• Title/Summary/Keyword: Fiber Identification

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Extraction of dietary fibers from cassava pulp and cassava distiller's dried grains and assessment of their components using Fourier transform infrared spectroscopy to determine their further use as a functional feed in animal diets

  • Okrathok, Supattra;Thumanu, Kanjana;Pukkung, Chayanan;Molee, Wittawat;Khempaka, Sutisa
    • Animal Bioscience
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    • v.35 no.7
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    • pp.1048-1058
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    • 2022
  • Objective: The present study was to investigate the extraction conditions of dietary fiber from dried cassava pulp (DCP) and cassava distiller's dried grains (CDG) under different NaOH concentrations, and the Fourier transform infrared (FTIR) was used to determine the dietary fiber components. Methods: The dried samples (DCP and CDG) were treated with various concentrations of NaOH at levels of 2%, 4%, 6%, and 8% using a completely randomized design with 4 replications of each. After extraction, the residual DCP and CDG dietary fiber were dried in a hot air oven at 55℃ to 60℃. Finally, the oven dried extracted dietary fiber was powdered to a particle size of 1 mm. Both extracted dietary fibers were analyzed for their chemical composition and determined by FTIR. Results: The DCP and CDG treated with NaOH linearly or quadratically or cubically (p<0.05) increased the total dietary fiber (TDF) and insoluble fiber (IDF). The optimal conditions for extracting dietary fiber from DCP and CDG were under treatment with 6% and 4% NaOH, respectively, as these conditions yielded the highest TDF and IDF contents. These results were associated with the FTIR spectra integration for a semi-quantitative analysis, which obtained the highest cellulose content in dietary fiber extracted from DCP and CDG with 6% and 4% NaOH solution, respectively. The principal component analysis illustrated clear separation of spectral distribution in cassava pulp extracted dietary fiber (DFCP) and cassava distiller's dried grains extracted dietary fiber (DFCDG) when treated with 6% and 4% NaOH, respectively. Conclusion: The optimal conditions for the extraction of dietary fiber from DCP and CDG were treatment with 6% and 4% NaOH solution, respectively. In addition, FTIR spectroscopy proved itself to be a powerful tool for fiber identification.

Cannabinol Synthase Gene Based Molecular Markers for Identification of Drug and Fiber Type Cannabis sativa (마약성과 비마약성 대마 품종의 식별을 위한 카나비놀 생합성 유전자 분석법)

  • Park, Hyun-Seung;Oh, Hye Hyun;Kim, Sungmin;Park, Jee Young;Kim, Jintae;Shim, Hyeonah;Yang, Tae-Jin
    • Korean Journal of Pharmacognosy
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    • v.52 no.2
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    • pp.69-76
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    • 2021
  • Cannabis sativa is an important industrial plant utilized to produce fiber, oil, and medicinal ingredients. A chemotype of cannabis is divided into "Drug type" with predominance of tetrahydrocannabinolic acid (THCA) and "Fiber type" with cannabidiolic acid (CBDA). To develop molecular markers for the discrimination of these two types, nucleotide sequences of THCA synthase and CBDA synthase as well as their pseudogenes were retrieved from the recently published cannabis genome in chromosome scale. Gene-specific SNPs were discovered by multiple alignment of these sequences, and 2 dominant marker sets from each gene were designed for selective amplification. Our markers successfully identified "Drug type" and "Fiber type" cannabis plants as well as forensic samples including processed materials. Our molecular markers will provide a fast and efficient system for molecular-based identification of the cannabis plant.

Study on the Baekje's Cotton Fabrics Excavated in Neungsan-ri Temple Site (부여 능산리 사지 출토 백제 면직물연구)

  • Sim, Yeon Ok;Chung, Yong Jae;Yu, Ji A;Namgung, Seung
    • Korean Journal of Heritage: History & Science
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    • v.44 no.3
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    • pp.4-17
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    • 2011
  • The Baekje's cotton fabrics were excavated from 'Neungsan-ri temple site in Buyeo' (September 1999-April 2000) and stored at Buyeo National Museum after conservation treatment. In this study, it carred out non-destructive, chemical and morphological analysis for fiber identification, also considered on influx, features and difference between the 'Baek-cheop-po(Three kingdom period's cotton fiber)' and 'Mok-myeon(imported by Munikjeom, late Korea dynasty)'. As a result, the fiber proved cellulose fiber through analytical researches like color reaction, FT-IR(chemical analysis). It was also confirmed lumens, typical dimensional structure(morphological analysis) as an features of cotton fiber. The fiber was the first evidence in ancient Korea's cotton. But it can not prove that whether weaving were made in Baekje's area. However there were documentation that people in Beakje make cloth to silk fabric from 'Mahan period'. We can suppose that they have had an old weaving techniques. This study has a great historical, academic values as the only evidence for the hypothesis of a weaving technique of the Baekje's cotton. Through comparison to each region's ancient cottons, we can investigate the species of Baekje's cotton and ancient Korea cotton's influx.

Concentration Characteristics of Indoor and Outdoor Airborne Total Fiber Particles and Identification of Asbestos in Gyeongnam Provinces (경남지역의 실내외 공기 중 총섬유 입자의 농도특성 및 석면 입자의 확인)

  • Park, Hee-Eun;Park, Jeong-Ho;Kim, Hyoung-Kab
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.22 no.2
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    • pp.119-127
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    • 2012
  • Objectives: The aim of this study is to identify concentration characteristics of indoor and outdoor airborne total fiber particles and asbestos in Gyeongnam Provinces. Methods: This study investigated concentration characteristics of indoor fiber particles from 748 schools and 38 public facilities as well as outdoor particles from 11 sites through PCM (phase contrast microscope). SEM/EDX (scanning electron microscope/energy dispersive using X-ray analysis) was used to obtain physicochemical information of asbestos fiber particles. The study identified asbestos rate in the 15 samples from indoor and outdoor airborne total fiber particles. Results: 1. The average indoor airborne concentrations of total fiber particles were $0.0011{\pm}0007$ f/cc in schools and $0.0015{\pm}0007$ f/cc in public facilities by PCM. Over 90% of the fiber particles were identified as single fibers. 2. The average outdoor airborne concentrations of total fiber particles were $0.0007{\pm}0002$ f/cc, and they were lower than those of indoor airborne concentrations. 3. The results showed that the form of asbestiform was diverse as skein of thread like form and long needle, which was relatively narrower than that of glass fiber and rock wool. 4. The results of SEM/EDX analysis of 15 areas where total fiber particle was relatively high showed that the form was rather similar to that of asbestos, but chemical composition was proven to be non-asbestos. Conclusions: The concentration of indoor and outdoor airborne total fiber particles of Gyeongnam Provinces satisfied the IAQ (Indoor air quality) level of 0.01 f/cc and asbestos was not found in most of the samples by SEM/EDX.

Numerical study for identifying damage in open-hole composites with embedded FBG sensors and its application to experiment results

  • Yashiro, S.;Murai, K.;Okabe, T.;Takeda, N.
    • Advanced Composite Materials
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    • v.16 no.2
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    • pp.115-134
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    • 2007
  • This study proposes two new approaches for identifying damage patterns in a holed CFRP cross-ply laminate using an embedded fiber Bragg grating (FBG) sensor. It was experimentally confirmed that the reflection spectrum from the embedded FBG sensor was significantly deformed as the damage near the hole (i.e. splits, transverse cracks and delamination) extended. The damage patterns were predicted using forward analysis (a damage analysis and an optical analysis) with strain estimation and the proposed damage-identification method as well as the forward analysis only. Forward analysis with strain estimation provided the most accurate damage-pattern estimation and the highest computational efficiency. Furthermore, the proposed damage identification significantly reduced computation time with the equivalent accuracy compared to the conventional identification procedure, by using damage analysis as the initial estimation.

Review of Radio Frequency Identification and Wireless Technology for Structural Health Monitoring

  • Dhital, Dipesh;Chia, Chen Ciang;Lee, Jung-Ryul;Park, Chan-Yik
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.3
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    • pp.244-256
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    • 2010
  • Radio frequency identification(RFID) combined with wireless technology has good potential for structural health monitoring(SHM). We describe several advantages of RFID and wireless technologies for SHM, and review SHM examples with working principles, design and technical details for damage detection, heat exposure monitoring, force/strain sensing, and corrosion detection in concrete, steel, carbon fiber reinforced polymer(CFRP), and other materials. Various sensors combined with wireless communication are also discussed. These methodologies can be readily developed, implemented, and customized. There are some technical difficulties, but solutions are being addressed. Lastly, a surface acoustic wave-based RFID system is presented, and possible future trends of SHM based on RFID and wireless technology are presented.

Identification of Cutting Mechanisms in Orthogonal Cutting of Glass Fiber Reinforced Composites

  • Choe Gi-Heung
    • Proceedings of the Korean Institute of Industrial Safety Conference
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    • 2000.11a
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    • pp.39-45
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    • 2000
  • In recent years, composite materials such as fiber reinforced plastics (FRP) have gained considerable attention in the aircraft and automobile industries due to their light weight, high modulus and specific strength. In practice, control of chip formation appears to be the most serious problem since chip formation mechanism in composite machining has significant effects on the finished surface [1,2,3,4,5]. Current study will discuss frequency analysis based on autoregressive (AR) time series model and process characterization in orthogonal cutting of a fiber-matrix composite materials. A sparsely distributed idealized model composite material, namely a glass reinforced polyester (GFRP) was used as workpiece. Analysis method employs a force sensor and the signals from the sensor are processed using AR time series model. The experimental correlation between the different chip formation mechanisms and model coefficients are established.(omitted)

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Multi-modal Vibration Control of Intelligent Laminated Composite Plates Using System Identification and Optimal Control (시스템식별과 최적제어를 이용한 지능형 복합적층판의 다중보드 진동제어)

  • 김정수;강영규;박현철
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.12 no.1
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    • pp.5-11
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    • 2002
  • Active vibration control of intelligent laminated composite plates is performed experimental1y Laminated composite place is modeled by the system identification method. For the system identification process, the laminated composite place is excited by two piezoelectric actuators with PRBS signals. At the same time, the displacement of the laminated composite plate is measured by a gap sensor. From these excited PRBS signals and the measured displacement sequence, system parameters of the laminated composite plate are estimated using a recursive prediction error method. Model of the laminated composite plate with two piezoeletric actuators is assumed to be the form of ARMAX. From the estimated ARHMAX model, a state space equation of the observable canonical form is obtained. With this state space equation, a controller and an observer for active vibration control is designed using the optimal control method. Controller and observer are implemented on a digital system. Experiments on the vibration control are Performed with changing the outer layer fiber orientation of intelligent composite plates.

Analysis of fiber and pigment in Palsapumdo from Hyeonchungsa (현충사관리소 소장 팔사품도(八賜品圖)에 사용된 직물 · 종이 섬유 식별 및 안료 분석)

  • Park, Ji-Hee;Kim, So-Jin;Kim, Soon-Kwan
    • 보존과학연구
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    • s.32
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    • pp.75-87
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    • 2011
  • The materials analysis is important in conservation science for cultural assets since conservators can make appropriate decision of treatment and environment through understanding manufacturing, period and materials. Palsapumdo is the painting of Palsapum which was given by Yi Sun-shin from the emperor Shinjong in The Ming Dynasty. Palsapumdo painted with various pigments on the fabric has remained to adhere a sheet of lining paper. In this study, we carried out the fiber identification about the fabric and lining paper and the analysis of the pigments. This study identified a fabric and a lining paper and analised pigments for the painting. As a result of fabric analysis, it was confirmed as cotton because ribbon twists and shape of kidney bean in a cross section. After the analysis of lining paper, color changed to yellow by Graff "C" staining tests, and had short fiber and tracheid. Therefore, it is supposed to be a paper which is made of conifer pulp. In addition, the results of SEM-EDS, the pigments are indicated as Orpiment($As_2S_3$), Minium($Pb_3O_4$), Hematite($Fe_2O_3$), Emeraldgreen ($C_2H_3As_3Cu_2O_8$), Ultramarine [$2(Na_2O{\cdot}Al_2O_3{\cdot}2SiO_2){\cdot}Na_2S_2$], talc[$Mg_3Si_4O_{10}(OH)_2$], bariumsulfate($BaSO_4$) and brass.

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Identification of Hydrophobic Components in Cambodian Kapok Fiber (캄보디아산 케이폭 섬유의 소수성에 영향을 미치는 성분규명)

  • Sung, Yong Joo;Yun, Su-Young;Oh, Sung-Hoon;Shin, Soo-Jeong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.5
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    • pp.30-36
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    • 2013
  • Hydrophobic property of Kapok fiber was investigated by sequential removal of its components by different extraction methods. Acetone extraction for the removal of the hydrophobic extractives, holo-cel-lulose preparation after the removal of lignin and xylan extraction by potassium hydroxide was applied. The degree of hydrophobicity of each samples were measured by the water sorption ability. The water sorption ability of Kapok fiber was increased by the sequential treatment of acetone extraction, holocellulose preparation and xylan removal. Based on holocellulose compositional analysis by $^1H$-NMR spectroscopic method, the unusual high amount of the acetyl groups in the holocellulose of Kapok partially contributed to the hydrophobicity of Kapok holocellulose fiber.