• 한국재료학회지
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• 제14권5호
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• pp.368-373
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• 2004

To improve the conventional cathode-supported tubular solid oxide fuel cell (SOFC) from the viewpoint of low cell power density, expensive fabrication process and high operation temperature, the anode-supported tubular solid oxide fuel cell was investigated. The anode tube of Ni-8mol% $Y_2$O$_3$-stabilized $ZrO_2$ (8YSZ) was manufactured by extrusion process, and, the electrolyte of 8YSZ and the multi-layered cathode of $LaSrMnO_3$(LSM)ILSM-YSZ composite/$LaSrCoFeO_3$ were coated on the surface of the anode tube by slurry dip coating process, subsequently. Their cell performances were examined under gases of humidified hydrogen with 3% water and air. In the thermal cycle condition of heating and cooling rates with $3.33^{\circ}C$/min, the anode-supported tubular cell showed an excellent resistance as compared with the electrolyte-supported planar cell. The optimum hydrogen flow rate was evaluated and the air preheating increased the cell performance due to the increased gas temperature inside the cell. In long-term stability test, the single cell indicated a stable performance of 300 mA/$\textrm{cm}^2$ at 0.85 V for 255 hr.

• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제52권12호
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• pp.579-585
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• 2003

Recently the utilization of the ozone dissolved de-ionized water(DI-O3 water) in semiconductor wet cleaning process to replace the conventional RCA methods has been studied. In this paper, we propose the water-electrode type ozone generator which has the ozone gas characteristics of the high concentration and high purity to produce the high concentration DI-O3 water for the silicon wafer surface cleaning process. The ozone generator has the dual dielectric tube structure of silent discharge type and the water is both used to electrode and cooling water. We investigate the performance of the proposed ozone generator which has the design goal of the concentration of 7[wt%] and ozone generation quantity of 6[g/hr] at flow rate of 1[$\ell$/min). The experiment results show that the water electrode type ozone generator has the characteristics of 8.48[wt%] of concentration, 8.08[g/hr] of generation quantity and 76.2[g/kWh] of yield and it's possible to use the proposed ozone generator for the DI-O3 water cleaning process of silicon wafer surface.

• 오토저널
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• 제5권4호
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• pp.10-16
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• 1983

액체의 미립화는 기계산업분야 뿐만 아니라, 농약살포, 화학 공학의 분무건조, 반응의 촉진, 분 체제조, 식품공업 등 폭넓게 이용되며 또한 각분야에서 그 필요성이 강조되고 있다. 특히 기계 산업분야에서는 액체연료의 분무연소(boiler, gas turbine, 자동차용engine등) 원자로 노심의 spray cooling, spray drying, spray painting 등 그 이용도는 날로 증가되는 추세에 있다. 액체를 미 립화하는 이유는 각각의 분야나 사용하는 목적에 따라 다르지만, 대별하면 다음과 같다. (1) 액체의 단위 체적당 표면적을 증대시키기 위하여 (2) 직경이 작은 입자의 필요성 (3) 균일한 입경의 액적군을 얻기 위하여 등을 들 수 있다. 액체의 미립화에 대한 요구는 산업의 발당, 대기오염, 생energy 등의 문제가 중요시됨에 따라 다양화되고 있다. 따라서 응용면에서는 atomizer의 성능개선과 설계법, 새로운 미립화방법, 상업에의 분무이용기술, 분무계측법 등의 개발이 필요하게 된다. 액체미립화에서 취급하는 사항은 그 내용에 따라 다음과 같이 분류된다. (1) 액체의 미립화기구 : 기액계면의 불안정성과 분열기구에 관한 것으로, 액체형상으로써 액주, 액막 및 액적으로 나눌 수 있다. (2) 액체의 미립화 방법과 특성 : energy의 종유와 부가방식에 따랄 나누어진다. (3) 합체, 분산, 증발 등 분무의 운동이나 열적거동 (4) 분무입경이나 운동의 계측법과 특성도시 (5) 액체미립화의 각종응용 본보에서는 상기의 각 항목중, 특히 액체의 미립화방법과 분무특성에 대해서만 말하기로 한다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2013년도 제45회 하계 정기학술대회 초록집
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• pp.190.2-190.2
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• 2013

Vanadium dioxide ($VO_2$) has been widely attracted for academic research and industrial applications due to its metal-insulator transition (MIT) temperature close to room temperature. We synthesized VOx film on (0001) sapphire substrate with vanadium target (purity: 99.9%) using DC magnetron sputtering in Ar ambience at a pressure of $10^{-3}$ Torr at $400{\sim}700^{\circ}C$. The VOx film subsequently was annealed at difference temperatures in ambience of Ar and $O_2$ gas mixture at $60{\sim}800^{\circ}C$. The structural properties of the films were investigated using scanning electron microscopic (SEM), x-ray diffraction (XRD) and x-ray absorption fine structure (XAFS) measurements. SEM reveal that small grains formed on the substrates with a roughness surface. XRD shows oriented $VO_2$(020) crystals was deposited on the $Al_2O_3$(006) substrate. From I-V measurements, the electric resistance near its MIT temperature were dramatically changed by ${\sim}10^4$ during heating and cooling the films. We will also discuss the temperature-dependent local structural changes around vanadium atoms using XAFS measurements.

• Journal of Welding and Joining
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• 제22권1호
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• pp.77-82
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• 2004

The effect of bonding condition on tensile properties of joints diffusion bonded spheroidal graphite cast iron, FCD60 to Cr-Mo steel, SCM 440 was investigated. Diffusion bonding was performed with various temperatures, holding times, pressures and atmospheres. All tensile specimens were fractured at the bonding interface. The tensile strength and elongation was increased with increasing bonding temperature. Especially, tensile strength of joints bonded at 1123K was higher than that of a raw material, FCD60, and tensile strength of joints bonded at 1173K was equal to that of a raw material, SCM440, but elongation of all joints was lower than those of raw materials. There was little the effect of holding time on the tensile properties. In comparison with bonding atmosphere, the difference of tensile strength was not observed, but elongation of joint bonded at vacuum(6.7mPa and 67mPa) was higher than that of Ar gas. Higher the degee of vacuum, elongation increased. Tensile properties of diffusion bonds depended on microstructures of cast iron at the interface and void ratio. Microstructures of cast iron at interface changed with temperature, because decarburizing and interdiffusion at the interface occurs and transformation of austenite-1 ferrite + graphite occurs on the cooling process. The void ratio decreased with increasing temperature, especially, effected on the elongation.

• 한국화재소방학회:학술대회논문집
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• 한국화재소방학회 1997년도 International Symposium on Fire Science and Technology
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• pp.289-296
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• 1997

This paper discribes an experimental explosion risk assessment study on refrigerators containing flammable hydrocarbon refrigerant. A refrigerator used in this study is a larder fridge type, 215 liter in volume. The hydrocarbon refrigerant used in the refrigerator is iso-butane(C$_4$H$_{10}$). For the explosion safety assessment of the refrigerator, temperature of compressor, cooling air circulation fan motor, defrost heater and inner lamp were measured during the operation. And to confirm the ignitablity of flammable gas by the electric spark of the switches of the refrigerator, ON-OFF test of all switches were conducted with compulsorily near the stoichiometric concentration atmosphere of iso-butane-air mixture. As the result of experiment above mentioned and another experiment for the explosion safety assessment, we can conclude that explosion hazard in connection with the use of hydrocarbon refrigerant was few.w.

• 한국산학기술학회논문지
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• 제9권3호
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• pp.587-592
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• 2008

이산화탄소 냉매 시스템용 내부 열교환기의 성능을 조사하기 위하여 4종류의 내부 열교환기를 사용하여 냉방운전조건에서 실험을 수행하였다. 내부 열교환기의 길이, 관 개수, 운전조건, 형상 변화에 대한 영향이 연구되었다. 내부 열교환기 길이가 증가할수록 능력과 효율은 향상되었다. 압력강하는 고압측보다 저압측에서 더 크게 나타났다. 가스쿨러의 온도가 높아질수록 능력과 효율은 선형적으로 증가하였으며, 증발기의 운전조건은 과열도보다는 이상영역을 설정하면 효율증대 효과 측면에서 유리하였다. 마이크로 채널의 경우가 튜브보다 능력과 효율이 크게 우수하였지만 압력강하 측면에서는 크게 불리하였다.

• Advances in materials Research
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• 제9권1호
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• pp.15-32
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• 2020

In this article, an analytical solution is presented for the steady-state axisymmetric thermal stress distributions in a composite hollow cylinder. The cylinder is composed of two isotropic and anisotropic materials which is subjected to the thermal boundary conditions of convective as well as radiative heating and cooling on the inner and outer surfaces, respectively. The solution of the temperature is obtained by means of Bessel functions and the thermal stresses are developed using Potential functions of displacement. Numerical results are derived for a cylinder which is similar to a gas turbine combustor and showed that the maximum temperature and thermal stresses (radial, hoop, axial) occurred in the middle point of cylinder and the values of thermal stresses in anisotropic cylinder are more than the isotropic cylinder. It is worthy to note that the values of the thermal conditions which estimated in this research, not to be presented in any other papers but these values are very accurate in calculation.

• Bulletin of the Korean Chemical Society
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• 제22권7호
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• pp.703-708
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• 2001

K2NiF4-type organic-based perovskites of the (C4H9NH3)2FexPb1-xCl4 (x=0.00, 0.25, 0.50, and 0.75) system have been synthesized using a low-temperatu re solution method under a flowing argon gas. When stoichiometric butylamine, iron chloride, and lead chloride are mixed, a yellow solution are obtained from slow cooling of 90 to -10 $^{\circ}C.$ The final product is a plate-like yellow crystal. The X-ray crystallographic analysis has been carried out using XRD in the range of $5^{\circ}{\leq}$ 2${\theta}$ ${\leq}80^{\circ}.$ The local symmetry around the absorbing Pb atom of the samples has been determined by the EXAFS spectroscopic study. The crystals assign to orthorhombic system by the XRD analysis. The FT-IR spectra are analyzed in the range of 600 to 3300 cm-1 . DSC and TGA are measured to detect thermal stability between 30 and 300 $^{\circ}C.$ Two endothermic peaks are detected in all samples. The electrical conductivity has been measured using the four-probes technique for the (C4H9NH3)2FexPb1-xCl4 system in 300-460 K. Photoluminescence phenomenon was also investigated at room-temperature.

• 한국추진공학회지
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• 제6권4호
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• pp.1-6
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• 2002

소형 연소기의 냉각 유로 설계를 위하여 열전달 및 냉각 유로의 구조해석을 수행하였다. 연소기의 고온가스에서의 열전달에 관한 2차원 해석을 수행하여 연소실 벽으로의 열유속을 예측한 다음 이를 3차원 해석을 위한 열경계 조건으로 적용하였다. 위 방법으로 예측한 열 유속은 기존의 경험식과 비교하여 검증하였으며 냉각수의 유량에 둔감한 것으로 판명되어 냉각 조건이 변화하더라도 동일한 열경계 조건을 사용할 수 있었다. 단일 냉각 유로에 대한 3차원 해석을 수행하여 연소실 벽의 최대온도 변화를 예측하였으며 이는 재사용 연소기 개발에 적용될 것이다. 냉각 유로의 정적 구조 해석을 통해 응력 분포와 구조 안전성을 예측하였다.