necessary that the seismic performance of LNG receiving terminals is evaluated and the facilities that lack of seismic capacity have to be rehabilitated. In this paper, a procedure of seismic performance evaluation of such facilities is developed such that the procedure consists of three phases, namely pre-analysis, analysis, and evaluation phases. In the pre-analysis phase, design documents are reviewed and walk-on inspection is performed to determine the current state of the material properties. In the analysis phase, a structural analysis under a given earthquake or a seismic effect is performed to determine the seismic response of the structure. In the evaluation phase, seismic performance of the structure is evaluated based on limit states. Two of the important facilities, i.e. the submerged combustion vaporizer (SMV) and pipe racks of one of the Korean LNG receiving terminals are selected and evaluated according to the developed procedure. Both of the facilities are safe under the design level earthquake.