• Title/Summary/Keyword: Fine powder

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Preparation of Fine Co Powder from Co(OH)2 Slurry by Hydrothermal Reduction with Hydrogen

  • Kening Yu;Kim, Dong J.;Hun S. Chung
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06b
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    • pp.87-107
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    • 1996
  • The fine Co powder with an average particle sie of less than 1$\mu\textrm{m}$ was prepared by hydrothermal reduction with hydrogen from Co(OH)2 slurry obtained by mixing the solutons of CoSO4$.$7H2O and NaOH. A method to control pH of the end solution around neutrality was proposed. The reduction rate was found to be a function of pH, temperature, hydrogen pressure and the amount of catalyst.

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The Effect of Al Powder as an Additive on the Sintering of $Al2_O_3$ (I. In air, $1350~1550^{\cire}C$) (첨가된 알루미늄 분말의 산화가 알루미나 소결에 미치는 영향(I. 공기중, $1350~1550^{\cire}C$에서))

  • 박정현;안주삼;김해두
    • Journal of the Korean Ceramic Society
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    • v.20 no.1
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    • pp.49-54
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    • 1983
  • The main object of this study is to investigate the effect of Al powder as an additive on the sintering of calcined alumina comparing with that of calcined alumina alone. The degree of Al oxidation is calculated by measuring the weight increase during the firing Water absorption bulk density and compressive strength of the $Al_2O_3+Al$ system at each temperature are compared with those of $Al_2O_4$ alone. The $Al_2O_3+Al$ system shows better physical propeties than Al2O3 alone and it seems by the SEM observation that the fine oxidized Al particles(fine $Al_2O_3$ particles submicron unit) fill the interstices of the original $Al_2O_3$ par-ticles and thus result in the well-close-packed arrangement of the particles.

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Influence of Mold Temperature, Lubricant and its Additional Quantity on Compressibility in Warm Compaction

  • Ushirozako, Tsutomu;Yamamoto, Masayuki
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.195-196
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    • 2006
  • In recent years, demands for sintered ferrous material with higher strength are increasing. To satisfy these demands, studies and commercial use of the die wall lubrication method, the warm compaction method and the combination of both methods are widely carried out to achieve high density. The die wall lubrication warm compaction method makes it possible to achieve high density by reducing internal lubricant through die wall lubrication, although the method involves several issues such as prolonged cycle time due to lubricant spraying and difficulty in spraying lubricant in the case of compacting with complicated geometry. Meanwhile, the conventional warm compaction method requiring no die wall lubricant application cannot achieve such a high density as in the case of die wall lubrication warm compaction due to higher volume of internal lubricant. However, this report discloses our study result in which the possibility of improving density is exhibited by using a lubricant type with superior dynamic ejection property that can reduce volume of lubricant additive.

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The Evaluation of Thermal Properties for W-Cu Composite Sintered from Mechanically Alloyed Powders (기계적 합금화한 W-Cu 복합분말 소결체의 열물성 평가)

  • 오낭렴;김대건;석명진;김영환;김영도;문인형
    • Journal of Powder Materials
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    • v.7 no.3
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    • pp.154-160
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    • 2000
  • In order to enhance sinterability of W-Cu composites used for heat sink materials, mechanical alloying process where both homogeneous mixing of component powders and fine dispersion of minor phase can be easily attained was employed. Nanostructured W-Cu powders prepared by mechanical alloying showed W grain size ranged of 20-50 nm and were able to be efficiently sintered owing to the fine particle size as well as uniform distribution of Cu phase. The thermal properties such as electrical resistivity, coefficient of thermal expansion and thermal conductivity were evaluated as functions of temperature and Cu content. It was found that the coefficient of thermal expansion could be controlled by changing Cu content. The measured electrical resistivities and thermal diffusivities were also varied with Cu content. The thermal conductivities calculated from the values of resistivities and diffusivities showed similar tendency as a function of temperatures. However, this is in contradiction with thermal conductivities of pure W and Cu which decrease with increasing temperature.

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Development and Application of Metal Nanoparticles for Printed Electronics: Application to Metal Ink in Ink-Jet Technology (Printed Electronics용 금속 나노입자 개발 및 응용: 잉크젯용 금속잉크에의 적용)

  • Lee, Kun-Jae;Choa, Yong-Ho
    • Journal of Powder Materials
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    • v.15 no.2
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    • pp.81-86
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    • 2008
  • 최근프린팅기술은 전자부품소재 산업의 대형화 및 저가격화의 해법으로 기대되고 있다. 특히 전자부품소재 프린팅 기술 중 잉크젯공정은 최신 디스플레이용 전극소재, PCB, FPCB 및 기타 소재공정에 이용하려는 움직임이 활발히 진행되고 있다. 그러나 잉크젯 기술은 재료의존도 비중이 높은 기술로서 소재(금속잉크)의 개발이 최우선시 되어야한다. 전자부품소재용 금속잉크에 사용되는 금속 나노입자는 우수한 전기전도성과 산업적응용이 가능해야 한다. 따라서 최근 연구되고 있는 금속 나노입자의 연구결과 중 전자잉크에 적용 가능한 연구결과와 응용분야에 대하여 서술하였다.

A Study on the Alkali Application of Recycled Aggregates as a Solution to Reduced Intial Intensity of Blast Furnace Slags (고로슬래그의 초기강도 저하 해결방안으로써 순환 잔골재의 알칼리 활용가치에 대한 연구)

  • Kwak, Yong-Jin;Zhao, Yang;Jung, sang-woon;Heo, Young-sun;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2013.05a
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    • pp.85-86
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    • 2013
  • Weakness of fine powder of blast furnace slags includes the decrease of initial intensity and delay of setting time. To solve this problem, there has been research on the alkali activation to induce hardening using alkaline chemical. However, the use of chemicals is dangerous and not cost effective, which can be solved by using recycled aggregates, one of construction wastes. The role of alkali activator can be substituted by alkali of non-hydrated cement included in recycled aggregates. In this study, the alkaline value of recycled aggregates will be evaluated through the comparison of molarity of sodium hydroxide (NaOH).

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Development of a High-Volume Simultaneous Sampler for Fine and Coarse Particles using Virtual Impactor and Cyclone Techniques

  • Okuda, Tomoaki;Shishido, Daiki;Terui, Yoshihiro;Fujioka, Kentaro;Isobe, Ryoma;Iwaki, Yusuke;Funato, Koji;Inoue, Kozo
    • Asian Journal of Atmospheric Environment
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    • v.12 no.1
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    • pp.78-86
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    • 2018
  • Filter-based sampling techniques are the conventional way to collect particulate matter, but particles collected and entangled in the filter fibers are difficult to be removed and thus not suited for the following cell- and animal-based exposure experiments. Collecting aerosol particles in powder form using a cyclone instead of a filter would be a possible way to solve this problem. We developed a hybrid virtual-impactor/cyclone high-volume fine and coarse particle sampler and assessed its performance. The developed system achieved 50% collection efficiency with components having the following aerodynamic cut-off diameters: virtual impactor, $2.4{\mu}m$; fine-particle cyclone, $0.18-0.30{\mu}m$; and coarse-particle cyclone, $0.7{\mu}m$. The virtual impactor used in our set-up had good $PM_{2.5}$ separation performance, comparable to that reported for a conventional real impactor. The newly developed sampler can collect fine and coarse particles simultaneously, in combination with exposure testing with collected fine- and coarse-particulate matter samples, should help researchers to elucidate the mechanism by which airborne particles result in adverse health effect in detail.

Enhancement of Lowsintering Temperature and Electromagnetic Properties of (NiCuZn)-Ferrites for Multilayer Chip Inductor by Using Ultra-fine Powders (초미세 분말합성에 의한 칩인덕터용 (NiCuZn)-Ferrites의 저온소결 및 전자기적 특성 향상)

  • 허은광;강영조;김정식
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.4
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    • pp.47-53
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    • 2002
  • In this study, two different (NiCuZn)-ferrite which were fabricated by using ultra-fine powders synthesized by the wet processing and conventionally commercialized powder, were investigated and compared each other in terms of the low temperature sintering and electromagnetic properties. Composition of x and w in $(Ni_{0.4-x}Cu_xZn_{0.6})_{1+w}(Fe_2O_4)_{1-w}$ were controlled as 0.2 and 0.03, respectively. The sintering temperature were $900^{\circ}C$ for ultra-fine powders by way of initial heat treatment and $1150^{\circ}C$ for commercialized powders. The (NiCuZn)-ferrite by ultra-fine powders showed love. sintering temperature than that of commercialized powders by over $200^{\circ}C$, and excellent electromagnetic properties such as the quality factor which is a important factor in the multi-layered chip inductor. In addition, characteristics of B-H hysteresis, crystallinity, microstructure and powder morphology were analyzed by a vibrating sample method(VSM), x-ray diffractometer(XRD), transmission electron microscope (TEM) and scanning electron microscope(SEM).

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Synthesis of Oxide Ceramic Powders by Polymerized Organic-Inorganic Complex Route

  • Lee, Sang-Jin;Lee, Chung-Hyo;Waltraud M. Kriven
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 2000.06a
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    • pp.151-163
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    • 2000
  • A polymerized organic-inorganic complexation route is introduced for the synthesis of oxide ceramic powders. Polyvinyl alcohol was used as the organic carrier for precursor ceramic gel. Porous and soft powders, which have a high specific surface area, were obtained after calcinating the aerated precursors. The PVA content and its degree of polymerization had a significant influence on the homogeneity of the final powder. In particular, attrition milling process with the porous powder resulted in ultra-fine particles. In the case of the preparation of cordierite powder, nano-size powder, which has a high specific surface area of 181 ㎡/g, was obtained by the milling process. The complexation route was also applied to the synthesis of unstable phase in room temperature like beta-cristobalite, high temperature form of silica.

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Optimum Mixture Proportion of Self-Compacting Concrete Considering Packing Factor of Aggregate and Fine Aggregate Volume Ratio (골재 채움율과 잔골재 용적비를 고려한 자기충전형 콘크리트의 최적배합)

  • 최연왕;정문영;정지승;문대중;안성일
    • Proceedings of the Korea Concrete Institute Conference
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    • 2002.10a
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    • pp.549-554
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    • 2002
  • In Powder System, SCC demands high dosage of superplasticizer and a lage amout of powder for suitable fluidity and viscosity. Okamura's method of most representative mixing design method in SCC of Powder-System is unfavorable economically because of using a large amount of powder. In addition, many ready-mixed concrete plants do not use his mix design method and procedure due to complexity for practical application. Therefore, Nan Su proposed more simple mix design method than Okamura's. It had an advantage in simplicity in practical application and required a smaller amount of powders compared with Okamura's method. This paper proposed an optimal mixture proportion of SCC with consideration of Nan Su's method. The new and modified mix design method required a smaller amount of powder than that of Nan Su's. To check the properties of SCC, considered with the requirements specified by the Japanese Society of Civil Engineering.(JSCE)

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