• 한국세라믹학회지
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• 제44권4호
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• pp.208-213
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• 2007

Alumina/silver ($Al_2O_3/Ag$) nanocomposites with Ag content up to 9 vol% were prepared from nanopowder by soaking method using ${\gamma}-Al_2O_3$ of needle type and spark plasma sintering (SPS). The mechanical properties of specimens were investigated three-point flexural strength and toughness as a function of the Ag contents. The maximum flexural strength of the alumina/silver nanocomposite was 850 MPa for the 1 vol% composite, and also higher than monolith alumina as about 800 MPa at 3, 5, and 7 vol% Ag contents. Fracture toughness by single edged V-notch beam (SEVNB) was $4.05MPa{\cdot}m^{1/2}$ for the 3 vol% composite and maintained about $4.00MPa{\cdot}m^{1/2}$ at 5, and 7 vol% Ag content. Microstructure of fracture surface for each fracture specimens was observed. Due to the inhibition effect of alumina grain growth, the average grain size of nanocomposites depends on the content of Ag nano particles. The fracture morphology of nanocomposite with dislocation (sub-grain boundary) by silver nano-particles of second phases in the alumina matrix also showed transgranular fracture-mode compare with intergranular of monolith alumina. Thermal conductivity of specimens at room temperature was about 40 W/mK for the 1 vol% Ag content.

• 마이크로전자및패키징학회지
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• 제18권4호
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• pp.63-70
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• 2011

Anorthite forming glass frits in amounts up to 25 vol% of the silver powder were added to improve the adhesion between the conductor pattern formed by thick film photoimageable process and the low temperature co-fired ceramics (LTCC) substrate. The sheet resistance of the conductor pattern was raised from 0.13 ${\Omega}/{\square}$ to 2.25 ${\Omega}/{\square}$ as the volume percentage of glass frit increased up to 25 vol%. The adhesion strength was improved with this glass frit increase, but it decreased when the glass content exceeded 20 vol% which are possibly attributed to the liquid pool effect and the reduced fracture toughness in the interface between conductor and LTCC layer. The shrinkage of the width of the conductor pattern decreased with the addition of glass contents.

• 한국세라믹학회지
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• 제25권6호
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• pp.601-608
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• 1988

The effect of SiO2 addition on sintering characteristics of 8 mole percent yttria-stabilized zirconia ceramics is investigated. As the addition of SiO2 is increased, sinterbility, microstructure, and Vickers hardness of the zirconia ceramic increased but fracture toughness and electrical conductivity are decreased. It is considered that the electrical conductivity decrease with the increase of SiO2 is due to the decrease of defect concentration of ionized oxygen. From the complex impedance measurement, it is shown that the influence of SiO2 is more dominant at the resistivity of bulk region than of grain boundary region.

• 한국지하수토양환경학회지:지하수토양환경
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• 제7권3호
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• pp.33-44
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• 2002

도수로터널 주변 지역의 대수층에 대한 유동성 단열을 규명하기 위하여 야외시험이 실시되었다. 단열들에 대한 정보를 얻기 위하여 지표 지질조사 지질구조조사 및 초음파주사검층을 실시하였다. 지표에서의 단열발달은 퇴적암의 층리면과 층리절리 및 화강암류의 판상절리와 같은 저각의 경사를 가지는 부분과 75$^{\circ}$ 이상의 고각의 경사를 가지는 부분의 두 개의 뚜렷한 단열군으로 형성되어 있다. 층리절리와 판상절리의 평균 주향과 경사는 각각 N70-80$^{\circ}$W.25$^{\circ}$SW, N35$^{\circ}$W.12$^{\circ}$NE이다. 고각의 절리들은 퇴적암 지역에서는 N80$^{\circ}$W.70-85$^{\circ}$SW와 N$10^{\circ}$E.85$^{\circ}$SE 두 방향의 단열조가 우세하며, 화산암 및 화강암 지역은 N40-50$^{\circ}$.E 85$^{\circ}$SE/85$^{\circ}$NE, N70$^{\circ}$E.80$^{\circ}$SE, 그리고 N70-75$^{\circ}$W.80$^{\circ}$SW 방향의 단열조가 우세하게 발달한다. 초음파주사검층에 의하여 얻어진 시추공내의 단열들은 N60-80$^{\circ}$W.20-45$^{\circ}$SW, N10-35$^{\circ}$E.64-83$^{\circ}$SE, N40-65$^{\circ}$E.60-85$^{\circ}$SE, N70$^{\circ}$E.80$^{\circ}$SE, N60-80$^{\circ}$W.45-85SE/SW의 단열군들이 우세하다. 공내 수리전도도의 수직적인 분포를 파악하기 위하여 정압주입시험을 실시하였다. 계산된 수리전도도는 3.363E-10 m/sec 에서 2.731E-6 m/sec의 범위로서 최대값과 최소값은 4차수(four order)의 차이를 보였다. 단열대의 분포 특성을 파악하기 위하여 지구물리검층을 실시하였고, 각 시험에 의해 획득된 결과들과의 비교를 통하여 유동성이 높은 단열들이 규명되었다. 온도검층은 유동성 단열과 일반적인 단열들을 구별하는 좋은 지시자로 나타났다. 그 결과, N70-80$^{\circ}$W.60-85$^{\circ}$NE/SW, N75-80$^{\circ}$W.25-30$^{\circ}$SW, N50-64$^{\circ}$W.60-85$^{\circ}$NE, N35-45$^{\circ}$E.65-75$^{\circ}$SE, 그리고 N65-72$^{\circ}$E.80$^{\circ}$SE/60$^{\circ}$NW의 단열들이 연구지역의 지하수 흐름을 지배하는 뚜렷한 유동성 단열로 규명되었다.

• 한국지하수토양환경학회:학술대회논문집
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• 한국지하수토양환경학회 2001년도 총회 및 춘계학술발표회
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• pp.93-97
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• 2001

시추공의 구간별 수리전도를 추정하는 방법으로는 수압시험(packer test)이 많이 이용되는데 최근에는 유속측정기(flowmeter)를 이용한 시추공 검층법이 개발되어 활발한 연구가 진행 중이다. 본 연구에서는 열원(heat-pulse) 공급 방식의 유속측정기를 이용하여 공주대학 교내에 설치된 시추공에서 자연 유속(ambient flow) 및 양수 유발 유속(pump-induced flow)을 측정하였으며, 자료를 분석하여 수리전도도의 수직적인 분포를 산정하였다. 분석 결과는 수압시험에 의해 산정된 수리전도도의 분포와 잘 일치하였으며, BIPS에 의해 촬영된 시추공 영상 자료와 비교함으로써 지하수 유동과 관련된 투수성 단열(conductive fracture) 들의 수직적인 위치를 정확하게 파악할 수 있었다. 분석 결과는 암반 대수층 내에 발달된 단열망(fracture network)에 대한 3차원적인 정보를 제공할 수 있으며, 이는 효과적인 지하수 모니터링, 모델링, 및 정화 설계(remedial design)에 필요한 기초 자료로 활용될 수 있을 것으로 기대된다.

• 마이크로전자및패키징학회지
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• 제24권1호
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• pp.35-43
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• 2017

The three-dimensional integrated circuit (3D-IC) is a general trend for the miniaturized and high-performance electronic devices. The through-silicon-via (TSV) is the advanced interconnection method to achieve 3D integration, which uses vertical metal via through silicon substrate. However, the TSV based 3D-IC undergoes severe thermo-mechanical stress due to the CTE (coefficient of thermal expansion) mismatch between via and silicon. The thermo-mechanical stress induces mechanical failure on silicon and silicon-via interface, which reduces the device reliability. In this paper, the thermo-mechanical reliability of TSV based 3D-IC is reviewed in terms of mechanical fracture, heat conduction, and material characteristic. Furthermore, the state of the art via-level and package-level design techniques are introduced to improve the reliability of TSV based 3D-IC.

• 한국세라믹학회지
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• 제56권1호
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• pp.77-83
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• 2019

MgO-C refractories are used in basic furnaces and steel ladles due to their many desirable properties, such as excellent thermal shock resistance via low thermal expansion, and high thermal conductivity. However, the mechanical and thermal properties of the refractory continuously deteriorate by spalling phenomena and pore generation due to the oxidation of graphite, used as a carbon source, indicating that the characteristics and performance of MgO-C refractories need to be improved by using a new material or composition. In this study, the use of a Hertzian indentation test as a method for determining the damage and fracture behavior of an MgO-C refractory is described. The results highlight that Hertzain indentation tests can be one of the important evaluation tools for quasi-plastic damage accumulation of MgO-C refractories during falling process of scrap metal.

• 열처리공학회지
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• 제36권4호
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• pp.206-214
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• 2023

Tungsten carbide has many industrial applications due to its high electrical and thermal conductivity, high melting temperature, high hardness and good chemical stability. Because tungsten carbide is difficult to sinter, it is sintered with nickel or cobalt as a binder and is currently used in nozzles, cutting tools, and molds. Alumina is reported to be a viable binder for tungsten carbide due to its higher oxidation resistance and lower cost than nickel and cobalt. The ultrafine tungsten carbide-graphene-alumina composites were rapidly sintered in a high frequency induction heating active sintering unit. The microstructure and mechanical properties (fracture toughness and hardness) of the composites were investigated and analyzed by Vickers hardness tester and electron microscope. Since the high-frequency induction heating sintering method enables high-speed sintering, ultrafine composites can be prepared by preventing grain growth. In the tungsten carbide-graphene-alumina composites, the grain size of tungsten carbide increased with the amount of alumina participation. The hardness and fracture toughness of the tungsten carbide-5% graphene- x% alumina (x = 0, 5, 10,15) composites were 5.1, 8.6, 8.6, and 8.4 MPa-m^1/2 and 2384, 2168, 2165, and 2102 kg/mm², respectively. The fracture toughness increased without a significant decrease in hardness. Sinterability was improved by adding alumina to tungsten carbide-graphene.

• 한국지하수토양환경학회:학술대회논문집
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• 한국지하수토양환경학회 2006년도 총회 및 춘계학술발표회
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• pp.92-96
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• 2006

Borehole geophysical techniques were adopted for characterizing aquifer properties of crystalline rock formation in Bongmyong borehole test site, Kangwon National University. Specific fractures and/or fracture zones accompanying groundwater flow were delineated well by high resolution flowmeter and dilution measurements, and could be confirmed fromconventional well log methods. These geophysical techniques have been proved to be the most effective in aquifer characterization in crystalline rock formation.

• 한국세라믹학회지
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• 제44권7호
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• pp.343-348
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• 2007

Alumina/silver nanocomposites were fabricated using a soaking method through a sol-gel route to construct an intra-type nanostructure. The pulse electric-current sintering (PECS) technique was used to sinter the nanocomposites. Several specimens were annealed after sintering. The microstructure, mechanical properties, critical frontal process zone (FPZ) size, and thermo-mechanical properties of the nanocomposites were estimated. The relative densities of the specimens sintered at 1350 and $1450^{\circ}C$ were 95% and 99%, respectively. The maximum value of the three-point bending strength was found to be 780 MPa for the $2{\times}2{\times}10 mm$ specimen sintered at $1350^{\circ}C$. The fracture toughness of the specimen sintered at $1350^{\circ}C$ was measured to be $3.60 MPa{\cdot}m^{1/2}$ using the single-edge V-notched beam (SEVNB) technique. The fracture mode of the nanocomposites was transgranular, in contrast to the intergranular mode of monolithic alumina. The fracture morphology suggested that dislocations were generated around the silver nanoparticles dispersed within the alumina matrix. The specimens sintered at $1350^{\circ}C$ were annealed at $800^{\circ}C$ for 5 min, following which the maximum fracture strength became 810 MPa and the fracture toughness improved to $4.21 MPam^{1/2}$. The critical FPZ size was the largest for the specimen annealed at $800^{\circ}C$ for 5 min. Thermal conductivity of the alumina/silver nanocomposites sintered at $1350^{\circ}C$ was 38 W/mK at room temperature, which was higher than the value obtained with the law of mixture.