• 제목/요약/키워드: Field emission scanning electron microscope (FESEM)

검색결과 66건 처리시간 0.025초

Ga$_2$O$_3$ 나노물질 합성에 관한 연구 (The study on the synthesise of Ga$_2$O$_3$ nanomaterials)

  • 이종수;박광수;노태용;성만영;김상식
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2002년도 하계학술대회 논문집
    • /
    • pp.13-17
    • /
    • 2002
  • Ga$_2$O$_3$ nanomaterials were synthesized from mechanically ground GaN powders with thermal annealing Ga$_2$O$_3$ nanobelts were farmed in a nitrogen atmosphere, while Ga$_2$O$_3$ nanoparticles were formed inan oxygen atmosphere. The structural properties of the Ga$_2$O$_3$ nanomaterials were investigated by X-ray diffractometer (XRD) and high-resolution transmission eleotron microscope (HRTEM). The study of field emission scanning electron microscopy (FESEM) on the microstructures of nanomaterials revealed that the nanobelts are with the range of about 10∼200nm width and 10∼50nm thickness, and that nanoparticles are with the range of about 20∼50nm radius. On the basis of XRD and HRTEM data, we determined that the nanobelts grow toward a direction perpendicular to the (010) lattice plane and that they are enclosed by facets of the (10T) and (101) lattice planes. The formation of the nanobelts may be described by the vapor-solid(VS) mechanism, and the supersaturation device of gaseous phase may play an important role in the formation of Ga$_2$O$_3$ nanomaterials.

  • PDF

LTCC 기판을 이용한 PZT 압력 센서의 제작 및 특성 연구

  • 허원영;황현석;이태용;이경천;송준태
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2010년도 춘계학술대회 논문집
    • /
    • pp.13-13
    • /
    • 2010
  • Piezoelectric sensors are extensively used to measure force because of their high sensitivity and low cost. however, the development of device with reduced size but with improved sensitivity is highly important. Low-temperature co-fired ceramic (LTCC) is one of promising materials for this application than a silicon substrate because it has very good electrical and mechanical properties as well as possibility of making various three dimensional (3D) structures. In this work, piezoelectric pressure sensors based on hybrid LTCC technology were presented. The LTCC diaphragms with thickness of $400\;{\mu}m$ were fabricated by laminating 12 green tapes which consist of alumina and glass particle in an organic binder. The piezoelectric sensing layer consists of PZT thin film deposited by RF magnetron sputtering method on between top and bottom Au electrodes. The PZT films deposited on LTCC diaphragms were successfully grown and were analyzed by using X-ray diffraction method (XRD) and field emission scanning electron microscope (FESEM).

  • PDF

ZnO:Al 투명도전막의 열처리에 따른 전기적 및 광학적 특성 (Electrical and optical properties of ZnO:Al transparent conductive films with thermal treatments)

  • 마대영;박기철
    • 전기전자학회논문지
    • /
    • 제24권2호
    • /
    • pp.435-440
    • /
    • 2020
  • 고주파 마그네트론 스퍼터링으로~500 nm 두께의 ZnO:Al막을 증착하였다. 증착된 ZnO:Al막을 100 ℃, 200 ℃, 300 ℃ 및 400 ℃에서 10시간 동안 열처리하였다. ZnO:Al막의 열처리에 따른 저항률, 캐리어 농도 및 이동도 변화를 측정하였다. XRD, FESEM 결과를 통해 열처리에 따른 ZnO:Al막의 저항률 변화 원인을 조사하였다. ZnO:Al막의 광 투과율을 측정한 후 에너지 밴드 갭, Urbach 에너지 및 굴절률을 도출하였다. ZnO:Al막의 전기적 특성 변화를 광특성과 연관지어 설명하였다.

Performance of concrete modified with SCBA and GGBFS subjected to elevated temperature

  • Palaskar, Satish Muralidhar;Vesmawala, Gaurang R.
    • Advances in materials Research
    • /
    • 제9권3호
    • /
    • pp.203-218
    • /
    • 2020
  • This research paper presents the outcomes in terms of mechanical and microstructural characteristics of binary and ternary concrete when exposed to elevated temperature. Three parameter were taken into account, (a) elevated temperature (i.e., 200, 400, 600 and 800℃) (b) binary concrete with cementitious material sugarcane bagasse ash (SCBA) and ground granulated blast furnace slag (GGBFS) replacement percentage (i.e., 0, 15, 20, 25 and 30%) and (c) ternary concrete with cementitious material SCBA and GGBFS replacement percentage (i.e., 0, 15, 20, 25 and 30%). A total of 285 standard cube specimens (150 mm × 150 mm × 150 mm) containing Ordinary Portland Cement (OPC), SCBA, and GGBFS were made. These specimens then exposed to several elevated temperatures for 2 h, afterword is allowed to cool at room temperature. The following basic physical, mechanical, and microstructural characteristics were then determined and discussed. (a) mass loss ratio, (b) ultrasonic pulse velocity (UPV) (c) physical behavior, (d) compressive strength, and (e) field emission scanning electron microscope (FESEM). It was found that compressive strength increases up to 400℃; beyond this temperature, it decreases. UPV value and massloss decrease with increase in temperature as well as the change in color and crack were observed at a higher temperature.

Self-Assembly Monolayers 처리 공정이 블록 공중합체를 이용한 나노패턴 제조에 미치는 영향

  • 황영현;권순묵;김영환;조원주;김용태
    • 한국진공학회:학술대회논문집
    • /
    • 한국진공학회 2011년도 제40회 동계학술대회 초록집
    • /
    • pp.339-339
    • /
    • 2011
  • 기존의 광학리소그래피방법으로는 나노크기의 패턴을 형성하는데에 있어서 많은 제약이 있으며, 사실상 수십나노크기의 패턴을 형성하는데에는 전자빔리소그래피등 새로운 패턴형성 방법이 요구되고 있다. 블록 공중합체를 이용한 나노 패턴은 서로 다른 화학적 구조를 가지는 고분자들이 공유결합으로 연결되어 있는 분자구조를 이용하여, 하나의 분자 내에 서로 다른 블록들이 상분리를 일으키려는 것과 동시에 이들의 공유결합으로 인해 그 정도가 제한되는 것을 이용하여 라멜라, 실린더, 구 등의 주기적으로 배열된 형태의 구조물을 형성하는 패터닝 기술이다. 블록 공중합체를 이용한 나노크기의 패턴 형성은 열역학적으로 안정적인 구조이며, 대면적으로 구현 할 수 있어서 차세대 소자제작을 위한 제작기술로 많은 관심을 가지고 있다. 하지만 블록공중합체를 이용한 나노패턴 기술은 선행적으로 나노구조체를 결함이 없고, 원하는 형태로 제작 할 수 있는 공정의 확립이 필요하다. 따라서 본 연구에서는, 이러한 블록 공중합체을 이용한 나노패턴을 제조하는 공정에서, 폴리스틸렌과 실리콘 산화물 박막과의 표면반응을 막기 위한 Self-Assembly Monolayers (SAMs) 처리 공정이 패턴 형성에 미치는 영향을 알아보기 위하여 MPTS의 농도 및 처리시간을 변화시켰다. 나노패턴을 분석, 확인하기 위하여 Atomic Force Microscopic (AFM)과 Field Emission Scanning Electron Microscope (FESEM)을 이용하였다.

  • PDF

Linear Ion Source에 의해 증착된 Diamond-Like Carbon(DLC) 박막의 질화층 형성에 따른 밀착력 특성 연구 (Study on the Adhesion of Diamond Like Carbon Films Using the Linear Ion Source with Nitriding Layers)

  • 신창석;박민석;권아람;김승진;정원섭
    • 한국표면공학회지
    • /
    • 제44권5호
    • /
    • pp.190-195
    • /
    • 2011
  • Diamond-like carbon (DLC) has many outstanding properties such as low friction, high wear resistance and corrosion resistance. However, it is difficult to achieve enough adhesion on the metal substrates because of weak bonding between DLC film and the metal substrate. The purpose of this study is to enhance an adhesion of DLC film. For improving adhesion, the substrate was treated by active screen plasma nitriding before DLC film deposing. Nitrided substrates were investigated by Glow Discharge Spectrometer (GDS), Micro-Vickers Hardness. DLC films were deposited on several metals by linear ion source, and characteristics of the films were investigated using nano-indentation, Field Emission Scanning Electron Microscope (FESEM). The adhesion was measured by scratch tester. The adhesion of DLC films was increased when nitriding layer was formed before DLC deposition. Therefore, the adhesion of DLC film can be enhanced as increasing the hardness of materials.

Microstructure of the Silk Spinning Nozzles in the Lynx Spider, Oxyopes licenti (Araneae: Oxyopidae)

  • Moon, Myung-Jin
    • Animal cells and systems
    • /
    • 제10권2호
    • /
    • pp.85-91
    • /
    • 2006
  • The lynx spiders are free wandering spiders with long spines on their legs. They do not build web, but hunt small insects on plants. In spite of the facts that the wandering spiders do not produce webs for prey-catching, they also have silk apparatuses even though the functions are not fully defined. This paper describes the microstructural organization of the silk-spinning nozzles and its silk glands of the lynx spider, Oxyopes licenti, revealed by the field emission scanning electron microscope (FESEM). The silkspinning nozzles of this spider were identified as three groups: ampullate, pyriform and aciniform glands. Each group of silk gland feed silk into one of the three pairs of spinnerets. Two pairs of major ampullate glands send secretory ductules to the anterior spinnerets, and another two pair of minor ampullate glands supply the middle spinnerets. In addition, the pyriform glands feed silk into the anterior spinnerets (25-30 pairs in females and 24-40 pairs in males), and the aciniform glands send ductules to the middle (9-12 pairs in females and 7-11 pairs in males) and the posterior spinnerets (16-20 pairs in females and 16-17 pairs in males). Among these, the ampullate one is the most predominate gland in both sexes. However the flagelliform and the aggregate glands which had the functions of cocoon production or adhesive thread production in other webbuilding spiders were not observed at both sexes of this spider.

The effect of thickness and operation temperature on Ga doped ZnO thin film NOx gas sensor

  • 황현석;여동훈;김종희;송준태;김정호
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
    • /
    • pp.365-365
    • /
    • 2008
  • In this work, Ga-doped ZnO (GZO) thin films for NOx gas sensor application were deposited on low temperature co-fired ceramics (LTCC) substrates, by RF magnetron sputtering method. The LTCC substrate is one of promising materials for this application since it has many advantages (e.g., low cost production, high manufacturing yields and easy realizing 3D structure etc.). The LTCC substrates with thickness of 400 pm were fabricated by laminating 12 green tapes which consist of alumina and glass particle in an organic binder. The structural properties of the fabricated GZO thin films with different thickness are analyzed by X-ray diffraction method (XRD) and field emission scanning electron microscope (FESEM). The GZO gas sensors are tested by gas measurement system under varing operation temperature and show good performance to the NOx gas in sensitivity and response time.

  • PDF

증착 온도 변화에 따른 IGZO 박막의 특성

  • 김성연;이태일;명재민
    • 한국재료학회:학술대회논문집
    • /
    • 한국재료학회 2009년도 춘계학술발표대회
    • /
    • pp.23.1-23.1
    • /
    • 2009
  • Transparent thin film transistor(TTFT)는 기존의 디스플레이가 가지고 있는 공간적, 시각적 제약을 해소하는 것이 가능하며, 이는 디스플레이 산업 및 기술이 지향하는 대면적, 저가격, 공정의 단순함을 해결해 줄 수 있기 때문에 최근 TTFT에 관한 연구가 급증하고 있다. 산화물 기반의 TFT는 유리, 금속, 플라스틱 등등 그 기판 종류에 상관없이 균일한 제작이 가능하며, 상온 및 저온에서 대면적으로 제작 가능하고, 저렴한 비용으로 제작 가능하다는 장점 때문에 최근 산화물을 기반으로 하는 TFT 연구가 많이 이루어지고 있다. 현재 TTFT 물질로 많이 연구되고 있는 산화물은 ZnO(3.4 eV)나 $InO_x$(3.6 eV), $GaO_x$(4.9 eV), $SnO_x$(3.7 eV)등의 물질과 각각의 조합으로 구성된 재료들이 주로 사용되고 있다. 가장 많은 연구가 이루어진 ZnO 기반의 TFT는 mobility와 switching 속도에서 우수한 특성을 보이나, amorphous ZnO 기반의 TFT의 경우 소자의 안정성이 떨어지는 것으로 보고되고 있다. 따라서 본 연구에서는 ZnO 보다 넓은 bandgap energy를 가질 수 있으며, n-type 특성을 보이고, amorphous 구조로 제작 가능한 IGZO 물질을 사용하여 RF magnetron sputtering 방법으로 박막 증착 온도의 변화를 주어 증착하였고, 증착된 IGZO 박막의 열처리를 통해 이에 따른 특성 변화를 분석하였다. Field emission scanning electron microscope(FESEM)와 surface profiler를 이용하여 IGZO 박막의 표면의 형상과 두께를 확인하였으며, x-ray diffraction(XRD) 분석을 통해 박막의 결정학적 특성을 관찰하였다. TTFT 물질로서 IGZO 박막의 적합성 여부를 확인하기 위하여 TFT를 만든 후 I-V를 측정하였으며, UV-vis를 이용하여 IGZO 박막의 투과율을 분석하여 TTFT로의 응용 가능성을 확인하였다.

  • PDF

테라헤르츠 영역에서의 BST 박막의 유전 특성 평가 (Terahertz dielectric characteristics of (Ba,Sr)$TiO_3$ thin films)

  • 조광환;강종윤;윤석진;이영백;맹인희;손주혁
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2007년도 추계학술대회 논문집
    • /
    • pp.28-28
    • /
    • 2007
  • Ferroelectric $(Ba_{0.5}Sr_{0.5})TiO_3$ (BST) thin films of thickness 500nm were deposited on $LaAlO_3$, (LAO) substrates by at $800^{\circ}C$. BST films were characterized for structure using X-ray diffraction (XRD). The surface morphology and thickness of BST the films were characterized by atomic force microscopy (AFM) and field emission scanning electron microscope (FESEM). We measured the dielectric properties at microwave frequencies (1~3 GHz) using a symmetrical stripline resonator with shorted ends and terahertz frequencies (0.2~2.5 THz) using a time-domain terahertz spectroscopy. The real and imaginary parts of the complex dielectric constant of the BST thin films on LAO substrates were in agreement with those previously reported.

  • PDF