• Proceedings of the Korean Magnestics Society Conference
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• 2000.09a
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• pp.433-440
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• 2000

Barium ferrite particles were synthesized from Ba(NO$_3$)$_2$, Fe(NO$_3$)$_3$ and KOH mixed solutions using hydrothermal crystallization in supercritical water. The experimental apparatus for production of barium ferrite is a flow-type apparatus. Fine barium ferrite particles were produced because supercritical water causes the metal hydroxides to be rapidly dehydrated before significant growth takes place. The effects of Fe/Ba ratio and reaction time on the formation, particle size, and magnetic properties of barium ferrite were studied. When Fe/Ba ratio were varied from 0.5 to 12, single-phase barium ferrite powder was only produced in the range of 0.5〈Fe/Ba〈2. Also, with elevating reaction time, the BaO.6Fe$_2$O$_3$ particle size grew smaller. Especially, uniform barium hexaferrite particles of size 100-200nm were obtained at 80sec. In this study, therefore, single-phase barium ferrite particles are highly stable and can be produced continuously in a reaction time of less then 2min.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2017.11a
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• pp.155-156
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• 2017

Borosilicate glass was incorporated to improve the neutron shielding capability of concrete. Boron is a typical neutron shielding material, and it is contained in borosilicate glass. However, borosilicate glass causes alkali-silica reaction, which damages the concrete. Therefore, studied to reduce the expansion due to alkali-silica reaction and to improve the neuton shielding capability. The measurement of the expansion due to the alkali-silica reaction was based on ASTM C 1260. Experimental results show that the expansion due to alkali-silica reaction is reduced when borosilicate glass powder incorporated. In addition, the neutron shielding capability was significantly improved when the fine aggregate replaced with borosilicate glass.

• Journal of the Korean Ceramic Society
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• v.33 no.7
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• pp.779-784
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• 1996

The spinel/cubic stabilized zirconia composites were fabricated via, The reaction sintering of monoclinic zirco-nia(baddeleyite) added with MgAl powder. During heating Mg and Al were oxidizedfirst and subsequently the oxides formed spinel (MgAl2O4) and finally remained MgO stabilized the zirconia, Because the oxides formed during the oxidation process would have very fine grain size (order of submicron) mainly due to the effects of attrition milling the reaction sintering was more effective in densification and improvement of strength and fracture toughness than conventional sintering with direct addition of MgO. The sintering behavior phase transformation during firing and mechanical properties of sintered body were investigated with emphasis on the relations between spinel formation due to MgAl addition and sintering and mechanical properties.

• Journal of the Korean Ceramic Society
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• v.27 no.5
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• pp.613-618
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• 1990

The pure and 6mol% MgO-doped ZrO2 powders were prepared by hot petroleum drying method. The power characterization of homogeneous fine powder was indentified by the method of thermal analysis, BET and electron microscope. The transformation, content of t-ZrO2, crystallite size and apparent strain were measured by X-ray diffraction technique. The prepared powders were transformed in order of amorphouslongrightarrowmetastable cubic ZrO2longrightarrowmetastable tetragonal ZrO2longrightarrowstable monoclinic ZrO2 by a adequate heat treatment. The stabilization of metastable phase can be discussed in terms of energetial concept ; the difference of surface energy and internal strain in particle.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2001.11a
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• pp.577-580
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• 2001

Very fine cobalt oxide ambigel powder were prepared using a unique solution chemistry associated with the sol-gel process. The mesoporous structure of the initial gel is maintained by removing fluid under conditions where the capillary forces that result extraction are either low or no existent, are either low or nonexistent. Controling both the pore and solid architecture on the nanoscale offers a strategy for the design of supercapacitor. But $CoO_{x}$ have the low voltage, so we experiment using CO/PVA composite electrode.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1997.11a
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• pp.80-84
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• 1997

In this experiment, A1$_2$O$_3$ thick films were prepared by electrophoretic method using A1$_2$O$_3$ fine Powder of which composition were FA-5-500 and FA-5-900. The growth behavior of A1$_2$O$_3$ thick films were characterized as preparation conditions, such as applied voltage, deposition time and adding conditions. As a result, A1$_2$O$_3$ thick films were successfully fabricated by electrophoretic method on molybdnum plate in which etanol and distilled used were used as a solvent. Deposition conditions for good uniformity of the A1$_2$O$_3$ thick films were applied voltage of 60volts, deposition time of 2 seconds, heat treatment at 1$700^{\circ}C$ for 5 minutes.

• Journal of the Korea Institute of Building Construction
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• v.6 no.4 s.22
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• pp.93-98
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• 2006

Admixture materials are used in mixing concrete or mortar to improve quality and performance of the concrete. This study examines the potential use of talc as a substitute for cement, the benefits of recycling waste resources for economical efficiency and quality improvement of concrete. The test was carried out by replacing the plain mix with fine grains of talc at the rate of 10%, 20%, and 30%. Talc was divided into three groups depending on the degree of pulverizing. For wet concrete, porosity, slump, bleeding per unit, and setting time by penetration resistance were measured; similarly, for dry concrete, strength and watertight Property were tested. Test results showed that the amount of bleeding and setting time could be shortened, but the strength and watertight proofing severely deteriorated. However, at the replacement rate of 10%, talc showed equal performance with the plain at all degrees of pulverization, which suggests its potential use as admixture material.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.11a
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• pp.263-266
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• 2003

The fine $YBa_2Cu_3O_x$ powder ($0.2{\sim}1.0\;{\mu}m$) is produced by sol-gel method, and electrophoresis deposition is used for the preparation of $YBa_2Cu_3O_x$ thick films which are deposited on Ag wire. The oriented $YBa_2Cu_3O_x$ was tried to be prepared by the zone-melting method under low oxygen partial pressure. The orientation and the phase composition were examined by the X-ray diffraction and the superconductivities were measured by 4 line method. The critical current densities are still quite low, which may be due to unsuitable technical parameters for zone-melting of $YBa_2Cu_3O_x$ thick films. Therefore the heat treatment condition and controlling of low oxygen partial pressure should be improved in the future experiment.

• Nuclear Engineering and Technology
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• v.48 no.2
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• pp.299-303
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• 2016

Prompt gamma activation analysis using a thermal neutron-guided beam at Japan Atomic Energy Agency JRR-3M was applied for the precise determination of Si in silicon nitride ceramic reference materials [Japan Ceramic Reference Material (JCRM) R 003]. In this study, the standard addition method coupled with internal standard was used for the nondestructive determination of Si in the sample. Cadmium was used as internal standard to obtain the linear calibration curves and to compensate for the neutron beam variability. The analytical result of determining Si in JCRM R 003 silicon nitride fine powder ceramic reference materials using prompt gamma activation analysis was in good agreement with that obtained by classical gravimetric analysis. The relative expanded measurement uncertainty (k = 2) associated with the determined value was 2.4%.

• Journal of Welding and Joining
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• v.7 no.3
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• pp.55-62
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• 1989

Variation of the spray droplet velocity with spraying distance and the microstructural characteristics of spray deposits fromed by oxy-fuel thermal spraying with Ni-base alloy powder contained chrome boride for hard facing were examined. Measurements of spray droplet velocity as a function of distance from the nozzle tip were inexcellent agreement with computer simulated predictions. Optimum condition for thermal spray deposits in this experiment was found to be under #10kg/cm^2$ of acceleration gas pressure with 15cm of spraying distance. Fine microstructure and higher microhardness of the initial part of the deposits due to rapid solidification were found to be able to maintained in a thickness up to 0.4mm, and this initial microstructure and properties could be maintained throughout the thickness of a thick spray deposits by performing the multipass spraying with 0.4mm thickness of each pass.