• Title/Summary/Keyword: Fe-Si-B-Nb-Cu

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EFFECT OF FLASH ANNEALING ON MAGNETIC PROPERTIES OF Fe-BASED NANOCRYSTALLINE ALLOYS

  • Yu, Xiaojun;Quan, Baiyun;Sun, Guiqin;Narita, Kenji
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.507-510
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    • 1995
  • A heat-treatment method of pre-annealing and then flash annealing(FA) has been used to improve the soft magnetic properties of nanocrystalline $Fe_{76}CuSi_{13}B_{10}$ and $Fe_{74}CuNb_{3}Si_{12}B_{10}$ alloys. Outstanding magnetic properties of nanocrystalline $Fe_{74}CuNb_{3}Si_{12}B_{10}$ alloy were attained by flash-annealing in air after annealed at $500^{\circ}C$ for 0.5hr below the crystallization temperature. The same results were obtained for $Fe_{74}CuSi_{13}B_{10}$ alloy. The measurment of relief of stress and X-ray diffraction were used to analyze the effect of flashannealing.

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Electromagnetic Wave Absorption Characteristics of Nanocrystalline FeCuNbSiB Alloy Flakes/Polymer Composite Sheets with Different Flake Thickness

  • Lee, Tae-Gyu;Kim, Ju-Beom;Noh, Tae-Hwan
    • Journal of Magnetics
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    • v.14 no.4
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    • pp.155-160
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    • 2009
  • This study examined the effects of a decrease in thickness of magnetic alloy flakes on the electromagnetic wave absorption characteristics of nanocrystalline $Fe_{73.5}Cu_1Nb_3Si_{15.5}B_7$ (at.%) alloy flakes/polymer composite sheets available for a quasi-microwave band. The thickness of FeCuNbSiB alloy flakes decreased to 1-2 $\mu$m with increasing milling time up to 24 h, and the composite sheet including alloy flakes milled for 24 h exhibited considerably enhanced power loss properties in the GHz range compared to the sheets having non-milled alloy powders. Although a considerable increase in loss factor upon milling was observed in the narrow frequency range of 4-6 GHz, there was no correlation between the complex permeability and flake thickness. However, the complex permittivity increased with increasing milling time, and there was good agreement between the milling time and the frequency dependences of the complex permittivity and power loss.

Structure and Magnetic Properties of a Fe73.5Si13.5B9Nb3Cu1 Alloy Nanopowder Fabricated by a Chemical Etching Method and Milling Procedure

  • Hong, Seong-Min;Kim, Jeong-Gon;Kim, Cheol-Gi
    • Journal of Magnetics
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    • v.14 no.2
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    • pp.71-74
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    • 2009
  • The magnetic and structural properties of FINEMET (the Hitachi product name of the Fe-Si-B-Nb-Cu alloy) nanopowder with a composition of $Fe_{73.5}Si_{13.5}B_9Nb_3Cu_1$ atomic percent were investigated after annealing, chemical etching, and mechanical milling. The primary and secondary crystallization temperatures were 523 and $550^{\circ}C$, respectively. The grain size of the particles was adjusted by annealing time. Optimally annealed particles exhibited a homogenous microstructure composed of nanometer-sized crystalline grains. The grain boundary of the annealed particles was etched preferentially by chemical etching. Chemically etched particles were broken at the grain boundary by high-energy ball milling. As a result, a nanometer-sized FINEMET powder with a uniform size of crystalline grains was fabricated.

Dynamic Magneto-mechanical Behavior of Magnetization-graded Ferromagnetic Materials

  • Chen, Lei;Wang, Yao
    • Journal of Magnetics
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    • v.19 no.3
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    • pp.215-220
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    • 2014
  • This study investigates the dynamic magneto-mechanical behavior of magnetization-graded ferromagnetic materials Terfenol-D/FeCuNbSiB (MF). We measure the dynamic magneto-mechanical properties as a function of the DC bias magnetic field ($H_{dc}$). Our experimental results show that these dynamic magneto-mechanical properties are strongly dependent on the DC bias magnetic field. Furthermore, the dynamic strain coefficient, electromechanical resonance frequency, Young's moduli, and mechanical quality factor of Terfenol-D/FeCuNbSiB are greater than those of Terfenol-D under a lower DC bias magnetic field. The dynamic strain coefficient increases by a factor of between one and three, under the same DC bias magnetic field. In particular, the dynamic strain coefficient of Terfenol-D/FeCuNbSiB at zero bias achieves 48.6 nm/A, which is about 3.05 times larger than that of Terfenol-D. These good performances indicate that magnetization-graded ferromagnetic materials show promise for application in magnetic sensors.

Effects of Annealing Temperature on Electromagnetic Wave Absorption Characteristics in FeCuNbSiB Alloy Flakes/Polymer Composite Sheets (FeCuNbSiB 합금 박편/폴리머 복합 시트의 전자파 흡수 특성에 미치는 자성분말 어닐링 온도의 영향)

  • Noh, Tae-Hwan;Lee, Tae-Gyu
    • Journal of the Korean Magnetics Society
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    • v.17 no.5
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    • pp.198-204
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    • 2007
  • The effects of annealing temperature on electromagnetic wave absorption characteristics in $Fe_{73.5}Cu_1Nb_3Si_{15.5}B_7$ (at%) alloy flakes/polymer composite sheets available for quasi-microwave band have been investigated. The composite sheet including the magnetic flakes annealed at $425{\sim}475^{\circ}C$ for 1 h exhibited highest power loss in the GHz frequency range as compared with the sheets composed of the alloy flakes annealed at higher temperature than $475^{\circ}C$ or in as-milled state. Moreover the imaginary part of complex permeability had largest value in the GHz frequency range for the sheets including the flakes annealed at $425{\sim}475^{\circ}C$. The large value of power loss of the sheets including the magnetic flakes annealed at $425{\sim}475^{\circ}C$ was attributed to the high imaginary part of the complex permeability. However, because of its large transmission parameter $S_{21}$, the composite sheet having the magnetic flakes annealed at $525^{\circ}C$ showed low power loss.

Permeability Aftereffect in FeCuNbSiB Alloy (FeCuNbSiB 합금의 투자율 여효)

  • Lee, Yong-Ho;Sin, Yong-Dol;No, Tae-Hwan;Gang, Il-Gu
    • Journal of the Korean Magnetics Society
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    • v.2 no.3
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    • pp.216-221
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    • 1992
  • Annealing effects on the permeability aftereffect(disaccommodation) of liquid quenched single strip $Fe_{73.5}Cu_1Nb_3Si_{16}B_{6.5}$ alloys were investigated with pulse method. The initial susceptibility X, $B_{10},$ (the flux density at 10 Oe) and disaccommodation intensity D (D = [X(1 s)-X(64 s)]/X(1 s), where X(1 s) and X(64 s) are the susceptibility of 1 and 64 s of rest time after A. C. demagnetization) were about 800, 0.8 T and 16 %, respectively. The soft magnetic properties were improved with isothermal annealing for 1 hour at $300{\sim}600^{\circ}C.$ X, $B_{10},$ and D at $570^{\circ}C$ of optimum annealing temperature were 15000, 1.2 T and 1.1 %, respectively. The origin of the change of characteristics were examined with fine crystalline structure and magnetostriction.

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