• 제목/요약/키워드: FT4

검색결과 1,590건 처리시간 0.023초

Change of Heating Value, pH and FT-IR Spectra of Charcoal at Different Carbonization Temperatures

  • Kwon, Sung-Min;Jang, Jae-Hyuk;Lee, Seung-Hwan;Park, Sang-Bum;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • 제41권5호
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    • pp.440-446
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    • 2013
  • To understand transition characteristics from wood to charcoal, Quercus variabilis wood was carbonized at 200, 250, 300, 340, 540 and $740^{\circ}C$, respectively. Heating value, pH and surface property by FT-IR spectroscopy of the carbonized charcoal were investigated. Heating value and pH increased with increasing carbonization temperature from 4500 cal/g and 4.3 of the control wood to 8,000 cal/g and 9 of the charcoal carbonized at $740^{\circ}C$, respectively. From FT-IR spectroscopy, the peaks from O-H, C-H and C-O stretching disappeared during carbonization at 540 and $740^{\circ}C$. Aromatic skeletal vibration at near $1,506{\sim}1,593cm^{-1}$ was repidly increased until $540^{\circ}C$. These results suggest that the chemical and physical characteristics of wood components in cell wall can be easily changed by increasing carbonization temperature and the carbonization seem to be incomplete at temperature below $540^{\circ}C$.

Thermal and uplift histories of Mesozoic granites in Southeast Korea: new fission track evidences

  • Shin, Seong-Cheon;Susumu Nishimura
    • 암석학회지
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    • 제2권2호
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    • pp.104-121
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    • 1993
  • Fission track (FT) thermochronological analyses on Mesozoic granites provide new information about cooling and uplift histories in Southeast Korea. Twenty-nine new FT sphene, zircon and apatite ages and seven track length measurements are presented for eleven granite samples. Measured mineral ages against assumed closure temperatures yield cooling rates for each sample. Relatively rapid (7-$15^{\circ}C$/Ma) and simple cooling patterns from the middle Cretaceouss (ca. 90-100 Ma) granites are caused mainly by a high thermal contrast between the intruding magma and country rocks at shallow crustal levels (ca. 1-2.5 km-depths). On the contrary, a slow overall cooling (1-$4^{\circ}C$/Ma) of the Triassic to Jurassic granites (ca. 250-200 Ma), emplaced at deep depths (>>9 km), may mainly depend upon very slow denudation of the overlying crust. The uplift history of the Triassic Yeongdeog Pluton in the Yeongyang Subbasin, west of the Yangsan Fault, is characterized by a relatively rapid uplift (~0.4 mm/a) before the total unroofing of the pluton in the earliest Cretaceous (~140 Ma) followed by a subsidence (~0.2mm/a) during the Hayang Group sedimentation. Stability of original FT zircon ages (156 Ma) and complete erasure of apatite ages suggest a range of 3 to 5.5 km for the basin subsidence. Since 120 Ma up to present, the Yeongyang Subbasin has been slowly uplifted (~0.04 mm/a). The FT age patterns of Jurassic granites both from the northeastern wing of the Ryeongnam Massif and from the northern edge of the Pohang-Kampo Block indicate that the two geologic units have been slowly uplifted with a same mean rate (~0.04 mm/a) since early Cretaceous. Estimates of Cenozoic total uplifts since 100 Ma are different: Ryeongnam Massif (~6 km)=Pohang-Kampo Block (~6 km)>Yeongyang Subbasin(~4 km).

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Nondestructive Evaluation for the Viability of Watermelon (Citrullus lanatus) Seeds Using Fourier Transform Near Infrared Spectroscopy

  • Lohumi, Santosh;Mo, Changyeun;Kang, Jum-Soon;Hong, Soon-Jung;Cho, Byoung-Kwan
    • Journal of Biosystems Engineering
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    • 제38권4호
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    • pp.312-317
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    • 2013
  • Purpose: Conventional methods used to evaluate seeds viability are destructive, time consuming, and require the use of chemicals, which are not feasible to implement to process plant in seed industry. In this study, the effectiveness of Fourier transform near infrared (FT-NIR) spectroscopy to differentiate between viable and nonviable watermelon seeds was investigated. Methods: FT-NIR reflectance spectra of both viable and non-viable (aging) seeds were collected in the range of 4,000 - 10,000 $cm^{-1}$ (1,000 - 2,500 nm). To differentiate between viable and non-viable seeds, a multivariate classification model was developed with partial least square discrimination analysis (PLS-DA). Results: The calibration and validation set derived from the PLS-DA model classified viable and non-viable seeds with 100% accuracy. The beta coefficient of PLS-DA, which represented spectral difference between viable and non-viable seeds, showed that change in the chemical component of the seed membrane (such as lipids and proteins) might be responsible for the germination ability of the seeds. Conclusions: The results demonstrate the possibility of using FT-NIR spectroscopy to separate seeds based on viability, which could be used in the development of an online sorting technique.

Poly(amic acid)/organoclay 나노복합체의 열적특성 및 난연성 (Thermal Properties and Flame Retardancy of Poly(amic acid)/organoclay Nanocomposites)

  • 김선;윤두수;조병욱;최재곤
    • Elastomers and Composites
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    • 제42권3호
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    • pp.177-185
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    • 2007
  • 유기화된 montmorillonite(O-MMT)와 인을 포함하는 polyamic acid(PPAA)를 용액 블렌딩하여 PAA/organoclay 나노 복합체를 제조하였다. 이들 나노 복합체들의 연구를 위하여 FT-IR, DSC, TGA, PCFC, SEM 그리고 XRD를 이용하였다. 나노복합체들의 제조확인은 FT-IR과 XRD 분석을 통하여 확인하였다. SEM 사진들은 O-MMT가 매트릭스 고분자에 비교적 고르게 분산되어 있음을 보여 주었고, XRD 결과를 통하여 O-MMT가 intercalation 되었음을 확인하였다. O-MMT/PPAA 나노복합체들의 열안정성 및 난연성은 순수한 PAA 보다 크게 높았으며, O-MMT/PPAA-0.2, 0.4, 0.6 복합체들의 열방출 용량과 총열방출 값들은 인의 함량 증가와 함께 감소하였다. 본 연구에서 제조된 나노복합체 필름들이 화재안전재료로서 사용될 수 있는 잠재성을 가지고 있음을 확인하였다.

시뮬레이션을 활용한 신기술 항만장비의 생산성 추정 (The Estimation of Productivity Considering New Technology Port- Equipment By Using Simulation)

  • 김동원
    • 한국컴퓨터정보학회논문지
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    • 제20권1호
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    • pp.237-246
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    • 2015
  • 본 논문에서는 컨테이너터미널에서 탠덤 리프트 안벽크레인과 고생산성 컨테이너 이송차량 Alternative ship-to-yard vehicles를 고려한 시뮬레이션을 활용하여 컨테이너터미널의 생산성 향상 모델을 제안한다. 이 방법의 특징은 탠덤 리프트 안벽크레인과 고생산성 컨테이너 이송차량의 데이터를 도출하고, 회귀분석 함으로써 탠덤 리프트 안벽크레인의 생산성 모델을 추정한다. 탠덤 리프트 안벽크레인은 한 사이클 당 20ft 컨테이너 4개, 40ft 컨테이너 2개를 동시에 취급함으로서 기존의 싱글 안벽크레인보다 이론상 약 2배의 컨테이너 생산성을 증가시키는 장비이고 Alternative ship-to-yard vehicles는 기존의 야드 트랙터보다 더 많은 최대 4TEU의 컨테이너를 운반시킬 수 있는 장비이다. 본 논문에서는 신기술 안벽장비인 탠덤 리프트 안벽크레인과 신기술 이송장비인 Alternative ship-to-yard vehicles를 적용한 시뮬레이션을 통하여 생산성에 관한 데이터를 도출하고 통계 기법인 회귀분석을 통하여 컨테이너 터미널의 생산성의 추정모델을 구해보고자 한다.

Antibacterial property of 4-hexylresorcinol incorporated in silk mat after sterilization

  • Kim, Seong-Gon;Kweon, HaeYong;Jo, You-Young
    • International Journal of Industrial Entomology and Biomaterials
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    • 제42권2호
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    • pp.46-50
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    • 2021
  • When 4-hexylresorcinol (4HR) incorporated silk mat is used for clinical application, sterilization process is essential. In this study, 4HR incorporated silk mat was sterilized with ethylene oxide (EO) gas or autoclave, and then antibacterial property was evaluated. For the examination of micro-structure after the sterilization, scanning electron microscopic (SEM) exam and Fourier Transform Infrared (FT-IR) spectroscopy were also done. There was no gross difference after sterilization in SEM exam and FT-IR spectra. Antibacterial property of 4HR was also maintained after the sterilization. In conclusion, EO gas or autoclave did not damage the antibacterial property of 4HR in the silk mat.

경남지역 특수학교 학생의 구강내 세균검사에 따른 영구치우식경험률에 관한 연구 (A study on analysis of the Relationship Oral bacteria to dental caries experience in disabled student's: in Gyeong-nam)

  • 조평규;박성숙
    • 한국치위생학회지
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    • 제8권4호
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    • pp.115-125
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    • 2008
  • The purpose of this study was to examine the relationship between the Dentocult SM and LB scores of students and their DMF rate. The subjects in this study were 134 special school students in south Gyeong-sang province. After they were tested to find out their, they received tooth brushing education and preventive treatment. The test, education and treatment were all conducted from March 17 to April 9, 2008. Their oral state was checked and recorded by using a mirror and explorer, and then the data on oral state were analyzed to their DMFT, DT, FT and MT rates. All the collected data were analyzed with SPSS 15.0 for Windows program, and independent-samples t-test, one-way ANOVA and crosstabs analysis were implemented to see what differences their disability type, gender, Dentocult-SM scores and Dentocult-LB scores made. The findings of the study were as follows: 1. As for connections between disability type and DMFT rate, the students with mental retardation were similar to the other students in that regard. The mentally retarded students had higher DT and FT rates than the other students, and the MT rate of the latter was higher than that of the former. 2. Concerning the relationship of gender to DMFT and DT rates, the girls had larger DMFT and DT rates than the boys, and the FT and MT rates of the boys were higher than those of the girls. 3. As to links between Dentocult SM scores on the tongue and DMFT, the students whose bacteria was mildly activated had the highest DMFT rate, and the students who had a severely activated bacteria had the highest DT and FT rates. Those who had a moderately activated bacteria had the highest MT rate. 4.Regarding the connection of Dentocult SM scores on maxillyright molar to DMFT and DT rates, the students whose bacteria was severely activated had the highest DMFT and DT rates. Those who had no activated bacteria had the largest FT rate, and the students who had a mildly activated bacteria had the highest MT rate. 5.Regarding the connection of Dentocult SM scores on maxillyleft molar to DMFT and DT rates, the students whose bacteria was severely activated had the highest DMFT and DT rates. Those who had no activated bacteria had the largest FT rate, and the students who had a mildly activated bacteria had the largest MT rate. 6. Regarding the connection of Dentocult SM scores on mandibularright molar to DMFT and DT, FT rates, the students whose bacteria was severely activated had the highest DMFT and DT, FT rates. Those who had a moderately activated bacteria had the highest MT rate. 7. Regarding the connection of Dentocult SM scores on mandibularleft molar to DMFT and DT rates, the students whose bacteria was mildly activated had the highest DMFT and DT rates. Those who had no activated bacteria had the largest FT rate, and the students who had a moderately activated bacteria had the highest MT rate. 8. Regarding the connection of Dentocult LB scores to DMFT and DT rates, the students whose bacteria was severely activated had the highest DMFT and DT rates. Those who had no activated bacteria had a moderately FT rate, the students who had a mildly activated bacteria had a mildly MT rate.

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총채벌레 및 고추탄저병의 동시 방제를 위한 곤충병원성 곰팡이 Isaria javanica FT333 선발 (Selection of Entomopathogenic Fungus Isaria javanica FT333 for Dual Control of Thrips and Anthracnose)

  • 이모란;정혜주;김재윤;김다연;안성호;이상엽;한지희
    • 한국균학회지
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    • 제46권4호
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    • pp.479-490
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    • 2018
  • 고추의 주요 병해충인 총채벌레(Thrips palmi)와 탄저병(Colletotrichum acutatum)을 방제하기 위해 다양한 화학농약이 사용되고 있지만, 농약의 오남용으로 인하여 이에 대한 저항성이 발생하여 방제가 힘들어지고 환경오염을 초래하는 문제가 있다. 그리하여 본 연구에서는 이러한 문제를 극복하고자 총채벌레에 대한 살충효과와 탄저병에 항균력이 우수한 균주를 선발하여 동시 방제의 가능성을 확인하고자 하였다. 토양으로부터 분리한 곤충병원성 곰팡이 13균주($1{\times}10^7conidia/mL$)를 오이총채벌레 성충과 약충에 처리하여 70~100%의 우수한 살충률을 나타내는 6균주를 선발하였다. 선발한 6균주의 항균활성을 검정하기 위하여 고추 탄저병균에 대치 배양한 결과, 항균력이 우수한 FT333 균주를 최종 선발할 수 있었다. 최종 선발된 균주를 형태학적 조사와 internal transcribed spacer, ${\beta}-tubulin$ 영역의 염기서열 분석을 통하여 Isaria javanica로 동정하였고, I. javanica FT333으로 명명하였다. I. javanica FT333 (KACC93316P)의 고추 탄저병균에 대한 방제 효과를 기내에서 검정한 결과($1{\times}10^5$, $1{\times}10^6$, $1{\times}10^7conidia/mL$) 95% 이상의 방제효과를 나타내었다. 이러한 결과들을 바탕으로 I. javanica FT333 균주가 고추 탄저병균과 미소해충인 오이총채벌레를 동시에 방제하기 위한 미생물제제로서 이용될 수 있는 가능성을 제시하였다.

동시형광 분광광도법에 의한 대기 시료 중의 다환방향족 탄화수소(PAHs)의 분석 (Determination of Polycyclic Aromatic Hydrocarbons (PAHs) in Atmospheric Samples by Synchronous 2nd Derivate Spectrofluorimetry)

  • 유광식;정선이;정지영
    • 한국대기환경학회지
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    • 제20권1호
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    • pp.129-138
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    • 2004
  • Determination of some PAHs in ambient air at Ulsan have been carried out by collection of the components into n-hexane followed by synchronous spectrofluorimetric technique. 10 PAHs, such as acenaphthene (Ace), anthracene (Anth), benz[a]anthracene (BaA), benzo[b]fluoranthene (BbFt), benzo[k]fluoranthene (BkFt) benzo[a]pyrene (BaP), chrysene (Chry), phenanthrene (Phen), fluoranthene (Ft), perlyrene (Per), and pyrene (Pyr) in air samples were able to determine separately by synchronous spectrofluorimetry. Calibration curves for those components were linear for the concentration range of 0.2∼166ppb PAHs with the correlation factor of 0.9985∼0.9999. The predominant contribution was phenanthrene which was included 36.9∼85.1% to the overall level of the 10 PAHs in some areas. Also benzo[a]pyrene which was known to carcinogenicity was detected from 6.4 to 55.8ng/㎥, benzo[a]anthracene of some areas was contained from 21.9∼153ng/㎥.

고강도와 보통 강도 콘크리트를 사용한 보-기둥 접합부의 휨강성화에 따른 이력거동 (The Effect of The Flexural Strength Ratio on Beam-Column Joint with High and Low Strength Concrete)

  • 신성우;안종문;문정일;김대근;이광수;박희민;이승훈;오정근
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1992년도 가을 학술발표회 논문집
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    • pp.185-190
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    • 1992
  • ACI318-89 Recommended that when the specified compressive strength of concrete in a column is greater than1.4 times that specified for a floor system, top surface of the column concrete shall extend 2ft(600mm)into the slab from the face of column to avoid unexpected brittle failure. The major variables are extension distance, flexural strength ratio(Mr), and shear reinforcement ratio(Vs). Test results are as follows ; (1) The failure modes of specimens under cyclic loading were concentrated at critical region from beam-column joint face. (2) Ductility index($\mu$f) were increased with increasing of shear confinement ratio and flexural strength ratio. (3)The specimens with 2ft extension distance showed more ductility than the specimens with 1ft extension distance.

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