• Title/Summary/Keyword: Function of MPA

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Residual Stresses and Phosphorous Concentration Dependence upon Electroless Nickel Process Conditions for MEMS (MEMS 소자를 위한 무전해 니켈도금의 잔류응력과 인 농도 의존성)

  • Yi, Seung-Hwan;Min, Nam-Ki;Ko, Ju-Yeol;Kim, Eun-Sok
    • Proceedings of the KIEE Conference
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    • 2000.07c
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    • pp.2224-2226
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    • 2000
  • In this paper, we tried to figure out the residual stress of Electroless Nickel (EN) films as a function of process conditions: bath temperatures, pH values, and hypophosphorous acid concentrations. The residual stresses of EN films were in the range of - 4 MPa to 250 MPa depending on process conditions and they were very sensitive to phosphorous concentration in EN film and also hypophosphorous acid concentrations in EN bath.

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Study on Sintering Properties of $TiB_2-TiC$ Composite by Self-Propagating High Temperature Synthesis Method (SHS법에 의한 $TiB_2-TiC$ 복합체의 소결특성에 관한 연구)

  • 이형복;조덕호;장준원
    • Journal of the Korean Ceramic Society
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    • v.29 no.7
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    • pp.577-585
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    • 1992
  • TiB2 and TiC were prepared from the mixture of metal titanium, boron and graphite powders in Argon atmosphere by Self-propagating High-temperature Synthesis method. The sintered properties of TiB2-TiC composite as a function of TiC content and sintering temperature were investigated in TiB2 matrix. The sintered properties were the most excellent at 10 wt% TiC content in TiB2-TiC composite. The relative density, M.O.R strength, hardness and fracture toughness of TiB2-10 wt% TiC composite sintered at 190$0^{\circ}C$ for 90 min by hot-pressing under the pressure of 30 MPa were 98.6%, 634 MPa, 2128.1 kg/$\textrm{mm}^2$ and 4.09 MN/m3/2, respectively.

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An Effective Pressure Law for the Transport Property of Granite (화강암의 수리적 특성을 고려한 유효압력법칙)

    • Tunnel and Underground Space
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    • v.7 no.4
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    • pp.293-298
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    • 1997
  • Permeability was not represented as a simple function of the difference between confining pressure($P_c$) and pore pressure($P_p$). The effective pressure($P_e$) for measurements of the permeability is shown to be $P_c-{\alpha}P_p$, where $\alpha$ is a coefficient of effective pressure. Local values of $\alpha$ were determined at intervals along the pressure path which range 25MPa to 55MPa. The values of $\alpha$ ranged 0.65 to 1.09 for Pocheon granite and 1.20 to 1.43 for Wonju granite. Also, the value of $\alpha$ calculated by the cross-plotting method was 0.90 for Pocheon granite, 1.59 for Wonju granite and 4.35 for jointed Pocheon granite. $\alpha$ was found to be stress-history dependent.

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Wear diagram and Wear Mechanisms of Bearing Steel in Frictional Sliding (미끄럼 마찰하에서의 베어링간의 마모 diagram과 마모기구)

  • 임대순;박성길;조성재;방건웅;문한규
    • Tribology and Lubricants
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    • v.6 no.1
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    • pp.108-115
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    • 1990
  • Wear diagrams, which are the three dimensional representations of the dependence of the wear rate on the applied pressure and the sliding speed, were constructed with the pin on ring type wear test results using 52100 wear couples. The pressure and speed ranges from 0.45 MPa to 45.30 MPa and from 0.012 m/sec to 0.12 (0.120)m/sec, respectively. The results show the mild to severe transition, which suggests the change of the wear mechanisms as a function of the pressure and sliding speed. The SEM micrographs of the corresponding worn area shows clearly that different wear mechanisms dominate.

Preparation and Properties of the Intra-type Al2O3Ag Nanocomposites (입내 분산형 Al2O3/Ag 나노복합체의 제조와 특성)

  • Cheon, Sung-Ho;Han, In-Sub;Awaji, Hideo
    • Journal of the Korean Ceramic Society
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    • v.44 no.4 s.299
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    • pp.208-213
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    • 2007
  • Alumina/silver ($Al_2O_3/Ag$) nanocomposites with Ag content up to 9 vol% were prepared from nanopowder by soaking method using ${\gamma}-Al_2O_3$ of needle type and spark plasma sintering (SPS). The mechanical properties of specimens were investigated three-point flexural strength and toughness as a function of the Ag contents. The maximum flexural strength of the alumina/silver nanocomposite was 850 MPa for the 1 vol% composite, and also higher than monolith alumina as about 800 MPa at 3, 5, and 7 vol% Ag contents. Fracture toughness by single edged V-notch beam (SEVNB) was $4.05MPa{\cdot}m^{1/2}$ for the 3 vol% composite and maintained about $4.00MPa{\cdot}m^{1/2}$ at 5, and 7 vol% Ag content. Microstructure of fracture surface for each fracture specimens was observed. Due to the inhibition effect of alumina grain growth, the average grain size of nanocomposites depends on the content of Ag nano particles. The fracture morphology of nanocomposite with dislocation (sub-grain boundary) by silver nano-particles of second phases in the alumina matrix also showed transgranular fracture-mode compare with intergranular of monolith alumina. Thermal conductivity of specimens at room temperature was about 40 W/mK for the 1 vol% Ag content.

Energy analysis-based core drilling method for the prediction of rock uniaxial compressive strength

  • Qi, Wang;Shuo, Xu;Ke, Gao Hong;Peng, Zhang;Bei, Jiang;Hong, Liu Bo
    • Geomechanics and Engineering
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    • v.23 no.1
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    • pp.61-69
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    • 2020
  • The uniaxial compressive strength (UCS) of rock is a basic parameter in underground engineering design. The disadvantages of this commonly employed laboratory testing method are untimely testing, difficulty in performing core testing of broken rock mass and long and complicated onsite testing processes. Therefore, the development of a fast and simple in situ rock UCS testing method for field use is urgent. In this study, a multi-function digital rock drilling and testing system and a digital core bit dedicated to the system are independently developed and employed in digital drilling tests on rock specimens with different strengths. The energy analysis is performed during rock cutting to estimate the energy consumed by the drill bit to remove a unit volume of rock. Two quantitative relationship models of energy analysis-based core drilling parameters (ECD) and rock UCS (ECD-UCS models) are established in this manuscript by the methods of regression analysis and support vector machine (SVM). The predictive abilities of the two models are comparatively analysed. The results show that the mean value of relative difference between the predicted rock UCS values and the UCS values measured by the laboratory uniaxial compression test in the prediction set are 3.76 MPa and 4.30 MPa, respectively, and the standard deviations are 2.08 MPa and 4.14 MPa, respectively. The regression analysis-based ECD-UCS model has a more stable predictive ability. The energy analysis-based rock drilling method for the prediction of UCS is proposed. This method realized the quick and convenient in situ test of rock UCS.

Shear Bond Strength of Porcelain Repair Systems (도재 수리 시스템의 전단결합강도에 관한 연구)

  • Woo, Soo;Shin, Soo-Youn;Cho, In-Ho
    • Journal of Dental Rehabilitation and Applied Science
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    • v.22 no.3
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    • pp.211-220
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    • 2006
  • Need of porcelain-repair system is largely demanding as dental porcelain restorations are increased in clinical dentistry. This study investigated shear bond strength of commercial porcelain-repair systems on dental porcelain and their reliability. Experimental groups were as follows; Group A Super Bond C&B, Group B Porcelain repair kit, Group C Ceramic repair, and Group D Spectrum system as a control. Porcelain disks were fired and embedded in epoxy resin. Porcelain surface were ground using 220 grit SiC disk, then cleaned in ultrasonic bath. Then porcelain specimens were treated with each repair system. A clear polystyrene cylinder 3.5 mm in internal diameter was filled with composite resin. Then the resin cylinder was polymerized with a visible light curing unit. Thirty one specimens at each group were prepared and stored at $37^{\circ}C$ distilled water for 48 h. Specimens were tested in an Instron testing machine according to ISO TR 11405. Mean shear bond strength and standard deviation of each group was $15.7{\pm}4.1MPa$ (Group A), $12.8{\pm}4.9MPa$ (Group B), $7.2{\pm}3.0MPa$ (Group C) and $9.6{\pm}2.2MPa$ (Group D). ANOVA and Tukey HSD post-hoc test showed that there were significant differences between groups (p<0.05). Data of bond strength were analyzed with two-parameter Weibull distribution. Confidence interval of Weibull modulus (m-parameter) at 95% of Group A (3.5-6.3) and Group D (3.6-6.0) were significantly higher than Group B (2.2-3.7) and Group C (2.0-3.4). There was little correlation between mean shear bond strength and Weibull modulus. Results indicated that acid-etching of porcelain surface increased porcelain-resin shear bonding strength.

Mechanical Properties of Zirconia Reinforced Glass-Ceramic (지르코니아 강화형 Glass-Ceramic의 기계적 성질)

  • Park, Eun-Eui;Dong, Jin-Keun;Lee, Hae-Hyoung;Song, Ki-Chang;Oh, Sang-Chun
    • Journal of Dental Rehabilitation and Applied Science
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    • v.17 no.3
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    • pp.199-204
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    • 2001
  • This study was to investigate the reused possibility of zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) with sprue button in the flexure strength and fracture toughness. 40 disk-shaped ceramic specimens (20 specimens: as-pressed material; 20 specimens: reused material) with approximately 1.7 mm thickness and 15 mm diameter were prepared by "lost wax" technique. The remnants(sprue buttons) were used for repressing. The surface treatments for the discs were gradually abraded with 320, 800, 1200, and 2000 grit SiC sandpaper. The specimens were evaluated their flexure strength with the biaxial flexure jig(ball-on-three balls) and their fracture toughness with Vickers Indentation-microfracture test. The Weibull moduli were calculated for biaxial flexural strength. The mean flexure strength and fracture toughness of each group were $122.2{\pm}18.3MPa$, $1.00{\pm}0.09MPa{\cdot}m^{0.5}$ (as-pressed ceramics), and $122.2{\pm}20.3MPa$, $1.01{\pm}0.10MPa{\cdot}m^{0.5}$ (reused ceramics). There were no significant differences in the strength and the fracture toughness between the as-pressed and the reused IPS Empress Cosmo ceramic (P>0.05). This implied zirconia reinforced glass-ceramic(IPS Empress Cosmo ceramic) could be used one more time by reusing of sprue button in the flexure strength and fracture toughness.

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A Stress-Strain Relationship of Alkali-Activated Slag Concrete (알칼리활성 슬래그 콘크리트의 응력-변형률 관계)

  • Yang, Keun-Hyeok;Song, Jin-Kyu;Lee, Kyong-Hun
    • Journal of the Korea Concrete Institute
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    • v.23 no.6
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    • pp.765-772
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    • 2011
  • The present study summarizes a series of compressive tests on concrete cylinder in order to examine the stressstrain relationship of alkali-activated (AA) slag concrete. The compressive strength and unit weight of concrete tested ranged from 8.6 MPa to 42.2 MPa and from $2,186kg/m^3$ to $2,343kg/m^3$, respectively. A mathematical equation representing the complete stress-strain curve was developed based on test results recorded from 34 concrete specimens. The modulus of elasticity, strain at peak stress, slopes of ascending and descending branches of stress-strain curves were generalized as a function of compressive strength and unit weight of concrete. The mean and standard deviation of the coefficient of variance between measured and predicted curves were 6.9% and 2.6%, respectively. This indicates that the stress-strain relationship of AA slag concrete is represented properly with more accuracy in the proposed model than in some other available models for ordinary portland cement (OPC) concrete.

Residual Stress Behavior of High Temperature Polyimide Thin Films depending on the Structural Isomers of Diamine (Diamine의 구조적 이성질체에 따른 내열성 폴리이미드 박막의 잔류응력거동)

  • 임창호;정현수;한학수
    • Journal of the Microelectronics and Packaging Society
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    • v.6 no.2
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    • pp.23-30
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    • 1999
  • The relationships between morphological structures and residual stress behaviors of polyimide thin films depending on isomeric diamines were investigated. For this study, Poly(phenylene biphenyltetracarboximide) (BPDA-PDA) and poly(oxydiphenylene biphenyltetracarboximide) (BPDA-ODA) films were prepared from their isomeric diamines: 1,3-phenylene diamine (1,3-PDA) 1,4-phenylene diamine (1.4-PDA), 3,4'-oxydiphenylene diamine (3,4'-ODA), and 4,4'-oxydiphenylene diamine (4,4'-ODA), respectively. For those films, residual stresses were detected in-situ during thermal imidization of the isomeric polyimide as a function of processing temperature over the range of 25~$400^{\circ}C$ using. Thin Film Stress Analyzer (TFSA). In comparison, residual stress of BPDA-1.4PDA having better in-plain orientation and chain order was the lowest value of 7MPa whereas those of BPDA-1,3-PDA, BPDA-3,4'-ODA, and BPDA-4,4'-ODA were in the range of 40-50MPa. Conclusively, the effect of morphological nature (chain rigidity, chain order, orientation) and chain mobility relating to the g1ass transition behavior on the residual stress of isomeric polyimide thin films wart analyzed.

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