• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2013년도 춘계학술대회 논문집
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• pp.1153-1154
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• 2013

• Bulletin of the Korean Chemical Society
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• 제31권7호
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• pp.1976-1980
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• 2010

A simple and reliable method has been developed to selectively separate and concentrate trace amounts of Fe(III) ions from water and food samples by using flame atomic absorption spectrometry. A new reagent, 5-hydroxy-4-ethyl-5,6-di-pyridin-2-yl-4,5-dihydro-2H-[1,2,4] triazine-3-thione, was synthesized and characterized by using FT-IR spectroscopy and elemental analysis. Effects of pH, concentration and volume of elution solution, sample flow rate, sample volume and interfering ions on the recovery of Fe(III) were investigated. The optimum pH was found to be 5. Eluent for quantitative elution was 10 mL of 2 M HCl. The preconcentration factor of the method, detection limit (3s/b, ${\mu}gL^{-1}$) and relative standard deviation values were found to be 25, 4.59 and 1%, respectively. In order to verify the accuracy of the method, two certified reference materials (TMDA 54.4 lake water and SRM 1568a rice flour) were analyzed. The results obtained were in good agreement with the certified values. The method was successfully applied to the determination of Fe(III) ions in water and food samples.

• Korean Chemical Engineering Research
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• 제54권5호
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• pp.636-647
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• 2016

Magnetite nanoparticles ($Fe_3O_4$ NPs) were synthesized by co-precipitating method under optimized condition. The $Fe_3O_4$ NPs coated with sodium dodecyl sulfate-thenoyltrifluoroacetone ($Fe_3O_4$ NPs-SDS-TTFA) were then exerted as the magnetic solid phase extraction (MSPE) adsorbent for the extraction process prior to introducing to a flame atomic adsorption spectrometry (FAAS). The synthesized $Fe_3O_4$ NPs-SDS-TTFA were applied for the extraction of Pb(II) ions from different water samples. The characterization studies of nanoparticles were performed via scanning electron microscopy-energy dispersive micro-analysis (SEM-EDAX), X-ray diffraction (XRD) and vibrating sample magnetometer (VSM) techniques. The substantial parameters affecting the extraction efficiency were surveyed and optimized. A dynamic linear range (DLR) of $10-400{\mu}g\;L^{-1}$ was obtained and the limit of detection (LOD, n=7) and relative standard deviation (RSD%, n= 6, $C=20{\mu}g\;L^{-1}$) were found to be $2.3{\mu}g\;L^{-1}$ and 1.9%, respectively. According to the results, the proposed method successfully applied for the extraction of Pb(II) ions from different environmental water samples and satisfactory results achieved.

• Earthquakes and Structures
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• 제18권3호
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• pp.285-296
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• 2020

Dams are important structures for management of water supply for irrigation or drinking, flood control, and electricity generation. In seismic regions, the structural safety of concrete gravity dams is important due to the high potential of life and economic loss if they fail. Therefore, the seismic analysis of existing dams in seismically active regions is crucial for predicting responses of dams to ground motions. In this paper, earthquake response of concrete gravity dams is investigated using the finite element (FE) method. The FE model accounts for dam-water-foundation rock interaction by considering compressible water, flexible foundation effects, and absorptive reservoir bottom materials. Several uncertainties regarding structural attributes of the dam and external actions are considered to obtain the fragility curves of the dam-water-foundation rock system. The structural uncertainties are sampled using the Latin Hypercube Sampling method. The Pine Flat Dam in the Central Valley of Fresno County, California, is selected to demonstrate the methodology for several limit states. The fragility curves for base sliding, and excessive deformation limit states are obtained by performing non-linear time history analyses. Tensile cracking including the complex state of stress that occurs in dams was also considered. Normal, Log-Normal and Weibull distribution types are considered as possible fits for fragility curves. It was found that the effect of the minimum principal stress on tensile strength is insignificant. It is also found that the probability of failure of tensile cracking is higher than that for base sliding of the dam. Furthermore, the loss of reservoir control is unlikely for a moderate earthquake.

• 한국지반공학회논문집
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• 제23권4호
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• pp.185-197
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• 2007

한계해석법인 상 하계법은 점착성, 점착성-마찰성, 마찰성분만 가지는 지반에서의 주로 얕은 터널에 대한 안정수를 구하기 위해 발전되어 왔다. 그러나 점성이 없고 마찰성분만 존재하는 지반에서의 비교적 깊은 터널에 대한 이러한 해석법의 연장은 현재까지 그 연구가 드물게 진행되어왔다. 따라서 본 연구는 이러한 상황에서의 터널붕괴하중을 구하기 위한 근사적인 해석법으로 응력불연속장에 근거하는 하계법과 동적 파괴메카니즘에 근거하는 상계법을 각각 제안하였다. 이러한 해석법에 의한 터널붕괴하중은 수치해석과 기존의 경계해석법과 비교되었으며 특히, 터널 수평축 상에 위치하는 유한지반요소들에 대한 유한요소해석 결과와 잘 일치됨을 보여 주었다.

• 토지주택연구
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• 제11권2호
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• pp.87-94
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• 2020

Offshore renewable energy resources are attractive alternatives in addressing the nation's clean energy policies because of the high demand for electricity in the coastal region. As a large portion of potential resources is in deep and farther water, economically competitive floating systems have been developed. Despite the advancement of floating technologies, the high capital cost remains a primary barrier to go ahead offshore renewable energy projects. The dynamically installed piles (DIPs) have been considered one of the most economical pile concepts due to their simple installation method, resulting in cost and time-saving. Nevertheless, applications to real fields are limited because of uncertainties and underestimated load capacity. Thus, this study suggests the appropriate analytical approach to estimate the inclined load capacity of the DIPs by using the upper bound plastic limit analysis (PLA) method. The validity of the PLA under several conditions is demonstrated through comparison to the finite element (FE) method. The PLA was performed to understand how flukes, soil profiles, and load inclinations can affect the inclined load capacity and to provide reliable evaluations of the total resistance of the DIPs. The studies show that PLA can be a useful framework for evaluating the inclined load capacity of the DIPs under undrained conditions.

• 열처리공학회지
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• 제1권1호
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• pp.8-12
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• 1988

This study has been carried out to evaluate gaseous nitrocarburizing treatment undertaken for pure iron at $570^{\circ}C$ in an atmosphere containing 50% endothermic gas, generated from natural gas, and 50% ammonia. The results obtained from the experiment are as follows ; 1) The microstructure of gaseous nitrocarburized pure iron consists of the compound layer on the surface and the diffusion zone beneath it. The compound layer progresses uniformly into ferrite with a thickness of $20{\mu}$ obtained after treating for 3 hours. 2) Chemical analysis has shown that the compound layer has a C/N ratio of 0.19 and that the average combined interstitial content of the compound layer is about 30 atomic percent, which is close to the lower limit of the ${\varepsilon}$-carbonitride phase field in Fe-C-N phase diagram. 3) X-ray diffraction analysis has revealed that the compound layer consists mainly of the c.p.h. phase, ${\varepsilon}-Fe_3$(C.N) and a small amount of $Fe_4N$ and traces of ferrite are also present in the compound layer. 4) The microhardness of the compound layer is about 600 V.H.N and shows a relatively sharp fall-off at the compound layer/diffusion zome interface. 5) The average actual degree of ammonia dissociation is calculated to be 27% for a gaseous nitrocarburizing treatment carried out at $570^{\circ}C$.

• 전기학회논문지
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• 제60권10호
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• pp.1846-1857
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• 2011

This paper deals with design and analysis of surface-mounted PM (SPM) motor for compressor of air-conditioning system for electric vehicle applications according to slot/pole combination. First, required torque-speed curve characteristics are determined from operating conditions of the compressor. Restricted conditions such as motor size limit and current density are also determined. And then, under same rated and restricted conditions, twelve models which have different slot/pole combinations each other are designed for various pole arc/pitch ratio using simple equations and 2-d finite element (FE) analyses. Designed models are analyzed and compared in terms of back-emf THD, cogging torque, torque ripple, power losses, efficiency, etc. On the basis of analysis results, it is found that the motor with a 6-pole PM rotor and a 27-slot stator has most outstanding performances in electromagnetic aspects. Finally, through the mechanical modal analysis and demagnetization analysis, it is concluded that the determined motor is most suitable for the compressor of air-conditioning system for electric vehicles.

• Structural Engineering and Mechanics
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• 제51권5호
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• pp.847-866
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• 2014

This paper describes a formulation to predict optimum post-tensioning forces and cable dimensioning for self-anchored cable-stayed suspension bridges. The analysis is developed with respect to both dead and live load configurations, taking into account design constrains concerning serviceability and ultimate limit states. In particular, under dead loads, the analysis is developed with the purpose to calculate the post-tensioning cable forces to achieve minimum deflections for both girder and pylons. Moreover, under live loads, for each cable elements, the lowest required cross-section area is determined, which verifies prescriptions, under ultimate or serviceability limit states, on maximum allowable stresses and bridge deflections. The final configuration is obtained by means of an iterative procedure, which leads to a progressive definition of the stay, hanger and main cable characteristics, concerning both post-tensioning cable stresses and cross-sections. The design procedure is developed in the framework of a FE modeling, by using a refined formulation of the bridge components, taking into account of geometric nonlinearities involved in the bridge components. The results demonstrate that the proposed method can be easily utilized to predict the cable dimensioning also in the framework of long span bridge structures, in which typically more complexities are expected in view of the large number of variables involved in the design analysis.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1998년도 춘계학술대회논문집
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• pp.205-209
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• 1998

Unlike the drawing of round section from round bar, the shaped drawing like polygonal section is known to have influence not only drawing stress but also comer filling. Therefore, this study analyze the drawing process of suqare rod from round bar using nonsteady state rigid-plastic FEM. To investigate effects of process variables of the drawing process of square rod from round bar, FE-simulations with variety of reduction in area and semi-die angle for a given frictional condition have been conduction. By this results, it has to suggest optimal process condition on the drawing stress and the comer filling. In addition, it has determined forming limit considering necking and bulging.