• Mass Spectrometry Letters
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• 제4권1호
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• pp.18-20
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• 2013

Headspace solid phase micro-extraction gas chromatography/flame ionization detection (HS-SPME-GC/FID) method was compared with headspace gas chromatography/mass selective detection (HS-GC/MS). Organic solvent-spiked urine as well as urine samples from workspace was analyzed under optimal condition of each method. Detection limit of each compound by HS-SPME-GC/FID was $3.4-9.5{\mu}g/L$, which enabled trace analysis of organic solvents in urine. Linear range of each organic solvent was $10-400{\mu}g/L$, with fair correlation coefficient between 0.992 and 0.999. The detection sensitivity was 4 times better than HS-GC/MS in selected ion monitoring (SIM) mode. Accuracy and precision was confirmed using commercial reference material, with accuracy around 90% and precision less than 4.6% of coefficient of variance. Among 48 urine samples from workplace, toluene was detected from 45 samples in the range of $20-324{\mu}g/L$, but no other solvents were found. As a method for trace analysis, SPME HS GC/FID showed high sensitivity for biological monitoring of organic solvent in urine.

• Mycobiology
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• 제34권2호
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• pp.99-103
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• 2006

Toxicity of the fungicide Flutolanil was in vitro tested against 20 isolates of Macrophomina phaseolina and cotton seedlings of ten commercial cotton cultivars. The isolates were recovered from roots of cotton plants obtained from different cotton-growing areas in Egypt. Most of the tested isolates were sensitive to Flutolanil; however, they varied in sensitivity. Twenty-five percent of the isolates were highly sensitive where $IC_{50}$ ranged from < 1 to $5.1{\mu}g/ml$, 20% of the isolates were sensitive where $IC_{50}$ ranged from 15 to $30{\mu}g/ml$, 45% of the isolates were moderately sensitive where $IC_{50}$ ranged from 46 to $58.5{\mu}g/ml$, and 10% of the isolates were not much sensitive (tolerant) where $IC_{50}$ was > $100{\mu}g/ml$. Flutolanil was very safe on both shoots and roots of the tested cultivars ($IC_{50}\;>\;100{\mu}g/ml$). Treating cotton seeds with Flutolanil resulted in highly significant (P < 0.01) reductions in pathogenicity of 18 isolates and a significant reduction (P < 0.05) in pathogenicity of isolate $M_{29}.\;M_{1}$ was the only isolate, which was insensitive to the application of Flutolanil. In vivo toxicity to Flutolanil was not correlated with its in vitro toxicity. However, a highly significant correlation (r = 0.60, P < 0.01) was observed between pathogenicity of isolates and the in vivo toxicity of the fungicide.

• 대한미생물학회지
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• 제22권4호
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• pp.445-451
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• 1987

Coagglutination method is widely used for the diagnosis of Salmonella infection. This test, however, has a disadvantage of false positive reaction due to the coagglutination of staphylococci with non-specific immune complexes or anti-staphylococci antibody in serum. Salmonell O antigen was detected by enzyme immunoassay with protein A-bearing Staphylococcus aureus as in the solid phase. Horse radish peroxidase was labeled to IgG specific against Salmonella O antigen. This enzyme immunoassay was much more sensitive than conventional coagglutination method without false poitive agglutination. To improve the sensitivity for detection of Salmonella O antigen in samples, we tried to determine the optimal concentration of normal IgG that inhibits non-specific binding of horse radish peroxidase labeled IgG to staphylococci, and to establish the optimal condition of reaction between antigen-antibody complex and staphylococci. Non-specific binding of horse radish peroxidase labeled specific IgG to staphylococci was almost blocked when the enzyme labeled IgG was 500-fold diluted with phosphate buffered saline containing 2mg/ml of normal IgG. When staphylococci coated with antibody to Salmonella O antigen were mixed with antigen-antibody complex and then incubated for 1 hour at room temperature, the minimal detectable concentration of Salmonella O antigen was 1ng/ml. The sensitivity of enzyme immunoassay was 100-fold greater than a conventional coagglutination method. This enzyme immunoassay could be expected as an improved method for detection of other infectious agents.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1995년도 하계학술대회 논문집 C
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• pp.1431-1433
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• 1995

This paper describes the characteristics of Si Hall sensors fabricated on a SOI(Si-on-insulator} structure, in which the SOI structure was forrmed by SDB(Si-wafer direct bonding) technology. The Hall voltage and the sensitivity of implemented Si Hall devices show good linearity with respect to the applied magnetic flux density and supplied current. The product sensitivity of the SDB SOI Hall device is average $600V/A{\cdot}T$. In the temperature range of 25 to $300^{\circ}C$, the shifts of TCO(Temperature Coefficient of the Offset Voltage) and TCS(Temperature Coefficient of the product Sensitivity) are less than ${\pm}6.7{\times}10^{-3}/^{\circ}C$ and ${\pm}8.2{\times}10^{-4}/^{\circ}C$, respectively. From these results, Si Hall sensors using the SOI structure presented here are very suitable for high-temperature operation.

• 한국자동차공학회논문집
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• 제4권5호
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• pp.9-15
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• 1996

A silicon microaccelerometer is designed and fabricated using silicon epitaxial layers for automotive electronic airbag applications. A cantilever structure is chosen for high sensitivity and piezoresistive detection method is adopted for circuit simplicity and low cost. An optimum design is used to find optimum microstructure sizes for maximum sensitivity subject to performance requirements and design constraints on natural frequency, damping ratio, maximum allowable stress and microfabrication limitations. The microaccelerometer is fabricated by micromachining processing steps, composed of material-selective and orientation-dependent chemical etching techniques. Fabricated prototype shows a sensitivity of 88.6$\mu\textrm{V}$/g within a resonant frequency of 1.75KHz. Estimated performance of the microaccelerometer is compared with measured one. Discrepancy between the theoretical values and the experimental values is discussed together with possible sources of the errors.

• 소성∙가공
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• 제16권2호
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• pp.120-125
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• 2007

Magnesium alloy has low formability at room temperature and therefore, in many cases, forming at elevated temperatures is necessary to obtain the required material flow without failure. Tn the present study, square cup deep drawing tests using the magnesium alloy AE31 sheet were experimentally conducted using the porches and dies with different edge radius to evaluate the formability sensitivity to the die design variables. The experimental results showed that the fracture position over the cup wall moved from the punch nose to the flange as the die temperature increased, and that the drawing depth change was more affected by the punch radius than the die radius.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2001년도 춘계학술대회 논문집
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• pp.221-224
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• 2001

The dynamic characteristics of a hydraulic press for micro-stamping are investigated by Finite Element Analysis. This machine requires high precision in producing milli-structure of electric products such as TFT-LCD back-up light reflector. First, the modal analysis of the parts and the assembly of the hydraulic press is performed. Then, the sensitivity analysis is carried out. The results show that the bearing stiffness and the base mounting stiffness affect the specific mode shapes.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2000년도 하계학술대회 논문집 A
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• pp.66-68
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• 2000

The Eigen analysis in large power system provides much useful information that is not got in nose curve. The branch participation factor is not quantitative information and is an indirect method calculating incremental change in branch reactive loss. But the Eigen sensitivity analysis to each mode is direct and provides of quantitative information but this method because of needing much time is used in large power system. In this paper the Hessenberg method is used to obtaining dominant eignvalues and corresponding eigenvectors of Jacobian matrix. Ranking the critical contingencies is done by computing the Eigen sensitivity of each dominant eignvalues for changes of each line. The proposed algorithm is tested on the New England 30-bus system and KEPCO system in the year of 2000, which comprises of 791-bus and 2500-branches.

• 제어로봇시스템학회:학술대회논문집
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• 제어로봇시스템학회 1988년도 한국자동제어학술회의논문집(국제학술편); 한국전력공사연수원, 서울; 21-22 Oct. 1988
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• pp.764-769
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• 1988

In this paper the failure possibility and the error possibility are used to represent reliability of a technical component and that of a human operator, respectively. The failure possibility and the error possibility are fuzzy sets on the interval [0,1]. In a man-machine system, reliability of the technical component and that of the human operator are usually affected by many factors, e.g., the environment in which a machine is operated, psychological stress of the human operator, etc. The possibility is derived from not only the failure or the error rate but also estimates of these factors. The fuzzy reasoning plays an important role in the derivation. The reliability analysis is performed by the use of the possibility obtained by the present method. Moreover this paper discusses the sensitivity analysis which evaluates what extent the change of the estimation of each factor has an influence on reliability of a man-machine system. The important factors to be ameliorated are shown through the sensitivity analysis.

• 열처리공학회지
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• 제12권3호
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• pp.215-220
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• 1999

Rotary bending fatigue tests were carried out to investigate the artificial defect sensitivity of fatigue limit in annealed and austempered ductile irons. Artificial defect(hole, diameter${\leq}0.4mm$) machined on specimen surface did not bring about an obvious reduction of fatigue limit in austempered ductile iron as compared with annealed. As a result of investigation on $\sqrt{area}$ c which is the critical artificial defect size. $\sqrt{area}$ c of austempered ductile iron is larger than that of annealed. This means that the crack initiation at artificial defect in austempered ductile iron is more difficult in comparison with annealed. In case that the $\sqrt{area}$ c of artificial defect and graphite nodule are same, the rate of crack initiation for graphite nodule is higher than that of artificial defect.