• Title/Summary/Keyword: Filler content

Search Result 394, Processing Time 0.023 seconds

Flame Retardant Properties of Basalt Fiber Reinforced Epoxy Composite with Inorganic Fillers (무기 필러가 첨가된 현무암섬유 강화 에폭시 복합재료의 난연 특성)

  • Mun, So Youn;Lee, Su Yeon;Lim, Hyung Mi
    • Composites Research
    • /
    • v.32 no.6
    • /
    • pp.368-374
    • /
    • 2019
  • Basalt fiber reinforced epoxy composites with inorganic filler (BFRP-F) such as Mg(OH)2 (magnesium hydroxide), Al(OH)3 (aluminum hydroxide), Al2O3 (aluminum oxide) and AlOOH (boehmite) were prepared by hand lay-up and hot pressing. The combustive properties of BFRP-F were improved comparing with basalt fiber reinforced epoxy composite (BFRP) without inorganic filler. At a 30 wt% resin content, the limited oxygen index (LOI) of BFRP is 28.9, which is higher than that of epoxy (21.4), and the LOI of BFRP-F is higher than that of BFRP. The BFRP-F showed the lower peak heat release rate (PHRR), total heat release (THR) and total smoke release rate (TSR) than those of BFRP. We confirmed that the flame retardant properties of the composite were improved by the addition of inorganic filler through the dehydration reaction and oxide film formation.

Effects of Orientation on Properties of Solid-State Extruded Polypropylene/Calcium Carbonate Composites (고상압출로 제조된 폴리프로필렌/탄산칼슘 복합재료의 물성에 미치는 배향의 영향)

  • Lee, Jaechoon;Ha, Chang-Sik
    • Journal of Adhesion and Interface
    • /
    • v.14 no.4
    • /
    • pp.175-182
    • /
    • 2013
  • In this work, we aim to investigate the specific gravity, thermal, and mechanical property changes of solid-state extruded polypropylene (PP)/calcium carbonate composites before and after orientation. For this work, we prepared $PP/CaCO_3$ composites having two different sizes (OM-1 and OM-10). On increasing the filler content, the specific gravity of the composites increases. The specific gravity of the oriented specimen containing filler in PP matrix is found to be much smaller than that of pre-specimen due to the formation of more microvoids. The presence of microvoids in case of oriented composite specimen significantly affected the tensile and flexural properties of the composites. It was observed that the effect of orientation on both flexural strength and modulus is much stronger than the effect of filler contents, regardless of the filler particle size.

Characteristics of Brazed Joint of Sintered Bronze/steel Using Ag-Cu-Zn Type Filler Materials (Ag-Cu-Zn-Cd 계 용가재를 이용한 Bronze 소결체/강의 브레이징 접합부 특성 평가)

  • 이정훈;이창희
    • Journal of Welding and Joining
    • /
    • v.17 no.3
    • /
    • pp.79-89
    • /
    • 1999
  • The study was carried out to examine in more detail metallurgical and mechanical properties of brazed joints of diamond cutting wheel. In this work, shank(mild steel) and sintered bronze-base tips were brazed with three different filler materials(W-40, BAgl and BAg3S). The machine used in this work was a high frequency induction brazing equipment. The joint thickness, porosities and microstructure of brazed joints with brazing variables(brazing temperature, holding time) were evaluated with OLM, SEM, EDS and XRD. Bending(torque) test was also performed to evaluate strength of brazed joints. Further wetting test was performed in a vacuum furnace in order to evaluate the wettability of filler metals on base metals9shank and tips). The brazing temperature had a strong influence on the joint strength and the optimum brazing temperature range was about $700~850^{\circ}C$ for the bronze/steel combinations. The strength of the brazed joint was found to be influenced by the three factors : degree of reaction region, porosity content, joint thickness. The reaction region was formed in the bronze-base tip adjacent to the joint. The reaction region resulted in a bad influence on the strength due to the formation of Cu5.6Sn, CuZn4, $\beta(CuZn)$ and CdAg, etc. Porosities increased as brazing variables(brazing temperature, holding time) increased, and the brazed joints with porosities of less than about 3-5% had an optimum strength for the bronze-base tip.

  • PDF

Physical and Dielectric Properties of Aluminoborosilicate-Based Dielectrics Containing Different Divalent Oxides

  • Shin, Dong-Wook;Saji, Viswanathan S.;Gupta, Ravindra K.;Cho, Yong-Soo
    • Journal of the Korean Ceramic Society
    • /
    • v.44 no.11
    • /
    • pp.613-617
    • /
    • 2007
  • The variations of physical and dielectric properties of low temperature dielectrics based on typical aluminoborosilicate glasses modified with several divalent oxides were investigated. The divalent oxides studied here included CaO, MgO, BaO, SrO and ZnO. All samples containing either 35 wt% or 45 wt% alumina filler were prepared at the same processing condition and then fired at $850^{\circ}C$ for 30 min. The resultant characteristics of fired samples depended on the choice of the divalent ion and the content of the alumina filler. Except for the ZnO modification, all other samples containing 35 wt% filler demonstrated promising densification as they exhibited reasonably high densities of 3.07-3.31 $g/cm^3$ and high shrinkages of 14.0-16.4%. Particularly, the sample containing ZnO was distinguished with large variations compared to the base sample, which can be highlighted with earlier densification and crystallization at unexpectedly low temperatures. The negative effects of the ZnO modification on densification and dielectric properties were thought to be associated with earlier crystallization potentially by influencing effective densification via viscous flow. As an optimum composition, the sample containing only CaO showed the most promising characteristics such as $k{\sim}8.05$ and $tan{\delta}{\sim}0.0018$ when 35 wt% alumina filler was used.

The Effects of a Filler with a High Coefficient of Thermal Expansion on a Sealant for High-Temperature (750 ~ 850℃) SOFCs (고온 (750 ~ 850℃) SOFC용 밀봉재의 특성에 미치는 고열팽창계수를 갖는 필러의 영향)

  • Kim, Bit Nam;Lee, Mi Jai;Hwang, Jong Hee;Lim, Tae Young;Kim, Jin Ho;Hwang, Hae Jin;Kim, Il Won;Chung, Woon Jin
    • Journal of the Korean Ceramic Society
    • /
    • v.50 no.6
    • /
    • pp.470-475
    • /
    • 2013
  • In this study, we report that effects of a filler with a high coefficient of thermal expansion on a sealant for high-temperature ($750{\sim}850^{\circ}C$) SOFC. We designed a $SiO_2-BaO-ZnO-B_2O_3-Al_2O_3$ glass system with a softening temperature higher than $750^{\circ}C$. The properties of the glass system show not only low volumetric shrinking but also low swelling. The glass system did not create a crystal phase during along-term heat treatment. We fabricated a seal gasket with 0, 10, 15, and 20 wt% cristobalite added as filler materials with glass powder. The coefficient of thermal expansion of the seal gasket increased according to cristobalite content. During along-term heat treatment, the leak rate decreased by about 5% after a heat treatment in an oxidizing atmosphere at $750^{\circ}C$ for 2000 h, also decreasing by about 6% after a heat treatment in a reducing atmosphere at $750^{\circ}C$ for 1000 h.

Experimental study of strength of cement solidified peat at ultrahigh moisture content

  • Wang, Rong
    • Geomechanics and Engineering
    • /
    • v.29 no.1
    • /
    • pp.13-23
    • /
    • 2022
  • Peat soil has the characteristics of high moisture content, large void ratio and low shear strength. In this study, unconfined compressive strength and SEM tests are conducted to investigate the effects of ultrahigh moisture content, cement content, organic content and pH value on the strength of solidified peat. As an increase in the cement content and curing period, the failure mode of solidified peat soil changes from ductile failure to brittle failure. The influence of moisture content on the strength of solidified peat is greater than the cement content. As cement content increases from 10% to 30%, strength of solidified peat at a curing age of 28 days increases by 161%~485%. By increasing water content by 100%, decreases of solidified peat at a curing age of 28 days is 42%~79%. Compared with the strength of solidified peat with a pH value of 5.5, the strength of peat with a pH value of 3.5 reduces by 10% ~ 46%, while the strength of peat with a pH value of 7.0 increases by 8% ~ 38%. It is recommended to use filler materials for stabilizing peat soil with moisture content greater than 200%. Because of small size of clay particles, clay added in the cement solidified peat can improve much higher strength that that of sand.

Analysis on the Causes of the Oil Leakage Phenomenon for Complex Waterproofing Methods of Asphalt Mastic and Modified Asphalt Sheet (콘크리트 구조물에 사용되는 개량아스팔트 시트와 아스팔트 매스틱을 복합화한 방수공법의 누유현상 원인 분석)

  • Park, Jin-Sang;Kim, Dong-Bum;Park, Wan-Goo;Oh, Sang-Keun
    • Journal of the Korea Institute of Building Construction
    • /
    • v.18 no.4
    • /
    • pp.337-345
    • /
    • 2018
  • In this study, observations of oil leakage samples taken from the actual site were performed to identify the causes of the oil leakage phenomenon. As a result, the separation of the material components was determined as the main cause of the oil leakage phenomenon based on the changes in the surface conditions, and verification of this was conducted. The evaluation results confirmed that the filler component of the asphalt mastic subsided with the lapse of the settling time, and that the difference ratio of the filler contents of the upper and lower specimens was up to 23.8% after day 28. Based on these results, a hypothesis on the oil leakage mechanism of asphalt mastic was established, and then modeling of the entire process of oil leakage was performed.

Effect of ,Shear Stress on the Viscosity and Electrical Conductivity for the Metal-Filled Composite Materials (금속입자 충전 복합재료의 전단응력에 따른 점도 및 전기 전도도 변화)

  • Lee, Geon-Woong;Choi, Dong-uk;Lee, Sang-Soo;Kim, Jun-Kyung;Park, Min
    • Polymer(Korea)
    • /
    • v.26 no.5
    • /
    • pp.644-652
    • /
    • 2002
  • This study aims at developing the conductive pastes consisting of room temperature vulcanizing (RTV) silicone and metal powder as matrix and filler, respectively. Electrical and rheological properties of metal - filled polymer composites are in general strongly affected by particle shape, side and dispersion state of the filler. In highly filled systems, particles tend to form very complex agglomerated structure which is easily changed when subjected to shear deformation. And the breakdown of agglomerated particles due to shear usually leads to the change of electrical conductivity of the composite. In this study, the effect of particle size and dispersion state of filler on the electrical conductivity of the composites are investigated to offer the selection criteria of conductive filler by measuring the rheological properties of uncured composites and the electrical conductivity of the cured composites. It was found that the type of metal filler systematically affected the rheological property, the susceptibility to shear and the degree of change of electrical conductivity of the composite. The effect of shear on the properties is more conspicuous in the composites containing large particle, indicating that both rheological and electrical properties can be improved by controlling the dispersion state at a given filler content.

Study on the Curing Safety of Thermosetting Resin Mold Meterial (열경화성수지 성형재료의 경화 안전성에 관한 연구)

  • 최일곤;최재욱;김상렬
    • Journal of the Korean Society of Safety
    • /
    • v.12 no.1
    • /
    • pp.71-76
    • /
    • 1997
  • In this paper, it was described results of study on curing safety of molding meterial, about the variation of phenol resin contents, wood flour contents and moisture of wood flour, under the same condition. The experimental results are summarized as follows ; 1) When the curing temperature was high, the curing time was short in the case of 4~8wt% moisture of wood flour, but in the case of more than l2wt% moisture of wood flour, the curing time was long. 2) The curing time for curing temperature was more short when 6wt% moisture of wood flour than 4wt% moisture of wood flour. 3) The more wood flour content and moisture of wood flour content, the longer curing time and the more mineral filler content, the shorter curing time. 4) When the phenol resin content of main matrix increase, the curing time was short.

  • PDF

Effect of Filter and Shrinkage Reducing Agent Influencing on Setting Shrinkage and Strength Properties of MMA-Modified Polymer Paste (충전재와 수축저감제가 MMA개질 폴리머 페이스트의 경화수축 및 강도특성에 미치는 영향)

  • Yeon, Kyu-Seok;Beck, Jong-Man;Jin, Xing-Qi;Lee, Chi-Won
    • Journal of the Korea Concrete Institute
    • /
    • v.18 no.2 s.92
    • /
    • pp.227-232
    • /
    • 2006
  • This article presents the results of experimental study that investigates the effect of filler and shrinkage reducing agent influencing on the strength properties of MMA-modified polymer paste that was produced to develop the surface-repair and coating materials of the concrete structures. Results show that the flexural and compressive strengths of the polymer paste increased 29 and 27%, respectively, when the aluminum hydroxide completely replaced the calcium carbonate as the filler Furthermore, when the shrinkage reducing agent was used 30%, both strengths decreased about 29% comparing to when the agent was not used. As in the cases of flexural and compressive strengths, the adhesive strength increased as the content of aluminum hydroxide as the filler increased, and it decreased as the content of shrinkage reducing agent increased. The adhesive strength with a dry concrete substrate turned out to be $30{\sim}40%$ higher than that with a wet concrete substrate.