• 한국분말재료학회지
• /
• 제17권1호
• /
• pp.44-51
• /
• 2010

The rheological behavior of a cordierite honeycomb extrusion paste was investigated by measuring torque values in a Brabender plastograph. The extrusion pastes were formulated using binder (methy cellulose, MC), solvent (water), plasticizer (ploy ethylene glycol, PEG) and lubricants (oleic acid, OA). The mixing sequence and optimum organic binder, at least for homogeneous mixed state, can be determined from the rheological point of view. 3%MC-30%$H_2O$-1.5%PEG-1.0%OA with respect to the cordierite powder was chosen as a binder composition for the extrusion process of cordierite powder.

• 한국세라믹학회지
• /
• 제27권3호
• /
• pp.355-360
• /
• 1990

One of the possible ways to make a flexible wire of high-Tc superconductiong ceramics is the extrusion of a mixture slurry of superconducting powder with an appropriate polymer binder. The fabrication procedure for $YBa_2Cu_3O_{7-{\delta}}$ superconducting coils with this plastic mass is described. The major factors limiting the formation of extruded wire are the binder content, powder size, and entrapped gas in the mixture slurries. The optimum content of binder for both good flexbility and strength of wire was estimated to be 30wt%. The finer the powder size is, the more homogeneous structure the extruded wire has. The vacuum degassing before extrusion was necessary to remove the entrapped gas in as-extruded wire. The formability of wire depends greatly on the wire radius and binder content. After burning out the binder and the successive sintering, the contacts between the superconducting grains could be made. The resistivity vs. temperature behavior measured in the final wire showed the transition temperature of 90K with narrow transition width. However, the critical current densities of these wires are much lower in comparison to those of conventional bulk specimens.

• Advances in concrete construction
• /
• 제9권1호
• /
• pp.93-102
• /
• 2020

In this study, we examined the relationship among the rheological properties, workability, and extrudability in the construction of concrete structures using additive manufacturing. We altered the component materials (binder type, water-binder (W/B) ratio, sand ratio) to assess their effect on the rheological properties experimentally. The results indicated that the W/B and sand ratios had the largest effect on the rheological properties. In particular, when the sand ratio increased, it indicated that adjusting the sand ratio would facilitate control over the rheological properties. Additionally, we compared the rheological properties with the results of a traditional workability evaluation, namely the table flow test. This indicated the possibility of inferring the rheological properties by using traditional methods. Finally, we evaluated extrusion quantity according to table flow. The extrusion rate was 350 g/s for a flow of 210 mm and 170 g/s for a flow of 130 mm, indicating that extrusion rate increased as flow increased; however, we concluded that a flow standard of approximately 140-160 mm is suitable for controlling the actual extrusion quantity and rate.

• 한국분말재료학회지
• /
• 제27권3호
• /
• pp.256-267
• /
• 2020

Metal additive manufacturing (AM) technologies are classified into two groups according to the consolidation mechanisms and densification degrees of the as-built parts. Densified parts are obtained via a single-step process such as powder bed fusion, directed energy deposition, and sheet lamination AM technologies. Conversely, green bodies are consolidated with the aid of binder phases in multi-step processes such as binder jetting and material extrusion AM. Green-body part shapes are sustained by binder phases, which are removed for the debinding process. Chemical and/or thermal debinding processes are usually devised to enhance debinding kinetics. The pathways to final densification of the green parts are sintering and/or molten metal infiltration. With respect to innovation types, the multi-step metal AM process allows conventional powder metallurgy manufacturing to be innovated continuously. Eliminating cost/time-consuming molds, enlarged 3D design freedom, and wide material selectivity create opportunities for the industrial adoption of multi-step AM technologies. In addition, knowledge of powders and powder metallurgy fuel advances of multi-step AM technologies. In the present study, multi-step AM technologies are briefly introduced from the viewpoint of the entire manufacturing lifecycle.

• 한국재료학회:학술대회논문집
• /
• 한국재료학회 2011년도 춘계학술발표대회
• /
• pp.54.1-54.1
• /
• 2011

Porous hydroxyapatite has been widely used as clinical implanted material. However, it has poor mechanical properties. To increase the strength as well as the biocompatibility of the porous HAp based artificial bone, it was fabricated by multi-extrusion process. Hydroxyapatite and graphite powders were mixed separately with ethylene vinely acetate and steric acid by shear mixing process. Hydroxyapatite composites containing porous microstructure were fabricated by arranging it in the die and subject it to extrusion process. Burn-out and sintering processes were performed to remove the binder and graphite as well as increase the density. The external and internal diameter of cylindrical hollow core were approximately 10.4 mm and 4.2 mm, respectively. The size of pore channel designed to increase bone growth (osteconduction) was around 150 ${\mu}m$ in diameter. X-ray diffraction analysis and SEM observation were performed to identity the crystal structure and the detailed microstructure, respectively.

• Korean Chemical Engineering Research
• /
• 제49권6호
• /
• pp.726-731
• /
• 2011

F-T 반응이 공업적으로 활용되기 위해서는 촉매의 대량 합성 및 성형체의 기계적 강도가 매우 중요한 변수로 적용될 수 있다. 따라서 본 논문에서는 F-T 합성반응용 촉매로 잘 알려진 Fe 계열 촉매의 성형체 제조를 위한 바인더의 영향을 알아보기 위한 연구를 수행하였다. 촉매 바인더로는 무기바인더와 유기바인더를 사용하여 촉매 성형체를 제조하였다. 무기바인더 및 유기바인더의 종류와 함량에 따른 성형촉매의 물리화학적 특성을 XRD, BET, PSD, TPR, UTM으로 분석하였으며, F-T 합성 반응성에 대한 영향을 관찰함으로써 최적의 성형 촉매 제조 조성을 확립할 수 있었다.

• 한국축산식품학회지
• /
• 제32권2호
• /
• pp.155-161
• /
• 2012

This study was carried out to investigate the encapsulation of lactic acid in starch matrix for the application into emulsified sausages. For the encapsulation of lactic acid in starch, the extrusion method was applied, by the different extrusion pressure level. The particle size and morphology of lactic acid containing starch granules and the rate of release of lactic acid from those granules were determined by using Mastersizer$^{(R)}$, a scanning electron microscopy, and electrical conductivity. The size varied slightly depending upon the extruder pressure and influenced entrapment efficiency. Lactic acid was released more slowly, when the extruder had fewer holes, which meant higher extrusion pressure, than when the extruder had more holes. Extruder pressure is therefore critical for producing finer granules that can retain lactic acid longer, during the processing of meat products.

• 동력기계공학회지
• /
• 제19권4호
• /
• pp.30-35
• /
• 2015

The purpose of this study is to identify the low temperature performance and strength characteristics of V-based extruded homogeneous SCR. The extruded catalyst and the coated catalyst showed 50% and 27% of NOx conversion performance respectively at about $210^{\circ}C$ of catalyst temperature, so the extruded SCR was higher in de-NOx performance than the coated SCR especially at a low temperature zone. The compressive strength of the Enhanced Extrusion #1, in which the content of promoters such as silica, clay, glass fiber and binder was optimized, was a 120% improvement compared to the Extrusion#1 catalyst, higher than the coated SCR.

• Korean Chemical Engineering Research
• /
• 제52권2호
• /
• pp.261-265
• /
• 2014

정수처리 방식에 있어서 소형화의 필요성이 증대됨에 따라 복합적인 기능을 갖는 단일구조 여과재 개발이 절실히 요구되고 있다. 본 연구에서는 단일구조를 가지는 필터개발을 위하여 활성탄과 고분자 바인더로 구성된 성형체를 압출소결방식으로 제조하여, 제조된 성형체의 밀도, 공극률 및 유량을 평가하여, 최대유량을 가지는 성형체의 최적 압출온도를 결정하였다. 또한 성형체의 공극률 평가에 있어서 전체 공극률뿐만 아니라 관통형 기공의 공극률을 추가로 평가하여 유량과의 상관성을 평가하였다. 압출온도가 고분자 바인더의 Melting point인 $133^{\circ}C$ 이상인 $140{\sim}230^{\circ}C$에서 단일구조 복합 활성탄 성형체 구성이 가능하였으며, 압출온도 $170^{\circ}C$가 복합성형체의 밀도가 낮고, 관통기공의 공극률이 높아, 최대유량을 가지는 복합성형체의 제조가 가능한 최적 압출온도로 확인되었다. 또한 복합성형체를 통해 흐르는 물의 유량은 성형체의 전체 공극률 보다 관통형기공의 공극률에 크게 의존함을 알 수 있었다.

• Korean Chemical Engineering Research
• /
• 제51권3호
• /
• pp.352-357
• /
• 2013

본 연구에서는 정수장 슬러지를 사용하여 제조한 정수슬러지 가공 분말의 압출공정을 통해서 입상흡착제를 제조하였다. 바인더 첨가와 소성과정이 입상형 흡착제의 물리 화학적 특성에 미치는 영향을 질소흡착, 압축강도, 주사전자현미경, 엑스선회절, 피리딘흡착 적외선분광법 등으로 분석하였다. 바인더의 함량을 5 wt%까지 증가시키면 압축강도가 3배 이상으로 개선되었으나 트리메틸아민을 흡착할 수 있는 표면적이 30% 정도 감소하여 입상흡착제의 트리메틸아민 파과시간이 단축되었다. 성형된 입상흡착제의 소성과정을 통해서 표면에 브뢴스테드산점과 루이스산점으로 구성된 산점이 발현되어, 염기성 기체인 트리메틸아민의 파과 시간이 3배 이상으로 증가하였다.