• Title/Summary/Keyword: Fractured surfaces

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THE EFFECT OF REMOVAL OF RESIDUAL PEROXIDE ON THE SHEAR BOND STRENGTH AND THE FRACTURE MODE OF COMPOSITE RESIN-ENAMEL AFTER TOOTH BLEACHING (생활치 표백술 후 수종의 자유 산소기 제거제 처리가 복합 레진-법랑질 전단 접착 강도 및 파절 양상에 미치는 영향)

  • 임경란;금기연;김애리;장수미
    • Restorative Dentistry and Endodontics
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    • v.26 no.5
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    • pp.399-408
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    • 2001
  • Tooth bleaching has been prevailing recently for its ability to recover the color and shape of natural teeth without reduction of tooth material. However, it has been reported that bleaching procedure adversely affects the adhesive bond strength of composite resin to tooth. At the same time the bond strength was reported to be regained by application of some chemical agents. The purpose of this in vitro study was to investigate the effect of the removal of residual peroxide on the composite- enamel adhesion and also evaluated fracture mode between resin and enamel after bleaching. Sixty extracted human anterior and premolars teeth were divided into 5 groups and bleached by combined technique using of office bleaching with 35 % hydrogen peroxide and matrix bleaching with 10% carbamide peroxide for 4 weeks. After bleaching, the labial surfaces of each tooth were treated with catalase, 70% ethyl alcohol, distilled water and filled with composite resin. Shear bond strength was tested and the fractured surfaces were also examined with SEM. Analysis revealed significantly higher bond strength values. (p<0.05) for catalase-treated specimens, but water-treated specimens showed reduction of bond strength, alcohol- treated specimens had medium value between the two groups(p<0.05). The fracture mode was shown that the catalase group and the alcohol group had cohesive failure but the water sprayed group had adhesive failure. It was concluded that the peroxide residues in tooth after bleaching seems to be removed by gradual diffusion and the free radical oxygen from peroxide prevents polymerization by combining catalyst in the resin monomer. Therefore it may be possible to eliminate the adverse effect on the adhesion of composite resin to enamel after bleaching by using water displacement solution or dentin bonding agent including it for effective removal of residual peroxide.

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Study on Cryogenic Mechanical Behavior of 6000 Series Aluminum Alloys (6000계열 알루미늄 합금의 극저온 기계적 거동 연구)

  • Park, Doo-Hwan;Kim, Jeong-Hyeon;Choi, Sung-Woong;Lee, Jae-Myung
    • Journal of Ocean Engineering and Technology
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    • v.29 no.1
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    • pp.85-93
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    • 2015
  • In this study, tensile tests were performed on aluminum alloys (AA6061 and AA6082) to investigate their mechanical behaviors at cryogenic temperatures. The temperature was varied from 110 K up to 293 K, and quasi-static strain rates of 10−4 s−1 −10−2 s−1 were taken into account for the tests. The experimental results were analyzed to find the dependence on the temperature, strain rate, and fractured surfaces. As a result, it was found that the strength and elongation of the aluminum alloys were improved when the temperature was decreased. In addition, it was confirmed that the mechanical behaviors of the aluminum alloys were not dependant on the strain rate. Under a tensile load, two types of fractures were seen in the aluminum alloys: cup-cone (AA6061) and shear (AA6082).

Development of Linear Annealing Method for Silicon Direct Bonding and Application to SOI structure (실리콘 직접 접합을 위한 선형가열법의 개발 및 SOI 기판에의 적용)

  • 이진우;강춘식;송오성;양철웅
    • Journal of the Korean institute of surface engineering
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    • v.33 no.2
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    • pp.101-106
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    • 2000
  • SOI (Silicon-On-Insulator) substrates were fabricated with varying annealing temperature of $25-660^{\circ}C$ by a linear annealing method, which was modified RTA process using a linear shape heat source. The annealing method was applied to Si ∥ $SiO_2$/Si pair pre-contacted at room temperature after wet cleaning process. The bonding strength of SOI substrates was measured by two methods of Razor-blade crack opening and direct tensile test. The fractured surfaces after direct tensile test were also investigated by the optical microscope as well as $\alpha$-STEP gauge. The interface bonding energy was 1140mJ/m$^2$ at the annealing temperature of $430^{\circ}C$. The fracture strength was about 21MPa at the temperature of $430^{\circ}C$. These mechanical properties were not reported with the conventional furnace annealing or rapid thermal annealing method at the temperature below $500^{\circ}C$. Our results imply that the bonded wafer pair could endure CMP (Chemo-Mechanical Polishing) or Lapping process without debonding, fracture or dopant redistribution.

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Investigation on nanoadhesive bonding of plasma modified titanium for aerospace application

  • Ahmed, Sabbir;Chakrabarty, Debabrata;Mukherjee, Subroto;Joseph, Alphonsa;Jhala, Ghanshyam;Bhowmik, Shantanu
    • Advances in aircraft and spacecraft science
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    • v.1 no.1
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    • pp.1-14
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    • 2014
  • Physico-chemical changes of the plasma modified titanium alloy [Ti-6Al-4V] surface were studied with respect to their crystallographic changes by X-Ray Diffraction (XRD) and Scanning Electron Microscope (SEM).The plasma-treatment of surface was carried out to enhance adhesion of high performance nano reinforced epoxy adhesive, a phenomenon that was manifested in subsequent experimental results. The enhancement of adhesion as a consequence of improved spreading and wetting on metal surface was studied by contact angle (sessile drop method) and surface energy determination, which shows a distinct increase in polar component of surface energy. The synergism in bond strength was established by analyzing the lap-shear strength of titanium laminate. The extent of enhancement in thermal stability of the dispersed nanosilica particles reinforced epoxy adhesive was studied by Thermo Gravimetric Analysis (TGA), which shows an increase in onset of degradation and high amount of residuals at the high temperature range under study. The fractured surfaces of the joint were examined by Scanning electron microscope (SEM).

Micromachining & Optical Properties of Li$_2$O-A1$_2$O$_3$-SiO$_2$ Glass System by Laser Treatment (레이저에 의한 Li$_2$O-A1$_2$O$_3$-SiO$_2$계 유리의 미세가공 및 광학적 특성)

  • 강원호
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.4
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    • pp.43-45
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    • 2001
  • For photosensitive and micro-structuring in $Li_2O-A1_2O_3-SiO_2$glasses by laser treatment, Nd:YAG laser in 355 nm and 1064 nm wavelength was irradiated to the glass to investigate fracture characterization and optical changes. The fractured glass surfaces irradiated by 1064 nm laser was observed by Scanning Electron Microscope(SEM) and optical microscope, and optical changes caused by 355 nm later was identified from absorption spectra. In this study, it could be expected that the laser treatment technology will be utilized for 3-dimensional micro-structure, internal waveguide, optical memory by optical absorption changes in glass matrix.

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Effect of Matrix Structures on the Fracture Characteristics of Austempered C/V Graphite Iron (오스템퍼링처리한 C/V흑연주철의 파괴특성에 미치는 기지조직의 영향에 관한 연구)

  • Kim, Chang-Gyu;Kim, Hong-Beum;Choi, Chang-Ock
    • Journal of Korea Foundry Society
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    • v.16 no.2
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    • pp.109-115
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    • 1996
  • Effect of various austempered structures on fracture characteristics of C/V graphite cast iron has studied. The tensile strength and hardness reached the maximum value of 971.4MPa and HB302 at the austempering temperature of $250^{\circ}C$, respectively. As the austempering temperature increased, the amount of retained austenite increased from 18% to 22, 29%, while $K_{IC}$ values ranged from the value of $65MPa{\cdot}m^{12} to 70MPa{\cdot}m^{1/2}, 66MPa{\cdot}m^{1/2}. This fact that $K_{IC}$ value was not sensitive to the increase of the amount of the retained austenite was that $K_{IC}$ was dependent on the matrix structure in lower bainitic matrix, while dependent on the notch effect from C/V graphite shape in upper bainitic matrix. Fractured surfaces showed a ductile fracture pattern at $300^{\circ}C$. Very large coalescence by C/V graphite and relatively small voids by spheroidal graphite were observed.

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A STUDY ON FLEXURE STRENGTH OF THE SOLDER JOINTS FORMED USING VARIOUS SOLDERING TECHNIQUES FOR CERAMO-METAL ALLOYS (도재소부전장관용 합금의 납착방법에 따른 납착부 굽힘강도에 대한 연구)

  • Kim, Jin-Yeoul;Chun, Young-Charn
    • The Journal of Korean Academy of Prosthodontics
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    • v.31 no.2
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    • pp.191-205
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    • 1993
  • In order to compare the strength of soldered joints relative to the various sol dering method, soldering processes were performed using Palladium based ceramo-metal alloy(Bond-on 4)and Nickel-cromium alloy(Vera Bond). The obtained data include difference in strength between presoldering and postsoldering The data also contain difference among postsoldered groups for 3 difference soldering methods(torch, infrared. Oven) The following results were obtained : 1. For postsoldering with Pd alloy, the oven-using group showed the highest strength while the difference in strength between the torch-using group and the infrared machine group was negligible. 2. For Pd alloy with the torch method, postsoldering resulted in the higher strength than presoldering. 3. There was a negligible difference in strength between presoldering and postsoldering when Ni-Cr alloy with torch method is used. 4. Through microscopic study of the fractured surfaces, the torch-using group showed more porosity than both the oven-using and the infrared machine groups. 5. In terms of fracturing patterns, the oven-using group showed adhesive failure while both the torch and the infrared machine groups showed cohesive failure and cohesive-adhesive failure.

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Glass Forming Ability and Mechanical Properties of (Fe79C11B8Si2)100-XCrX (X = 0-8) Amorphous Ribbons ((Fe79C11B8Si2)100-XCrX (X = 0-8) 조성 비정질 리본의 크롬 함량에 따른 비정질 형성능, 기계적 특성 평가)

  • Moon, Jae-Won;Park, Ji-Sung;Yi, Seong-Hoon
    • Journal of Korea Foundry Society
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    • v.36 no.1
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    • pp.18-23
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    • 2016
  • Iron based amorphous ribbons with the nominal compositions of $(Fe_{79}C_{11}B_8Si_2)_{100-X}Cr_X$ (X = 0,2,4,6,8 at%) have been developed as reinforcements that can be applied to the concrete materials. Mechanical properties and glass forming ability of the ribbons can be enhanced by the optimum amounts of Cr additions that can also improve corrosion properties of the ribbons. Vein patterns typical of the fractured surface morphology of amorphous alloys have been observed on the surfaces of ribbons after tensile tests. It is inferred from the EDS analysis results of vein patterns that carbon segregations occur within the narrow shear band regions.

Outcome of Open Reduction Via Retromandibular Approach for Mandibular Subcondyle Fracture (하악골 과두경부 골절에 있어서 후하악부 절개법을 이용한 관혈적 정복술의 유용성)

  • Lee, Hyung Chul;Kang, Dong Hee;Koo, Sang Hwan;Park, Seung Ha
    • Archives of Plastic Surgery
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    • v.32 no.6
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    • pp.739-743
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    • 2005
  • Subcondylar fractures have generally been treated by intermaxillary fixation except in cases where there is an absolute indication for open reduction. The reason behind a less aggressive surgical approach lies on the inherent difficulties in manipulating fragments in such a small area at the risk of damaging facial nerves or vessels such as the internal maxillary artery. However, long-term follow-up studies showed that conservative treatment of subcondylar fractures results in disturbances of occlusal function, deviation of the mandible, internal derangement of the temporomandibular joint, and ankylosis of the joint. We carried out open reduction of dislocated subcondylar fractures in 14 patients from 2000 to 2004 by a retromandibular approach. After the reduction of fractured bone, two H-shaped miniplates with 6 holes were fixed with screws at the anterior and posterior surfaces of the subcondyle. The retromandibular approach allowed good access and easy manipulation of the subcondyle. Immediate relief from malocclusion and correction of mandibular midline shifting were observed in all patients. Late temporomandibular dysfunction and ankylosis were not observed. Open reduction with plate osteosynthesis made it possible to avoid IMF in 7 of the 14 patients. The present study shows that open reduction through this retromandibular approach can produce good outcome in adult patients with subcondylar fracture.

Solid-liquid mixture flow characteristics in an inclined slim hole annulus (Slim hole 경사 환형관내 고-액 혼합유동 특성에 관한 연구)

  • Suh, Byung-Taek;Han, Sang-Mok;Woo, Nam-Sub;Kim, Young-Ju;Hwang, Young-Kyu
    • Proceedings of the SAREK Conference
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    • 2008.06a
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    • pp.1315-1320
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    • 2008
  • An experimental study was carried out to study the solid-liquid mixture upward flow in a vertical and inclined annulus with rotating inner cylinder. Lift forces acting on a fluidized particle plays a central role in many importance applications, such as the removal of drill cuttings in horizontal drill holes, sand transport in fractured reservoirs, sediment transport and cleaning of particles from surfaces, etc. Field measurements have revealed that the pressure drop over a borehole during drilling of a slim oil well or a well with a long reach can depend significantly on the rotation speed of the drill pipe. An accurate prediction of the annular frictional pressure drop is therefore important for conditions where the annular clearance is small. Effect of annulus inclination and drill pipe rotation on the carrying capacity of drilling fluid, particle rising velocity, and pressure drop in the slim hole annulus have been measured for fully developed flows of water and of aqueous solutions.

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