• 한국재료학회지
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• 제31권2호
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• pp.61-67
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• 2021

Fabrication of a ferromagnetic composite powder for the magnesium and BaFe12O19 system by mechanical alloying (MA) is investigated at room temperature. Mixtures of Mg and BaFe12O19 powders with a weight ratio of Mg:BaFe12O19 = 4:1, 3:2, 2:3 and 1:4 are used. Optimal MA conditions to obtain a ferromagnetic composite with fine microstructure are investigated by X-ray diffraction, differential scanning calorimetry (DSC) and vibrating sample magnetometer (VSM) measurement. It is found that Mg-BaFe12O19 composite powders in which BaFe12O19 is dispersed in Mg matrix are successfully produced by MA of BaFe12O19 with Mg for 80 min. for all compositions. Magnetization of Mg-BaFe12O19 composite powders gradually increases with increasing the amounts of BaFe12O19, whereas coercive force of MA powders gradually decreases due to the refinement of BaFe12O19 powders with MA time for all compositions. However, it can be seen that the coercivity of Mg-BaFe12O19 MA composite powders with a weight ratio of Mg:BaFe12O19=4:1 and 3:2 for MA 80 min. are still high, with values of 1260 Oe and 1320 Oe compared to that of Mg:BaFe12O19=1:4. This clearly suggests that the refinement of BaFe12O19 powders during MA process for Mg:BaFe12O19=4:1 and 3:2 tends to be suppressed due to ductile Mg powders.

• 대한금속재료학회지
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• 제47권8호
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• pp.488-493
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• 2009

Direct syntheses of bulk $Ti_3Al$ via electro-discharge-sintering (EDS) of a stoichiometric elemental powder mixture were investigated. A capacitor bank of $450{\mu}F$ was charged with three input energies, 0.5, 1.0, and 1.5 kJ. The charged capacitor bank was then instantaneously discharged through 0.3 g of a Ti-25.0 at.%Al powder mixture for consolidation. Complete phase transformation occurred in less than $200{\mu}sec$ by the discharge and a bulk $Ti_3Al$ compact was obtained. Compared with consolidated samples fabricated by conventional methods such as high vacuum sintering and casting, the electro-discharge-sintered $Ti_3Al$ compact shows a very fine microstructure with a hardness value of 425 Hv. Electro-discharge-sintering under a $N_2$ atmosphere successfully modified the surface Ti oxide of the $Ti_3Al$ compact into Ti nitride, which concurred with the synthesis and consolidation of $Ti_3Al$. Complete conversion yielding a single phase $Ti_3Al$ is primarily dominated by the fast solid state diffusion reaction.

• 방송공학회논문지
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• 제27권3호
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• pp.369-377
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• 2022

최근 딥러닝 기반의 얼굴 합성 연구는 전체적인 스타일이나 헤어, 안경, 화장과 같은 요소를 포함하는 매우 사실적인 얼굴을 생성하는 결과를 보인다. 그러나 피부의 미세 구조와 같은 매우 세부적인 수준의 얼굴은 생성하지 못한다. 본 논문에서는 이러한 한계점을 극복하고자 한 장의 얼굴 라벨 영상으로부터 피부 미세 요소의 종류와 강도 조절을 통해 더욱 사실적인 얼굴 영상을 합성하는 기법을 제안한다. 제안하는 기법은 Image-to-Image Translation 방법인 Pix2PixHD를 이용해 얼굴 영역과 피부 요소인 주름, 모공, 홍조가 표시된 라벨 영상을 변환하여 미세 요소가 추가된 얼굴 영상을 생성한다. 피부 요소 영역을 조절한 라벨 영상을 다양하게 생성함으로써 이에 대응하는 미세한 피부 요소가 반영된 다양한 사실적인 얼굴 영상을 생성할 수 있음을 실험을 통해 보인다.

• Structural Engineering and Mechanics
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• 제78권4호
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• pp.473-484
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• 2021

Similar to other structures, ultimate strength values showing the maximum load that the structure can resist without damaging has great importance on ships. Therefore, increasing the ultimate strength values will be an important benefit for the structure. Low carbon steels used in ships due to their low cost and good weldability. Improving the ultimate strength values without interfering with the chemical composition to prevent of the weldability properties of these steels would be very beneficial for ships. Grain refinement via severe plastic deformation (SPD) is an essential strengthening mechanism without changing the chemical composition of metallic materials. Among SPD methods, equal channel angular pressing (ECAP) is one of the most commonly used one due to its capacity for achieving bulk ultrafine-grained (UFG) materials. When the literature is examined, it is seen that there is no study about ultimate strength calculation in ships after ECAP. Therefore, the mean purpose of this study is to apply ECAP to a shipbuilding low carbon steel to be able to achieve mechanical properties and investigate the alteration of ship hull girder grillage system's ultimate strength via finite element analysis approach. A fine-grained (FG) microstructure with a mean grain size of 6 ㎛ (initial grain size was 25 ㎛) was after ECAP. This microstructural evolution brought about a considerable increase in strength values. Both yield and tensile strength values increased from 280 MPa and 425 MPa to about 420 MPa and 785 MPa, respectively. This improvement in the strength values reflected a finite element method to determine the ultimate strength of ship hull girder grillage system. As a result of calculations, it was reached significantly higher ultimate strength values (237,876 MPa) compared the non-processed situation (192,986 MPa) on ship hull girder grillage system.

• 소성∙가공
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• 제32권5호
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• pp.239-246
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• 2023

To reduce the forming load due to the temperature drop, during the hot forging process, a reheating hot forging process design is required that to repeat heating and forging. However, if the critical strain required for recrystallization is not induced during forging and grain growth becomes dominant due to the reduction in dislocation density due to repeated heating, the mechanical properties may deteriorate. Therefore, in this study, Inconel 706 alloy was applied, and the grain refinement behavior was comparatively analyzed according to the number of reheating times and effective strain during reheating hot forging process. Reheating was carried out with a total compression rate of 40% up to 4 times. The Inconel 706 compression test specimens heated once showed finer grains as the effective strain increased due to the dynamic recrystallization phenomenon. However, as the number of heating increases, grain refinement was observed even in a low effective strain distribution of 0.43 due to static recrystallization during reheating. Moreover, grain growth occurs at a relatively low effective strain of 0.43 when the number of reheating is four or more. Therefore, it was effective to apply an effective strain of 0.43 or more during hot forging to Inconel 706 in order to induce crystallization through grain refinement and improve the properties of forged products. In addition, we could notice that up to three reheating times condition was appropriate to prevent grain growth and maintain fine grain size.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2000년도 춘계학술발표회 초록집
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• pp.1-1
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• 2000

The results of the modification of metal materials treated by high temperature pulst:d plasma fluxes (HTlPPF) with a specific power of incident flux changing in the $(3...100)10^5{]\;}W/cm^2$ range and a pulse duration lying from 15 to $50{\;}\mu\textrm{s}$ have been presented. The results of HTPPF action were studied on the stainless steels of 18Cr-l0Ni, 16Cr- 15Ni, 13Cr-2Mo types; on the structural carbon steels of (13...35)Cr, St. 3, St. 20, St. 45 types; on the tool steels of U8, 65G, ShHI5 types, and others; on nickel and high nickel alloy of 20Cr-45Ni type; on zirconium- and vanadium-base alloys and other materials. The microstructure and properties (mechanical, tribological, erosion, and other properties) of modified materials and surface alloying of metals exposed to HTPPF action have been investigated. It was found that the modification of materials by HTPPF resulted in a simultaneous increase of several properties of the treated articles: microhardness of the surface and layers of 40...60 $\mu\textrm{m}$ in depth, tribological characteristics (friction coefficient, wear resistance), mechanical properties ({\sigma_y}, {\;}{\sigma_{0.2}}.{\;}{\sigma_r}) on retention of the initial plasticity ($\delta$), corrosion resistance, radistanation erosion under ion irradiation, and others. The determining factor of the changes observed is the structural-phase modification of the near-surface layers, in particular, the formation of the fine cellular structure in the near-surface layers at a depth of $20{\;}{\mu\textrm{m}}$ with dimension of cells changing in the range from 0.1 to $1., 5{\;}\mu\textrm{m}$, depending on the kind of material, its preliminary treatment, and the parameters of plasma fluxes. The remits obtained have shown the possibility of purposeful surface alloying of metals exposed to HTPPF action over a depth up to 20...45 $\mu\textrm{m}$ and the concentration of alloying element (Ni, Cr, V) up to 20 wt.%. Possible industrial brunches for using the treatment have been also considered, as well as some results on modifying the serial industrial articles by HTPPF.

• Advances in concrete construction
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• 제15권3호
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• pp.161-170
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• 2023

Ultra-high-performance concrete (UHPC) is produced using high amount of cementitious materials, very low water/cementitious materials ratio, fine-sized fillers, and steel fibers. Due to the dense microstructure of UHPC, it possesses very high strength, elasticity, and durability. Besides that, the UHPC exhibits high ductility and fracture toughness due to presence of fibers in its matrix. While the high ductility of UHPC allows it to undergo high strain/deflection before failure, the high fracture toughness of UHPC greatly enhances its capacity to absorb impact energy without allowing the formation of severe cracking or penetration by the impactor. These advantages with UHPC make it a suitable material for construction of the structural members subjected to special loading conditions. In this research work, the UHPC mixtures having three different dosages of steel fibers (2%, 4% and 6% by weight corresponding to 0.67%, 1.33% and 2% by volume) were characterized in terms of their mechanical properties including facture toughness, before using these concrete mixtures for casting the slab specimens, which were tested under high-energy impact loading with the help of a drop-weight impact test setup. The effect of fiber content on the impact energy absorption capacity and central deflection of the slab specimens were investigated and the equations correlating fiber content with the energy absorption capacity and central deflection were obtained with high degrees of fit. Finite element modeling (FEM) was performed to simulate the behavior of the slabs under impact loading. The FEM results were found to be in good agreement with their corresponding experimentally generated results.

• 열처리공학회지
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• 제35권2호
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• pp.74-81
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• 2022

This study aims to mitigate the microstructural heterogeneity arising from the manufacture of magnesium alloy plates using the twin roll casting (TRC) process. Homogenization was introduced through hot rolling and heat treatment, followed by confirmation of observed changes in the microstructure. Following the TRC process, the hot rolled 2mm plate exhibited a dendritic cast structure tilted in the roll rotation direction, while central segregation were developed. This nonuniform structure and central segregation disappeared upon heat treatment, followed by recrystallization to form uniform and fine grains. Abnormal grain growth (AGG) was observed over the course of heat treatment; grains exhibiting AGG occupied up to 75% of the total area after having held the sample at 400℃ for 64 h. The formation of coarse grains was also observed during heat treatment at 340℃ over a relatively long duration, though the maximum grain size was significantly smaller than that corresponding to the heat treatment at 400℃. AGG in the 400℃ heat treatment occurred because of movement of the grain boundary, which had been fixed prior as a result of the grain boundary fixing effect of the precipitation phase. The re-dissolution of the Ca₂Mg₅Zn₅ precipitated phase over the long duration of the high-temperature annealing process caused the surrounding grains to disappear and regrow.

• 한국재료학회지
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• 제33권6호
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• pp.242-250
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• 2023

Titanium, which has excellent strength and toughness characteristics, is increasingly used in the aerospace field. Among the titanium alloys used for body parts, more than 80 % are Ti-6Al-4V alloys with a tensile strength of 931 MPa. The spark plasma sintering (SPS) method is used for solidification molding of powder manufactured by the mechanical milling (MM) method, by sintering at low temperature for a short time. This sintering method avoids coarsening of the fine crystal grains or dispersed particles of the MM powder. To improve the mechanical properties of pure titanium without adding alloying elements, stearic acid was added to pure titanium powder as a process control agent (PCA), and MM treatment was performed. The properties of the MM powder and SPS material produced by solidifying the powder were investigated by hardness measurement, X-ray diffraction, density measurement and structure observation. The processing deformation of the pure titanium powder depends on the amount of stearic acid added and the MM treatment time. TiN was also generated in powder treated by MM 8 h with 0.50 g of added stearic acid, and the hardness of the powder was higher than that of Ti-6Al-4V alloy when treated with MM for 8 h. When the MM-treated powder was solidified in the SPS equipment, TiC was formed by the solid phase reaction. The SPS material prepared as a powder treated with MM 8 h by adding 0.50 g of stearic acid also formed TiN and exhibited the highest hardness of Hv1253.

• 한국전산구조공학회논문집
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• 제37권2호
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• pp.143-149
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• 2024

이미지 분석을 통한 재료의 상 구분은 재료의 미세구조 분석을 위해 필수적이다. 이미지 분석에 주로 사용되는 마이크로-CT 이미지는 대체로 재료를 구성하고 있는 상에 따라 회색조 값이 다르게 나타나므로 이미지의 회색조 값 비교를 통해 상을 구분한다. 순환골재의 고체상은 수화된 시멘트풀과 천연골재로 구분되는데, 시멘트풀과 천연골재는 CT이미지 상에서 유사한 회색조 분포를 보여 상을 구분하기 어렵다. 본 연구에서는 Unet-VGG16 네트워크를 활용하여 순환골재 CT 이미지로부터 천연골재를 분할하는 자동화 방법을 제안하였다. 딥러닝 네트워크를 활용하여 2차원 순환골재 CT 이미지로부터 천연골재 영역을 분할하는 방법과 이를 3차원으로 적층하여 3차원 천연골재 이미지를 얻는 방법을 제시하였다. 선별된 3차원 천연골재 이미지에서 각각의 골재 입자를 분할하기 위해 이미지 필터링을 사용하였다. 골재 영역 분할 성능을 정확도, 정밀도, 재현율 F1 스코어를 통해 검증하였다.