• Journal of Powder Materials
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• v.30 no.1
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• pp.13-21
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• 2023

In additive manufacturing, the flowability of feedstock particles determines the quality of the parts that are affected by different parameters, including the chemistry and morphology of the powders and particle size distribution. In this study, the microstructures and flowabilities of gas-atomized heat-resistant alloys for additive manufacturing applications are investigated. A KHR45A alloy powder with a composition of Fe-30Cr-40Mn-1.8Nb (wt.%) is fabricated using gas atomization process. The microstructure and effect of powder chemistry and morphology on the flow behavior are investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and revolution powder analysis. The results reveal the formation of spherical particles composed of single-phase FCC dendritic structures after gas atomization. SEM observations show variations in the microstructures of the powder particles with different size distributions. Elemental distribution maps, line scans, and high-resolution XPS results indicate the presence of a Si-rich oxide accompanied by Fe, Cr, and Nb metal oxides in the outer layer of the powders. The flowability behavior is found to be induced by the particle size distribution, which can be attributed to the interparticle interactions and friction of particles with different sizes.

• Proceedings of the Materials Research Society of Korea Conference
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• 1998.11a
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• pp.21-21
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• 1998

• Journal of ILASS-Korea
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• v.4 no.3
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• pp.32-41
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• 1999

In this research, internal-mixing twin-fluid atomizer using sonic energy is designed and manufactured. We are trying to intimate high efficiency twin-fluid atomizer to obtain good liquid atomization in the low pressure region. Define of geometric form of atomizer, characteristics of spray is influenced by position, depth and height variation of cavity resonator, variation of sound intensity and resonant sound frequency with liquid flow rate. The liquid atomization is promoted by multi-stage disintegration of mixing flow of gas with liquid and the optimum condition of position and depth of cavity resonator according to sonic energy is obtained from the condition at a=2.5mm and L=2mm. The velocity distribution of droplets shows negative value due to recirculation region at the center of axial, and as the radial direction distance is far, the velocity distribution of droplets decrease slowly after having a maximum value. However velocity and SMD show nearly uniform distribution at the down stream and as result compared to Nukiyama and Tanasawa's equation. atomization of mixing flow with air and liquid dispersing from the outlet of the nozzle is promoted by the effect of collision at the cavity resonator.

• Journal of Powder Materials
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• v.14 no.6
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• pp.372-379
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• 2007

The microstructure, mechanical and electrochemical properties of plasma electrolytic coatings (PEO) coatings on Mg-4.3 wt%Zn-1.0 wt%Y and Mg-1.0 wt%Zn-2.0 wt%Y alloys prepared by gas atomization, followed by compaction at 320 for 10 min under the pressure of 700 MPa and sintering at 380 and 420 respectively for 24 h, were investigated, which was compared with the cast Mg-1.0 wt%Zn alloy. All coatings consisting of MgO and $Mg_2SiO_4$ oxides showed porous and coarse surface features with some volcano top-like pores distributed disorderly and cracks between pores. In particular, the surface of coatings on Mg-1.0 wt%Zn-2.0 wt%Y alloy showed smaller area of pores and cracks compared to the Mg-4.3 wt%Zn-1.0 wt%Y and Mg-1.0 wt%Zn alloys. The cross section micro-hardness of coatings on the gas atomized Mg-Zn-Y alloys was higher than that on the cast Mg-1.0 wt%Zn alloy. Additionally, the coated Mg-1.0 wt%Zn-2.0 wt%Y alloy exhibited the best corrosion resistance in 3.5%NaCl solution. It could be concluded that the addition of Y has a beneficial effect on the formation of protective and hard coatings on Mg alloys by plasma electrolytic oxidation treatment.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.33 no.1
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• pp.62-68
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• 2005

An injector for fuel rich gas generator was designed and experimentally investigated. Five variations of F-O-F triplet impinging type injector were tested to evaluate spray characteristics with kerosene/water simulant propellant. Test was focused to find the effect of design variables of impinging angle, and impinging distance, on the atomization performance. A mixing efficiency is used to compare droplet distribution and local O/F ratio of each injector in the range of momentum ratio of 0.2~1.3. Test results shows the max value of mixing efficiency locates about the 0.8 in momentum ratio. And the injector with an impinging angle of 45 degree and impinging distance of 6mm shows the very good performance result suitable for fuel rich gas generator. A combustion test will be also conducted with selected injector to verify the spray pattern and mixing efficiency.

• Journal of Korea Foundry Society
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• v.31 no.1
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• pp.26-30
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• 2011

For the fabrication of bulk near-net-shape Ti-Ni-Cu shape memory alloys, consolidation of Ti-Ni-Cu alloy powders are useful because of their brittle property. In the present study, $Ti_{50}Ni_{30}Cu_{20}$ shape memory alloy powders were prepared by gas atomization and martensitic transformation temperatures and microstructures of those powders were investigated as a function of powder size. The size distribution of the powders was measured by conventional sieving, and sieved powders with the specific size range of 25 to $150\;{\mu}m$ were chosen for this examination. XRD analysis showed that the B2-B19 martensitic transformation occurred in the powders. In DSC curves of the as-atomized $Ti_{50}Ni_{30}Cu_{20}$ powders as a function of powder size, only one clear peak was found on each cooling and heating curve. The martensitic transformation start temperature($M_s$) of the $25-50\;{\mu}m$ powders was $31.5^{\circ}C$. The $M_s$ increased with increasing powder size and the difference of $M_s$ between $25-50\;{\mu}m$ powders and $100-150\;{\mu}m$ powders is only $1^{\circ}C$. The typical microstructure of the rapidly solidified powders showed cellular morphology and very small pores were observed in intercellular regions.

• Journal of Powder Materials
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• v.29 no.6
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• pp.459-467
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• 2022

Soft magnetic powder materials are used throughout industries such as motors and power converters. When manufacturing Fe-based soft magnetic composites, the size and shape of the soft magnetic powder and the microstructure in the powder are closely related to the magnetic properties. In this study, Fe-Si-Al-P alloy powders were manufactured using various manufacturing process parameter sets, and the process parameters of the vacuum induction melt gas atomization process were set as melt temperature, atomization gas pressure, and gas flow rate. Process variable data that records are converted into 6 types of data for each powder recovery section. Process variable data that recorded minute changes were converted into 6 types of data and used as input variables. As output variables, a total of 6 types were designated by measuring the particle size, flowability, apparent density, and sphericity of the manufactured powders according to the process variable conditions. The sensitivity of the input and output variables was analyzed through the Pearson correlation coefficient, and a total of 6 powder characteristics were analyzed by artificial neural network model. The prediction results were compared with the results through linear regression analysis and response surface methodology, respectively.

• Journal of ILASS-Korea
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• v.17 no.4
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• pp.205-209
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• 2012

This study focused on comparing macroscopic characteristics of DME and diesel fuel experimentally. DME fuel is one of the most promising alternative fuels because of its superiority in atomization characteristic and clearness in terms of exhaust gas compared with existing fossil fuels. In addition, DME fuel has high cetane number so it could be applied to compression ignition engine. However because DME fuel exists in gas phase at room temperature and atmospheric pressure, and it corrodes rubber parts of fuel line, DME fuel is hard to apply to commercial vehicles. To establish knowledge about DME fuel and furthermore, to develop commercial DME vehicles such as passenger cars, many research have been proceeded steadily. The present study, by comparing spray characteristics of DME fuel to those of diesel fuel, improved atomization characteristics in DME were revealed. Injection quantity measurement and spray visualization experiment were progressed and it was revealed that DME fuel shows small injection quantity than that of diesel fuel and axial development of spray in terms of spray tip penetration decreases when DME fuel was injected.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2010.05a
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• pp.300-303
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• 2010

This work shows the result of numerical simulation on a reacting flow by varying atomization properties which can be obtained from a injector for a small and low power aircraft gas turbine engine. Because the atomization properties mainly affect on the performance of the engine, a lot of efficiency tests are needed when a new injector is developed. Nowadays researches has been actively performed using computational analysis. Using commercial package CFD-ACE+, basic studies on the reacting flow field have been conducted. Those results show that the reaction rate is increased when higher pressure and wider angle spray condition are used. More smaller parcels can also enhance the fuel-air reaction.

• Journal of ILASS-Korea
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• v.20 no.2
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• pp.95-100
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• 2015

Lower recirculated gas temperature at EGR system reduces NOx and PM emissions. However, EGR Cooler can be polluted by PM generated from recirculated EGR gas, and it reduces cooling efficiency and the amount of EGR gas simultaneously. The SECFR(Steam EGR Cooler Fouling Remover) system which uses the evaporated washer fluid steam caused by high temperature of EGR gas was manufactured for removing fouling generated on the cooler surface. Since an injection pressure of wind shield washer fluid in the vehicle is approximately 0.5 bar, it is not enough to atomize the injected washer fluid. Thus, it is necessary to apply a method to atomize the washer fluid. In this study, the impinging plate was used to promote the atomization of spray washer fluid for the purpose of apply SECFR system to vehicles and measured the DAR(Droplet Area Ratio) and DUI(Droplet Uniformity Index) through the spray visualization.