• 제목/요약/키워드: Experimental Film

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진주담치 및 마른멸치 분말수우프의 제조 (Preparation of Powdered Dried Sea Mussel and Anchovy for Instant Soup)

  • 이응호;하재호;차용준;오광수;권칠성
    • 한국수산과학회지
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    • 제17권4호
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    • pp.299-305
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    • 1984
  • 진주담치와 멸치를 보다 효율적으로 이용하기 위한 방안의 하나로서 진주담치와 시판 마른멸치를 건조하여 분말화한 후 조미료를 배합하여 건조분말 수우프를 만들었으며, 또한 이것을 적층필름용기(cellophane/polyester/aluminium foil/polyester: $20{\mu}m/15{\mu}m/7{\mu}m/20{\mu}m,\;13{\times}14cm$)에 함기포장하여 상온저장 중의 품질안정성을 검토하였다. 진주담치 및 마른 멸치를 건조분말화한 다음 이것에 설탕 $3\%$, 식염 $2\%$, 글루탐산나트륨 $5\%$, 마늘가루 및 후추가루 가가 $0.2\%$를 배합하는 것이 즉석 분말수우프로서 가장 좋은 배합비이었다. 분말수우프 제품의 수분활성은 진주담치의 경우 0.41, 마른멸치의 경우는 0.31 정도이었다. 진주담치제품의 총카로테노이드함량은 저장 중 약간 감소하였고, 휘발성염기질소와 아미노질소는 전제품이 저장 중 거의 변화가 없었으며, TBA 값은 저장 30일까지 약간 증가하다가 그 후 서서히 감소하는 경향을 나타내었다. 관능검사 결과 멸치분말수우프 및 진주담치분말수우프 제품은 모두 저장 100일동안 품질에 큰 변화가 없었으므로 즉석분말수우프로 이용가능하다는 결론을 얻었다.

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화상분석법을 이용한 라텍스개질 콘크리트의 공극 구조와 투수성의 상관성 분석 (Estimation of Air Void System and Permeability of Latex-Modified Concretes by Image Analysis Method)

  • 정원경;윤경구;홍승호
    • 콘크리트학회논문집
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    • 제17권5호
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    • pp.695-702
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    • 2005
  • 라텍스개질 콘크리트는 라텍스의 첨가로 인하여 콘크리트의 내구성을 개선하는 것으로 알려져 있으며, 투수저항성이 크게 향상되는 것으로 연구되었다. 본 연구에서는 SBR 라텍스 혼입에 따른 콘크리트 내부 공극 구조의 변화를 연구하고자 화상분석법을 이용하여 라텍스개질 콘크리트의 W/C비, 라텍스 함량, 시멘트 종류에 변화를 주어 간격계수, 경화 후 공기량, 공극 직경에 따른 공극 분포 및 공극 구조 상태 분석 등을 파악하였다. 또한, 라텍스 첨가에 따른 내부 공극 구조 특성과 투수저항성과의 상관성을 비교하였다. 라텍스개질 콘크리트는 내부 공극 분석 결과, 동일 물-시멘트비 조건에서 AE감수제를 사용한 OPC에 비해 더 우수한 연행공극 효과가 있는 것으로 분석되었다. 초속경시멘트는 $100{\mu}m$ 미만의 연행공극의 수가 4배 이상 증가하였다. 조강 시멘트는 SBR 라텍스로 인하여 $50{\sim}500{\mu}m$ 범위의 미세 연행 공기량이 약 7배 이상 증가되는 현상을 나타내었다. 그러나 투수성에 있어서는 낮은 간격계수에도 불구하고 높은 투수저항 특성을 나타내었다. 내구성에 있어서 라텍스개질 콘크리트에서는 공극 구조의 영향보다는 라텍스 폴리머 필름에 의한 영향이 더 큰 것으로 판단되었다.

Aluminum Powder Metallurgy Current Status, Recent Research and Future Directions

  • Schaffer, Graham
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2001년도 추계학술강연 및 발표대회
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    • pp.7-7
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    • 2001
  • The increasing interest in light weight materials coupled to the need for cost -effective processing have combined to create a significant opportunity for aluminum P/M. particularly in the automotive industry in order to reduce fuel emissions and improve fuel economy at affordable prices. Additional potential markets for Al PIM parts include hand tools. Where moving parts against gravity represents a challenge; and office machinery, where reciprocating forces are important. Aluminum PIM adds light weight, high compressibility. low sintering temperatures. easy machinability and good corrosion resistance to all advantages of conventional iron bm;ed P/rv1. Current commercial alloys are pre-mixed of either the AI-Si-Mg or AL-Cu-Mg-Si type and contain 1.5% ethylene bis-stearamide as an internal lubricant. The powder is compacted in closed dies at pressure of 200-500Mpa and sintered in nitrogen at temperatures between $580~630^{\circ}C$ in continuous muffle furnace. For some applications no further processing is required. although most applications require one or more secondary operations such as sizing and finishing. These sccondary operations improve the dimension. properties or appearance of the finished part. Aluminum is often considered difficult to sinter because of the presence of a stable surface oxide film. Removal of the oxide in iron and copper based is usually achieved through the use of reducing atmospheres. such as hydrogen or dissociated ammonia. In aluminum. this occurs in the solid st,lte through the partial reduction of the aluminum by magncsium to form spinel. This exposcs the underlying metal and facilitates sintering. It has recently been shown that < 0.2% Mg is all that is required. It is noteworthy that most aluminum pre-mixes contain at least 0.5% Mg. The sintering of aluminum alloys can be further enhanced by selective microalloying. Just 100ppm pf tin chnnges the liquid phase sintering kinetics of the 2xxx alloys to produce a tensile strength of 375Mpa. an increilse of nearly 20% over the unmodified alloy. The ductility is unnffected. A similar but different effect occurs by the addition of 100 ppm of Pb to 7xxx alloys. The lend changes the wetting characteristics of the sintering liquid which serves to increase the tensile strength to 440 Mpa. a 40% increase over unmodified aIloys. Current research is predominantly aimed at the development of metal matrix composites. which have a high specific modulus. good wear resistance and a tailorable coefficient of thermal expnnsion. By controlling particle clustering and by engineering the ceramic/matrix interface in order to enhance sintering. very attractive properties can be achicved in the ns-sintered state. I\t an ils-sintered density ilpproaching 99%. these new experimental alloys hnve a modulus of 130 Gpa and an ultimate tensile strength of 212 Mpa in the T4 temper. In contest. unreinforcecl aluminum has a modulus of just 70 Gpa.

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방사선 치료용 고에너지 전자선의 조직 내 선량분포 특성에 관한 연구 (Study on Characteristics of Dose Distribution in Tissue of High Energy Electron Beam for Radiation Therapy)

  • 나수경
    • 대한방사선치료학회지
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    • 제14권1호
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    • pp.175-186
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    • 2002
  • The purpose of this study is directly measure and evaluate about absorbed dose change according to nominal energy and electron cone or medical accelerator on isodose curve, percentage depth dose, contaminated X-ray, inhomogeneous tissue, oblique surface and irradiation on intracavitary that electron beam with high energy distributed in tissue, and it settled standard data of hish energy electron beam treatment, and offer to exactly data for new dote distribution modeling study based on experimental resuls and theory. Electron beam with hish energy of $6{\sim}20$ MeV is used that generated from medical linear accelerator (Clinac 2100C/D, Varian) for the experiment, andwater phantom and Farmer chamber md Markus chamber und for absorbe d dose measurement of electron beam, and standard absorbed dose is calculated by standard measurements of International Atomic Energy Agency(IAEA) TRS 277. Dose analyzer (700i dose distribution analyzer, Wellhofer), film (X-OmatV, Kodak), external cone, intracavitary cone, cork, animal compact bone and air were used for don distribution measurement. As the results of absorbed dose ratio increased while irradiation field was increased, it appeared maximum at some irradiation field size and decreased though irradiation field size was more increased, and it decreased greatly while energy of electron beam was increased, and scattered dose on wall of electron cone was the cause. In percentage depth dose curve of electron beam, Effective depth dose(R80) for nominal energy of 6, 9, 12, 16 and 20 MeV are 1.85, 2.93, 4.07, 5.37 and 6.53 cm respectively, which seems to be one third of electron beam energy (MeV). Contaminated X-ray was generated from interaction between electron beam with high energy and material, and it was about $0.3{\sim}2.3\%$ of maximum dose and increased with increasing energy. Change of depth dose ratio of electron beam was compared with theory by Monte Carlo simulation, and calculation and measured value by Pencil beam model reciprocally, and percentage depth dose and measured value by Pencil beam were agreed almost, however, there were a little lack on build up area and error increased in pendulum and multi treatment since there was no contaminated X-ray part. Percentage depth dose calculated by Monte Carlo simulation appeared to be less from all part except maximum dose area from the curve. The change of percentage depth dose by inhomogeneous tissue, maximum range after penetration the 1 cm bone was moved 1 cm toward to surface then polystyrene phantom. In case of 1 cm and 2 cm cork, it was moved 0.5 cm and 1 cm toward to depth, respectively. In case of air, practical range was extended toward depth without energy loss. Irradiation on intracavitary is using straight and beveled type cones of 2.5, 3.0, 3.5 $cm{\phi}$, and maximum and effective $80\%$ dose depth increases while electron beam energy and size of electron cone increase. In case of contaminated X-ray, as the energy increase, straight type cones were more highly appeared then beveled type. The output factor of intracavitary small field electron cone was $15{\sim}86\%$ of standard external electron cone($15{\times}15cm^2$) and straight type was slightly higher then beveled type.

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제니핀을 첨가한 아교의 접착 특성과 물성 변화 연구 (A Study on Adhesion Characteristics and Physical Properties of Animal Glue Added Genipin)

  • 이준호;유지아;정용재
    • 보존과학회지
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    • 제34권3호
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    • pp.157-166
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    • 2018
  • 본 연구에서는 아교의 접착 특성 향상을 위해 가교제(Cross-linking Agent)를 첨가하는 방법으로 젤라틴 결합력을 증대하였다. 제니핀 첨가 아교는 물성 측정, 구조 분석, 색잔류도, 용출도, 파단강도를 측정하였으며, 수분과 자외선에 대한 내수성과 내광성을 비교하였다. 연구 결과 겔강도와 점도는 제니핀 첨가량에 따라 증가하였다. 구조분석 결과, 젤라틴에서는 구조적으로 안정된 콜라겐의 3중 구조의 흡수 피크가 관찰되었다. 색잔류도 결과, 명도가 낮아지기 때문에 피막이 관찰되는 것으로 판단된다. 용출량은 $50^{\circ}C$ 증류수에서 제니핀 첨가량이 증가할수록 용출된 아교 양이 증가하였고 파단강도는 제니핀 첨가량에 따라 증가하였다. 내수성과 내광성은 제니핀 첨가에 따른 열화 전 후 양상이 나타나지 않았다. 본 연구 결과를 바탕으로 제니핀 첨가 아교의 접착 특성을 확인할 수 있었으며 아교에 적용 가능한 실험 방법을 고찰하였다. 제니핀을 첨가한 후에도 아교 고유의 특성인 유연성, 재용해성, 접착력, 경화속도가 사라지지 않고 향상되기 때문에 균질한 아교가 확보된다면 문화재 보존 및 아교 제작에 적용이 가능할 것으로 기대한다.

포대단위 곡물건조방법의 개발에 관한 연구 (A Study on Development of Drying Method of Paddy Rice in Sack)

  • 서상룡;최재갑
    • 한국농공학회지
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    • 제17권4호
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    • pp.3980-3990
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    • 1975
  • This study was carried out to develop a method of grain drying ststem that can be done by forcing the heated-air directly into the grains within the sack. The air duct was pushed into the central position of the grain-deposited sack and the heated-air was forced to flow in the radial direction. The system is referred here as the unit sack drying system. At a first step of this study, an air flow resistance tester was constructed to measure the resistance of air flow to grains in cooperated with some different sack materials, the sack materials, the tested were rice-straw bag, sack of polyethylene film, and jute sack In addition, unit sack drying system was constructed to investigate the drying characteristics of the dryer. on this dryer, two kind of terminal air ducts were attached and tested to examine its effects on uniform drying, and also, aseries of drying test was performed to trace the effect of increasing air flow rate on uniform drying. The results are as follows: 1) Resistance of air flow for each sack material was increased almost proportional to the increasing rate of air flow. Experimental data showed little significant differences of the air flow resistance among the materials. 2) From the comparison with air flow resistance of sack material and that of roughrice, it was indicated that airflow resistance of sack material was much higher than that of rice rough Therefore, in the unit sack drying sysle in which air flow is destined to face the sach material after leaving the grain, it was suggested that air flow would be inuniform to each part of grain within sack because of much higher air flow resistance of sack material than that of grain, and the fact would results inuniform grain drying. 3) Drying test on the unit sack drying system in cooperated with different type of terminal air ducts showed that high speed air is better for uniform drying than in high pressure. with the drying system which was assembled with the air ducts delivering higher speed air, there also involved a problem of significant inuniform drying. Therefore, any means to improve the inuniform drying should be undertaken for practical use. 4) A series of drying test with in creasing air flow rate resulted that increasing air flow rate in the unitsack drying system gave little effect on uniform drying, therefore, it is recommened to change its drying system for drying grain uniformly.

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미분층반응기에서 양이온 교환수지에 의한 카드뮴(II)의 제거 (Removal of Cd(II) by Cation Exchange Resin in Differential Bed Reactor)

  • 김종태;정재관
    • 대한환경공학회지
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    • 제22권7호
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    • pp.1193-1203
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    • 2000
  • 본 연구는 흡착에 의한 Cd(II)의 제거를 위하여 일본 Diaion사에서 제조되고 있는 강산성양이온 교환수지(SK1B)를 흡착제로 사용하여 흡착평형실험, 탈착실험 및 흡착속도실험을 수행하였다. 흡착평형실험에서는 흡착능에 미치는 pH와 온도의 영향을 알아보았고 흡착등온식을 산출하였으며, 탈착실험에서는 재생회수에 대한 수지의 재생율의 변화에 대해서 알아보았다. 흡착속도실험에서는 수지를 미분층 반응기에 채워 유량별로 초기제거속도를 구하여 경막저항이 최소가 되는 최적유량을 구하였으며, 이 최적유량에서 흡착속도실험을 수행하여 총괄흡착속도식을 구하였다. 용액의 pH를 변화(2~7)시켜 제조하여 수지를 투여한 결과 pH가 증가할수록 흡착능이 증가하였으며 pH 6 이상에서는 흡착능이 일정한 경향을 나타내었다. 흡착능에 미치는 온도의 영향은 $10{\sim}50^{\circ}C$ 범위에서 온도가 증가할수록 흡착능도 증가함을 알 수 있었다. 회분식실험을 통해 얻은 자료를 각 흡착등온식에 적용해 본 결과 본 실험의 농도 영역(5~15ppm)에서는 Freundlich 흡착등온식과 Sips 흡착등온식이 Langmuir 흡착등온식보다 더 %편차가 적었다. 탈착제로서 0.01~2N 농도의 HCl 수용액을 사용할 경우에는 탈착제의 농도가 진할수록 흡착제의 재생율이 높았으며 재생 반복회수가 늘어날수록 재생율이 약간씩 감소하였다. 미분층 반응기를 이용한 연속공정실험($25{\pm}5^{\circ}C$)에서 경막확산저항이 최소가 되는 최적유량 $564m{\ell}/min$에서 수행한 수지에 대한 Cd(II) 수용액의 총괄흡착속도식은 다음과 같이 표현될 수 있다. $r=1.3785C_{fc}^{1.2421}-2.0907{\times}10^{0.0746C_i}\;q_e^{0.0121C_i-0.0301}$

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Biocompatibility of Poly(MPC-co-EHMA)/Poly(L-1actide-co-glycolide) Blends

  • Gilson Khang;Park, Myoung-Kyu;Jong M. Rhee;Lee, Sang-Jin;Lee, Hai-Bang;Yasuhiko Iwasaki;Nobuo Nakabayashi;Kazuhiko Ishihara
    • Macromolecular Research
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    • 제9권2호
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    • pp.107-115
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    • 2001
  • Poly(L-lactide-co-glycolide)(PLGA) was blended with poly[$\omega$-methacryloyloxyethyl phospho-rylcholine-co-ethylhexylmethacrylate (PMEH)] (PLGA/PMEH) to endow with new functionality i.e., to improve the cell-, tissue- and blood-compatibility. The characteristics of surface properties were investigated by measurement of contact angle goniometer, Fourier-transform infrared spectroscopy with attenuated total reflectance (FTIR-ATR) and electron spectroscopy for chemical analysis (ESCA). NIH/3T3 fibroblast and bovine aortic endothelial cell were cultured on control and PLGA/PMEH surfaces for the evaluation of ceil attachment and proliferation in terms of surface functionality such as the concentration of phosphoryl-choline. Also, the behavior of platelet adhesion on PLGA/PMEH was observed in terms of the surface functionality. The contact angles on control and PLGA/PMEH surfaces decreased with increasing PMEH content from 75$^{\circ}$ to about 43$^{\circ}$. It was observed from the FTIR-ATR spectra that phosphorylcholine groups are gradually increased with increasing blended amount of MPC. The experimental P percent values from ESCA analysis were more 3.28∼7.4 times than that of the theoretical P percent for each blend films. These results clearly indicated that the MPC units were concentrated on the surface of PLGA/PMEH blend. The control and PLGA/PMEH films with 0.5 to 10.0 wt% concentration of PMEH were used to evaluate cell adhesion and growth in terms of phosphorylcholine functionality and wettability. Cell adhesion and growth on PLGA/PMEH surfaces were less active than those of control and both cell number decreased with increasing PMEH contents without the effect of surface wettability. It can be explained that the fibronectin adsorption decreased with an increase in the surface density of phosphorylcholine functional group. One can conclude the amount of the protein adsorption and the adhesion number of cells can be controlled and nonspecifically reduced by the introduction with phosphorylcholine group. Morphology of the adhered platelets on the PLGA/PMEH surface showed lower activating than control and the number of adhered platelets on the PLGA/PMEH sample decreased with increasing the phosphorylcholine contents. The amount of fibrinogen adsorbed on the PLGA/PMEH surface demonstrated that the phospholipid polar group played an important role in reducing protein adsorption on the surface. In conclusion, this surface modification technique might be effectively used PLGA film and scaffolds for controlling the adhesion and growth of cell and tissue, furthermore, blood compatibility of the PLGA was improved by blending of the MPC polymer for the application of tissue engineering fields.

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Precision-TPA를 이용한 구치부 회전시 근심 및 원심삽입법에 따른 동적인 치아이동 양상에 관한 실험 연구 (An experimental study on the dynamic teeth movement of 3 types of the insertion method of Precision-TPA for derotating the posterior teeth)

  • 양성재;정성권;노준;전윤식
    • 대한치과교정학회지
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    • 제29권4호
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    • pp.425-433
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    • 1999
  • 회전된 구치를 개선시키기 위해 사용하는 precision-TPA(transpalatal arch)를 삽입 방법들-근심삽입법, 원심삽입법, 확장력을 부여한 근심삽입법(이하 근심확장법) -에 따라 동적인 치아이동의 양상과 치열궁의 변화를 비교하기 위해 본교실에서 개발, 제작한 Calorific machine을 이용하여 실험한 후 회전된 치아와 고정치간의 이동양상을 계측하여 통계처리한 결과 다음과 같은 결론을 얻었다. 1. 구치간 폭경은 근심삽입법에 의해 감소하였고, 원심삽입법과 근심확장법에 의해서는 증가하였다. 2. 원심삽입법에 의해서 치열궁 장경이 가장 증가하였고, 근심확장법, 근심삽입법 순으로 증가하였다. 3. 근심삽입법의 회전중심은 근심소와(mesial pit)와 중심소와(central pit)사이에 위치하였고, 원심삽입법에서는 원심소와(distal pit)와 원심설측교두(distolingual cusp)사이에, 근심확장법은 원심소와(distal pit)에 위치하였다.

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하악지 길이증가를 위한 수술방법들간의 회귀현상에 관한 실험적 연구 (EXPERIMENTAL STUDY ON RELAPSE AFTER RAMAL LENGTHENING IN DIFFERENT SURGICAL METHODS - RADIOGRAPHIC EVALUATION)

  • 이충국;장현호;박정현
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • 제26권6호
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    • pp.636-643
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    • 2000
  • Facial asymmetry is the most frequent disease in craniofacial deformities. And the primary causing area of that is mostly placing in mandible. That is to say, it is known that primarily, mandible grows excessively or deficiently, and other facial region involving maxilla undergoes compensatory growth secondarily, so asymmetric face develops. In facial asymmetry, the surgical correction of undergrowth is more difficult than that of overgrowth and the reason of it is the postoperative relapse caused by stress of surrounding soft tissues. It means the stress of surrounding soft tissues occurring after bone lengthening and reducing above stress is the same meaning with reducing postoperative relapse. Among various areas, mandibular ramus is the most difficult area to lengthen vertically and maintain its length. The reason of it is considered by many authors as the stress of surrounding pterygomasseteric sling which is enveloping lower border of mandible and interrupting elongation of ramal height. So we applied two different surgical procedures in which pterygomasseteric slings have different stress respectively to monkeys which have similar masticatory function and anatomy to human being and compared relapse by radiographic film and observed periodically the histochemical change of masseteric muscle fiber. So we could see the following results. The relapse was less in EVRO group in which we separated pterygomasseric sling in inferior border and didn't approximate muscle sling after vertical lengthening to minimize the stress of soft tissues than IVRO group in which we elongated ramal height preserving pterygomassetric sling. Of course, we could see a problem in EVRO group such as bone resorption in inferior border caused by uncovering the periosteum of inferior border. But we expect that such problem will be solved by developing periosteum substitutes for covering the exposed bone and minimizing the surgical trauma. In histochemical study of masseteric muscle fiber, the fiber constituents of EVRO group in which we minimized soft tissue stress was changed immediately after operation and maintained it for 1 year, whereas that of IVRO group in which we preserved soft tissue stress was changed in more portion after operation and recovered it by 1 year. By the histochemical results, we can see that the recovery of fiber constituents reflect the recovery of muscle stress and it is closely related with relapse phenomenon.

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