• Title/Summary/Keyword: Extraction of dye

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The Acquisition and dyeability of Gardenia jasminoides Colorant (치자색소의 염료화 및 염색성)

  • 서영숙;정지윤
    • The Research Journal of the Costume Culture
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    • v.7 no.2
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    • pp.315-322
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    • 1999
  • The acquistion and dyeability of the Gardenia jasminoides were examined to establish the optimum condition for extraction and storage in the process of obtaining the natural dye, Gardenia jasminoides colorant. Also the dyeability and colorfastness of Gardenia jasminoides were investigated. The results of this study are as follows. The optimum part-removed seed. In all experiments, the part of fat-removed seed and pericarp was used. The optimum condition for extraction of Gardenia jasminoides colorant was at 40℃ and for 90 min. in methanol. As storage temperature was higher, the absorbance of colorant extract decreased rapidly. The Gardenia jasminoides colorant exhibited dyeability to cotton, silk, wool, and nylon. The dyeability was the greatest in wool, and then nylon, silk, and cotton. Both wool and nylon had the greatest K/S value at pH3, however, nylon and cotton at pH 6 and pH 8 respectively. In addition, the increase in K/S value corresponded to temperature in wool and nylon, but the silk and cotton had the greatest K/S value at 60℃. Also, the K/S value increased in concomitant with the increased number of dyeing repetition. In the most cases, colorfastness of light was weak but colorfastness of laundry, sweat was relatively excellent.

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The Analysis of 1,4-Dioxane in Water Sample by Gas Chromatograph/Mass Spectrometer and Risk Assessment (기체크로마토그래프/질량분석계에 의한 물시료 중 1,4-dioxane의 분석 및 위해성 평가)

  • 홍지은;표희수;박송자
    • Environmental Analysis Health and Toxicology
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    • v.18 no.3
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    • pp.219-224
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    • 2003
  • 1,4-Dioxane is used as a solvent for lacquers, paints, varnish removers, dye baths and printing compositions. And it is also used for detergent preparations, cosmetics, deodorants and fumigants. A method is described for the determination of 1,4-dioxane in water samples by GC/MS. The extraction recoveries were studied for some solvents and solvent volume ratio were investigated using r-butyl methyl ether (MTBE). Optimum condition was obtained by the liquid-liquid extraction using the 10 mL of MTBE for 10 mL of water. Method detection limit of 1,4-dioxane in the 20 mL of water samples was 0.05 ng/mL. It could be determined in the range of 0.24∼240 ng/mL in treated water, and in the range of 0.69∼81.9 ng/mL in raw water, respectively. Risk assessments with 1,4-dioxane exposure by drinking water ingestion were carried out. Based on the results of analysis, chronic daily intake of 1,4-dioxane was 2.22${\times}$10$\^$-4/ mg/kg/day and excess cancer risk was calcu-lated to be 2.44${\times}$10$\^$-6/.

Steady-State and Transient Response Analysis of DSSC Based on Electron Diffusion Coefficient and Chemical Capacitance

  • J. C. Gallegos;J. Manriquez;R. Rodriguez;S. Vargas;D. Rangel
    • Journal of Electrochemical Science and Technology
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    • v.15 no.2
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    • pp.276-290
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    • 2024
  • A study of the transition from transitory state to steady state in DSSCs based on natural dyes is presented; cochineal was used as dye and Li+, Na+, and K+ were the ions added to the electrolyte. The photocurrent profiles were obtained as a function of time. Several DSSCs were prepared with different cations and their role and the transitory-to-steady transition was determined. A novel hybrid charge carrier source model based on the Heaviside function H(t) and the Lambert-Beer law, was developed and applied to analysis of the transient response of the output photocurrent. Additionally, the maximum effective light absorption coefficient α and the electronic extraction rate κ for each ion were determined: ${\alpha}_{Li^+,Na^+,K^+}\,=\,(0.486,\,0.00085,\,0.1126)\,cm^{-1}$, and also the electronic extraction rate ${\kappa}^{Li^+,Na^+,K^+}_{ext.}\,=\,(1410,\,19.07,\,19.69)\,cm\,s^{-1}$. The impedance model using Fick's second law was developed for carrier recombination to characterize the photocurrent.

천연염색에 사용되는 천연매염제에 관한 연구(I) - 볏짚재 -

  • 주영주;남성우
    • Textile Coloration and Finishing
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    • v.9 no.6
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    • pp.33-41
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    • 1997
  • This paper surveys the extraction condition of polygenetic natural dye, Sappan Wood and the effect of ash to the dyeability and fastness. The appropriate time for extracting Sappon Wood was 1hour. The pH was increased as the amount of ash increase. The pH was nearly invariable according to the time of ash solution, the extracting times and temperature. Absorbance of dyeing fabrics was about 480nm. From the result of K/S value determination of fabrics, 10g/$\ell$ quantity of ash was surfficient for treatment and the amount of Sappon Wood was in 100% o.w.f.. K/S value of fabrics pre-mordanted or post-mordanted were higher than that of fabrics simultaneous mordanted.K/S value was increased as pH of mordanting bath decrease and pre-mordanting and post-mordanting fabrics increased the amount of absorption (K/S value) compared with non-mordanted fabrics. It was found that pH of mordanting bath affected the amount of absorption and color change of dyed fabrics. Light fastness of fabric dyed was very poor and the fastness of fabric dyed was not influenced by the mordanting conditions and methods.

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Spectrophotometric Determination of Pipethanate Hydrochloride in Pharmaceutical Preparations with Methyl Orange

  • Chun, In-Koo;Chung, Hae-Soo;Lee, Min-Hwa;Chun, Bong-Kan
    • Journal of Pharmaceutical Investigation
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    • v.11 no.3
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    • pp.1-13
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    • 1981
  • A new application of monoacidic dye is reported for the determination of pipethanate hydrochloride(PTH). The method is based on solvent extraction into chloroform of an ion-pair compound formed between methyl orange(MO) and PTH. PTH is determined by measuring absorbance of the extracts over the range of $2.0{\sim}12.0{\mu}g/ml$ at 420nm. Best accuracy can be obtained for solutions containing $3.0{\sim}8.0{\mu}g/ml$. The color was stable for at least 5 days. The molar absorptivity was $2.88\;{\times}\;10^4\;l,\;mol^{-1},\;cm^{-1}$. Molar ratio and continuous variation plots have a maximum at 0.5 mol fraction of MO, indicating a 1 : 1 MO-PTH ratio.

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Studies on the Dyeing with plant pigments -extraction and UV/VIS spectrum of Carthamus flower- (직물색소에 의한 염색 연구I -홍화의 색소 추출 및 자외가시분광특성-)

  • 신인수
    • Journal of the Korean Home Economics Association
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    • v.32 no.1
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    • pp.229-238
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    • 1994
  • The purpose of this study was to investigate the objectification of coloring matter abstraction of the way to natural dye by cathamus flower. Watersoluble carthamin in the dyeing cathamus flower was removed for the fastness of dyeing and only insoluble carthamon was abstracted which came by solvent such as Sodium hydroxide(NaOH) Potassium hydroxide(KOH) Sodium carbonate(Na2CO3)and Potassi-um carbonate(K2CO3) Carthamon made abstract essence from a carthamus flower out of the pH6, pH7, pH9, pH11, solvent and by using a UV/VIS Spectra according to the change of pH. Silk dyes with solution abstract carthamon and it was treated by 5 kinds of mordant. The table of surface-colors was measured by the number of dyeing the color of silk dyed and by the kind of mordant which treated with and the dyeing was evaluated by measuring Color Fastness to Light and Washing.

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A Study on Spectrophotometric Determination of Oleic Acid by Basic Dye Methylen Bblue (염기성색소(鹽基性色素) Methylen Blue에 의(依)한 Oleic Acid의 흡광광도정량(吸光光度定量))

  • Lee, Sook-Yun
    • Journal of Pharmaceutical Investigation
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    • v.4 no.1_2
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    • pp.46-54
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    • 1974
  • A new spectrophotemetric method was estalished for the determination of oleic acid. This method is based on the 1,2-dichloroe-thane extraction of the ion-pair formed between methylene blue and oleic acid. But the absorbance of an ion-pair in the 1,2-dichloroe-thane layer was variable with the temperature, the ion-pair was extracted back into a diluted hydrochloric acid solution. The maximum absorbance of the acid extract observed at $660m{\mu}$ and a lineal relationship was observed from the initial amount over the range of $50-800{\gamma}/ml$ of oleic acid in the aqueous phase. The composition ratio of the ion-pair formed between methylene blue and oleic acid was determined to be 2 : 1 by both the mole ratio and continuous variation methods.

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Analysis of Pattern for Indonesian Traditional Textile Design (인도네시아 전통직물 디자인의 패턴 분석)

  • Koo Hee-Kyung
    • Journal of the Korea Fashion and Costume Design Association
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    • v.7 no.3
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    • pp.83-94
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    • 2005
  • This paper is to analyze patterns for Indonesian traditional textiles. Ikat is the resist-dyeing process in which designs are reserved in warp or weft yams by tying off small bundles of threads with fiber resists to prevent the penetration of dye. Batik is the technique applying a wax resist before dyeing to form a pattern in negative. Ikat and batik are the most renowned textile arts of Indonesia. Patterns are classified as geometric pattern, plant pattern, animal pattern. Also this paper discusses the origins of ikat and batik. Therefore this Paper proposes the classification and feature extraction of ikat and batik patterns. The results of this study can be effectively applied to develop competitive pattern design for Indonesian textile market.

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Tryptophan-Based Hyperproduction of Bioindigo by Combinatorial Overexpression of Two Different Tryptophan Transporters

  • Hyun Jin Kim;Sion Ham;Nara-Shin;Jeong Hyeon Hwang;Suk Jin Oh;Tae-Rim Choi;Jeong Chan Joo;Shashi Kant Bhatia;Yung-Hun Yang
    • Journal of Microbiology and Biotechnology
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    • v.34 no.4
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    • pp.969-977
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    • 2024
  • Indigo is a valuable, natural blue dye that has been used for centuries in the textile industry. The large-scale commercial production of indigo relies on its extraction from plants and chemical synthesis. Studies are being conducted to develop methods for environment-friendly and sustainable production of indigo using genetically engineered microbes. Here, to enhance the yield of bioindigo from an E. coli whole-cell system containing tryptophanase (TnaA) and flavin-containing monooxygenase (FMO), we evaluated tryptophan transporters to improve the transport of aromatic compounds, such as indole and tryptophan, which are not easily soluble and passable through cell walls. Among the three transporters, Mtr, AroP, and TnaB, AroP enhanced indigo production the most. The combination of each transporter with AroP was also evaluated, and the combination of AroP and TnaB showed the best performance compared to the single transporters and two transporters. Bioindigo production was then optimized by examining the culture medium, temperature, isopropyl β-D-1-thiogalactopyranoside concentration, shaking speed (rpm), and pH. The novel strain containing aroP and tnaB plasmid with tnaA and FMO produced 8.77 mM (2.3 g/l) of bioindigo after 66 h of culture. The produced bioindigo was further recovered using a simple method and used as a watercolor dye, showing good mixing with other colors and color retention for a relatively long time. This study presents an effective strategy for enhancing indigo production using a combination of transporters.

Dudleya brittonii extract promotes survival rate and M2-like metabolic change in porcine 3D4/31 alveolar macrophages

  • Kim, Hyungkuen;Jeon, Eek Hyung;Park, Byung-Chul;Kim, Sung-Jo
    • Asian-Australasian Journal of Animal Sciences
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    • v.32 no.11
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    • pp.1789-1800
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    • 2019
  • Objective: Although alveolar macrophages play a key role in the respiratory immunity of livestock, studies on the mechanism of differentiation and survival of alveolar macrophages are lacking. Therefore, we undertook to investigate changes in the lipid metabolism and survival rate, using 3D4/31 macrophages and Dudleya brittonii which has been used as a traditional asthma treatment. Methods: 3D4/31 macrophages were used as the in vitro porcine alveolar macrophages model. The cells were activated by exposure to phorbol 12-myristate 13-acetate (PMA). Dudleya brittonii extraction was performed with distilled water. For evaluating the cell survival rate, we performed the water-soluble tetrazolium salt cell viability assay and growth curve analysis. To confirm cell death, cell cycle and intracellular reactive oxygen species (ROS) levels were measured using flow cytometric analysis by applying fluorescence dye dichlorofluorescein diacetate and propidium iodide. Furthermore, we also evaluated cellular lipid accumulation with oil red O staining, and fatty acid synthesis related genes expression levels using quantitative polymerase chain reaction (qPCR) with SYBR green dye. Glycolysis, fatty acid oxidation, and tricarboxylic acid (TCA) cycle related gene expression levels were measured using qPCR after exposure to Dudleya brittonii extract (DB) for 12 h. Results: The ROS production and cell death were induced by PMA treatment, and exposure to DB reduced the PMA induced downregulation of cell survival. The PMA and DB treatments upregulated the lipid accumulation, with corresponding increase in the acetyl-CoA carboxylase alpha, fatty acid synthase mRNA expressions. DB-PMA co-treatment reduced the glycolysis genes expression, but increased the expressions of fatty acid oxidation and TCA cycle genes. Conclusion: This study provides new insights and directions for further research relating to the immunity of porcine respiratory system, by employing a model based on alveolar macrophages and natural materials.