• 한국정밀공학회지
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• 제24권9호
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• pp.68-75
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• 2007

The pitch and orthogonality of two-dimensional (2D) gratings have been measured by using a metrological atomic force microscope (MAFM) and measurement uncertainty has been analyzed. Gratings are typical standard artifacts for the calibration of precision microscopes. Since the magnification and orthogonality in two perpendicular axes of microscopes can be calibrated simultaneously using 2D gratings, it is important to certify the pitch and orthogonality of 2D gratings accurately for nano-metrology using precision microscopes. In the measurement of 2D gratings, the MAFM can be used effectively for its nanometric resolution and uncertainty, but a new measurement scheme was required to overcome some limitations of current MAFM such as nonnegligible thermal drift and slow scan speed. Two kinds of 2D gratings, each with the nominal pitch of 300 nm and 1000 nm, were measured using line scans for the pitch measurement of each direction. The expanded uncertainties (k = 2) of measured pitch values were less than 0.2 nm and 0.4 nm for each specimen, and those of measured orthogonality were less than 0.09 degree and 0.05 degree respectively. The experimental results measured using the MAFM and optical diffractometer were coincident with each other within the expanded uncertainty of the MAFM. As a future work, we also proposed another scheme for the measurements of 2D gratings to increase the accuracy of calculated peak positions.

• International Journal of Precision Engineering and Manufacturing
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• 제9권2호
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• pp.18-22
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• 2008

The pitch and orthogonality of two-dimensional (2-D) gratings were measured using a metrological atomic force microscope (MAFM), and the measurement uncertainty was analyzed. Gratings are typical standard devices for the calibration of precision microscopes, Since the magnification and orthogonality in two perpendicular axes of microscopes can be calibrated simultaneously using 2-D gratings, it is important to certify the pitch and orthogonality of such gratings accurately for nanometrology. In the measurement of 2-D gratings, the MAFM can be used effectively for its nanometric resolution and uncertainty, but a new measurement scheme is required to overcome limitations such as thermal drift and slow scan speed. Two types of 2-D gratings with nominal pitches of 300 and 1000 nm were measured using line scans to determine the pitch measurement in each direction. The expanded uncertainties (k = 2) of the measured pitch values were less than 0.2 and 0.4 nm for each specimen, and the measured orthogonality values were less than $0.09^{\circ}$ and $0.05^{\circ}$, respectively. The experimental results measured using the MAFM and optical diffractometer agreed closely within the expanded uncertainty of the MAFM. We also propose an additional scheme for measuring 2-D gratings to increase the accuracy of calculated peak positions, which will be the subject of future study.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2005년도 추계학술대회 논문집
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• pp.405-406
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• 2005

• 한국전자파학회논문지
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• 제13권1호
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• pp.47-52
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• 2002

1993년도 ISO에서 \"Guide to Expression of Uncertainty in Measurement\"를 발표함으로써 측정과학에 있어 측정결과의 오차분석 방법을 폐기하기로 사실상 선언하였다. 그리하여 측정의 소급성과 신뢰성을 확보한다는 전제 하에 오차의 개념을 버리고 측정시의 측정불확도를 분석하는 것이 측정과학에 있어서 세계적인 추세이다. 본 논문에서는 전달표준인 열 전압변환기를 사용하여 고주파전압계의 정밀 교정에서 불확도를 산출하기 위하여 수학적 모델을 설정하고 측정에 관계되는 모든 불확도 요인을 분석하였다. 케이블의 영향과 열전대감지기와 직류전압계의 상관관계, 직류소스, RF소스, 감쇠기, 반사계수와 DUT 등 측정에 있어서 관계되는 모든 불확도요인을 분석하여 확장불확도를 산출하였다.확도를 산출하였다.

• 해양환경안전학회지
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• 제26권3호
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• pp.269-276
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• 2020

Sea trial tests are necessary to verify speed-power performance, and are an import contract between ship owners and shipyards. The International Organization for Standardization (ISO) published ISO 15016:2015, which specifies the correlation method between model and full-scale ships. The results of sea trials have been questioned because of the uncertainty of speed and power measurements, especially when sea conditions differ from ideal calm water conditions. In this paper, such uncertainties were investigated by utilizing the standard speed-power trial analysis procedure defined in ISO 15016:2015 through Monte Carlo simulations. It was found that the expanded uncertainty of the delivered power (P_Did) at 95 % confidence interval (k = 2) was ±1.5 % under 75 % MCR conditions.

• Bulletin of the Korean Chemical Society
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• 제34권8호
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• pp.2394-2398
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• 2013

Nicotine is the main component of environmental tobacco smoke, and its presence in indoor air is widely used as a secondhand-smoke indicator. Environmental tobacco smoke is a major source of indoor air pollution, but sufficient investigation of the uncertainty of its measurement, which mirrors the reliability of nicotine measurement, has not been performed. We calculated the uncertainty of measurement of indoor air nicotine concentration at low, medium, and high concentrations of 11.3798, 10.1977, $98.3768{\mu}g/m^3$, respectively, and we employed the Guide to the Expression of Uncertainty in Measurements (GUM), proposed by the International Organization for Standardization (ISO). The factors considered in determining the uncertainty were uncertainty of the calibration curve (calibration curve and repeated measurements), desorption efficiency, extraction volume, and sampling airflow (accuracy and acceptable limits of flowmeter). The measurement uncertainty was highest at low concentrations; the expanded measurement uncertainty is $0.9435{\mu}g/m^3$ and is represented as a relative uncertainty of 63.38%. At medium and high (concentrations, the relative uncertainty was 13.1% and 9.1%, respectively. The uncertainty of the calibration curve was largest for low indoor nicotine concentrations. To increase reliability of measurement in assessing the effect of secondhand smoke, measures such as increasing the sample injection rate ($1{\mu}L$ or more), increasing sampling volume to increase collected nicotine, and using gas chromatography-mass spectrometry (GC/MS) or GC/MS/MS, which has a lower quantitation threshold, rather than gas chromatography with nitrogen phosphorous detector, should be considered.

• 한국진공학회지
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• 제10권2호
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• pp.173-181
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• 2001

1,333 Pa 용량의 용량형진공계를 저진공 국가표준기인 초음파간섭 수은주압력계(ultrasonic interferometer manometer)를 이용하여 교정하였다. 이 결과의 불확도를 국제표준화기구의 권고안의 A형 불확도, B형 불확도, 합성표준불확도, 확장불확도 등으로 구분하여 평가하였다. 표준압력 1.76 Pa~1.31$\times$$10^3$Pa에서의 합성표준불확도는 $1.38 \times10^{-2}\; Pa\sim3.03 \times10^{-1} $Pa이었으며, 상대불확도(합성표준불확도/표준압력)는 $2.3 \times 10^{-4}\;Pa\sim7.9 X\times10^{-3} $Pa 이었다.

• 드라이브 ㆍ 컨트롤
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• 제20권1호
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• pp.34-40
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• 2023

The agricultural tractor ROPS test method according to OECD code 4 is a test to assess whether the driver's safety area can be secured when a tractor overturns, and reliability should be ensured. In this study, a model formula and procedure for calculating measurement uncertainty expressing reliability in the field of agricultural machinery testing were established according to the ISO/IEC Guide 98-3:2008. The characteristics of the ROPS test device were assessed and repeated tests were performed, and the were used as factors to calculate the measurement uncertainty. As a result of repeated tests, the accuracy was higher than 1.9 % in all load directions; thus, they were, applied to calculate the type A standard uncertainty. The final expanded uncertainty was calculated within the range of less than ± 7.76 kN of force and ± 6.96 mm of deformation in all load directions.

• 대한환경공학회지
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• 제30권11호
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• pp.1123-1131
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• 2008

본 연구는 대기 중 PM2.5의 미량금속 중 As을 중성자방사화분석법을 이용하여 분석할 때 발생되는 측정불확도를 ISO GUM 방법과 MCS 방법을 모두 적용하여 비교, 평가하였다. 불확도의 요인은 ISO GUM을 엄격하게 준용하여 파악하였으며 특정일에 채취된 PM2.5 내 As 농도에 대해 두 방법의 계산 결과가 4% 미만으로 크게 다르지 않는 것으로 나타났다. 연구기간 중 채취된 총 60개의 PM2.5 시료에 대해 As 농도의 확장불확도를 역시 MCS 방법을 이용하여 산출하였는데, 연구지역에서의 As의 개별 농도값에 대한 95% 신뢰구간의 확장불확도는 대부분 10%의 범위에서 존재하는 것으로 나타났다. 확장불확도에 대한 표준불확도 요인의 기여율은 계측통계오차(62.3%), 검출효율(18.5%), 시료 채취 시 유량(12.3%), flux 변동(2.3%), 특정감마선 방출률(1.8%) 등의 순으로 크게 나타났다.

• 한국태양에너지학회 논문집
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• 제36권4호
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• pp.11-20
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• 2016

For accurate wind resource assessment and wind turbine performance test, it is essential to secure wind data covering a rotor plane of wind turbine including a hub height. In general, we can depict wind speed profile by extrapolating or interpolating the wind speed data measured from a meteorological tower where multiple anemometers are mounted at different heights using a power-law of wind speed profile. The most important parameter of a power-law equation is a vertical wind profile exponent which represents local characteristics of terrain and land cover. In this study, we calculated diurnal vertical wind profile exponents of 8 locations in Jeju Island who possesses excellent wind resource according to the GUM (Guide to the Expression of Uncertainty in Measurement) to evaluate its uncertainty. Expanded uncertainty is calculated by combined standard uncertainty, which is the result of composing type A standard uncertainty with type B standard uncertainty. Although pooled standard deviation should be considered to derive type A uncertainty, we used the standard deviation of vertical wind profile exponent of each day avoiding the difficult of uncertainty evaluation of diurnal wind profile variation. It is anticipated that the evaluated uncertainties of diurnal vertical wind profile exponents at 8 locations in Jeju Island are to be registered as a national standard reference data and widely used in the relevant areas.