• 대한전기학회:학술대회논문집
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• 대한전기학회 2008년도 제39회 하계학술대회
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• pp.1268-1269
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• 2008

$CuInS_2$ thin films were fabricated by sulpurization of Cu/In Stacked elemental layer deposited onto glass substrates by vacuum annealing at various temperatures. And structural and electrical properties were measured in order to certify optimum conditions for growth of the ternary compound semiconductor $CuInS_2$ thin films by composition ratio. Physical properties of the thin film were investigated at various fabrication conditions; substrate temperature, annealing temperature and annealing time by XRD, FE-SEM and hall measurement system. $CuInS_2$ thin film was well made at the heat treatment 200[$^{\circ}C$] of SLG/Cu/In/S stacked elemental layer.

• 분석과학
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• 제15권4호
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• pp.335-340
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• 2002

유도결합 플라스마 질량분석법 (ICP-MS)을 이용하여 모발 중 다원소 동시 정량법을 확립하였다. 0.05 g의 모발 시료에 내부표준물질인 In을 가하고 질산 1.5 mL와 함께 테플론 가압분해 용기에 넣어 마이크로파를 이용하여 분해하는 시료전처리법을 사용하였다. 측정값의 정확도 및 신뢰도를 확인하기 위하여 모발 인증표준물질인 GBW 09101을 반복 분석하였는데 측정값은 인증값과 불확도 범위 내에서 잘 일치하는 결과를 얻었다.

• Asian Journal of Atmospheric Environment
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• 제11권1호
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• pp.54-60
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• 2017

Quantifying the trace elements in infinitesimal ambient liquid samples (e.g., single raindrop, cloud/fog water, and the soluble fraction extracted from the particles collected for a short time) is an important task for understanding formation processes, heating/cooling rates, and their health hazards. The purpose of this study is to employ an in-air micro PIXE system for quantitative analysis of the trace elements in a thimbleful of reference liquid sample. The bag type liquid sample holder originally designed with $10{\mu}m$ thick $Mylar^{(R)}$ film retained the original shape without any film perforation and apparent peaks of film blank by the end of the analysis. As one of tasks to be solved, the homogeneity of the elemental distribution in liquid reference species was verified by the X-ray line profiles for several references. It was possible to resolve the significant peaks for whole target elements corresponding to the channel number of micro-PIXE spectrum. The calibration curves for the six target elements (Si, S, Cl, Fe, Ni, and Zn) in standard solutions were successfully plotted by concentration (ppm) and ROI of interest net counts/dose (nC).

• Environmental Engineering Research
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• 제23권3호
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• pp.265-270
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• 2018

This study was to measure the exposure of diesel vehicle drivers to elemental carbon (EC) as an indicator of diesel particulate matter (DPM) emitted from diesel vehicles in an underground coal mine over 3 years as per NIOSH Method 5040. Our study results (range $10{\mu}g/m^3-377{\mu}g/m^3$ for the loader drivers, $19{\mu}g/m^3-162{\mu}g/m^3$ for the SMV drivers) were similar or less than previous study results (range $5{\mu}g/m^3-2,200{\mu}g/m^3$) for normal mine operations. From this study results, it appeared that the exposures decreased in the second and the third year. It is thought that the reasons for the decreased personal DPM (EC) exposures over the 3 years were related to the following recommendations; more frequent monitoring and maintenance of the diesel vehicles and their DPM filtration systems, more consistent monitoring of the mine's ventilation system and changes of work practices such as minimizing the opening of diesel vehicle windows. An educational program on adverse health effects of exposure to DPM and use of respiratory protection (P2 respirators) also assisted in minimizing driver exposure to DPM.

• Mass Spectrometry Letters
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• 제9권4호
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• pp.105-109
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• 2018

A certified reference material (CRM) for the analysis of inorganic nutrients in nutritional supplements has been developed. Accurate mass fractions of chromium (Cr), iron (Fe), copper (Cu), and zinc (Zn) were determined by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). The measurement results were used to assign certified values for the CRM, which were metrologically traceable to the definitions of the measurement units in the International System of Units (SI). Production of a candidate reference material (RM) and the certification processes are summarized. Each nutrient in the CRM showed good homogeneity, which was estimated using relative standard deviations of the measurement results of twelve bottles in a batch. This CRM is expected to be an important reference to improve reliability and comparability of nutrient analyses in nutritional supplements and related samples in analytical laboratories.

• 분석과학
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• 제20권6호
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• pp.524-528
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• 2007

Variations of the twenty one metal components (Mg, Al, V, Cr, Co, Sr, Ba, Na, K Mn, Fe, Cu, Zn, As, Hg, Pb, Ca, P, Mo, Cd, Sb) were analyzed in human hair sample by inductively coupled plasma mass spectrometry (ICP-MS). The effect of bleach and permanent wave manipulation on the elemental composition of hair were investigated. It was found that the composition of hair varied with hair bleach and permanent wave. Hair sample was collected from male in the age of thirties. Hair sample (0.05 g) was added to the Teflon digestion bomb together with 1.5 mL of nitric acid and an appropriate amount of In as an internal standard. The sample was then decomposed in the microwave digestion system. In normal hair, the contents of V, Cr, Mn, Fe, Co, Cu, Zn, As, Mo, Cd, Sb and P were increased in permanent wave hair, and Mg, Al, V, Co, Sr, Ba, Na and K were increased in bleached hair. But Mg, Al, Sr, Ba, Hg, Pb, Na, K, and Ca contents were decreased with permanent wave hair, Mn, Fe, Cu, Zn, As, Hg, Pb and Ca contents were decreased with bleached hair.

• 대한치과기공학회지
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• 제31권1호
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• pp.55-61
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• 2009

Passive fitting of meso-structure and super-structures is a predominant requirement for the longevity and clinical success of osseointegrated dental implants. However, precision and passive fitting has been unpredictable with conventional methods of casting as well as for corrective techniques. Alternative to conventional techniques, electro discharge machining(EDM) is an advanced method introduced to dental technology to improve the passive fitting of implant prosthesis. In this technique material is removed by melting and vaporization in electric sparks. Regarding the efficacy of EDM, the application of this technique induces severe surface morphological and elemental alterations due to the high temperatures developed during machining, which vary between $10,000{\sim}20,000^{\circ}C$. The aim of this study was to investigate the morphological and elemental alterations induced by EDM process of casting dental gold alloy and non-precious alloy used for the production of implant-supported prosthesis. A conventional clinical dental casting alloys were used for experimental specimens patterns, which were divided in three groups, high fineness gold alloy(Au 75%, HG group), low fineness gold alloy(Au 55%, LG group) and nonprecious metal alloy(Ni-Cr, NP group). The UCLA type plastic abutment patterns were invested with conventional investment material and were cast in a centrifugal casting machine. Castings were sandblasted with $50{\mu}m\;Al_2O_3$. One casting specimen of each group was polished by conventional finishing(HGCON, LGCON, NPCON) and one specimen of each group was subjected to EDM in a system using Cu electrodes, kerosene as dielectric fluid in 10 min for gold alloy and 20 min for Ni-Cr alloy(HGEDM. LGEDM, NOEDM). The surface morphology of all specimens was studied under an energy dispersive X-ray spectrometer (EDS). The quantitative results from EDS analysis are presented on the HGEDM and LGEDM specimens a significant increase in C and Cu concentrations was found after EDM finishing. The different result was documented for C on the NPEDM with a significant uptake of O after EDM finishing, whereas Al, Si showed a significant decrease in their concentrations. EDS analysis showed a serious uptake of C and Cu after the EDM procedure in the alloys studied. The C uptake after the EDM process is a common finding and it is attributed to the decomposition of the dielectric fluid in the plasma column, probably due to the development of extremely high temperatures. The Cu uptake is readily explained from the decomposition of Cu electrodes, something which is also a common finding after the EDM procedure. However, all the aforementioned mechanisms require further research. The clinical implication of these findings is related with the biological and corrosion resistance of surfaces prepared by the EDM process.

• 한국수자원학회논문집
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• 제43권2호
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• pp.153-165
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• 2010

Large-Scale Particle Image Velocimetry (LSPIV)는 Particle Image Velocimetry (PIV)를 실험실내의 비교적 규모가 큰 흐름이나 하천에서의 표면유속장의 측정 등 넓은 영역에 적용할 수 있도록 확장시킨 것이다. LSPIV는 PIV의 구성요소를 포함하여 추적자 투하, 조명, 촬영, 이미지 변환, 이미지 처리 및 후처리의 여섯 단계로 구성된다. 본 연구에서는 LSPIV의 모바일 버전인 MLSPIV를 이용하여 하천에서의 유속측정시 각 단계별로 발생가능한 오차성분을 정의하였고, 기존의 연구 결과를 바탕으로 오차의 영향이 정량적으로 밝혀진 것을 정리하였다. 각 단계별로 오차 발생요인을 조사한 결과 27개의 성분오차성분을 파악하였다. 이중에서 5개의 오차요소는 기존에 연구가 진행되었고, 7개의 오차요소는 본 논문에서 적용시의 MLSPIV에는 그 효과가 미치지 않는 것으로 파악하였다. 나머지 15개의 오차성분 중 4가지 오차성분- 샘플링시간, 이미지 해상도, 추적자의 성질, 바람-에 대해서 유속산정시 미치는 영향을 파악하기 위하여 개수로 실험장치를 이용한 실내시험을 실시하였다. 이미지 프로세싱에 이용한 이미지수로부터 나타나는 유속계산 오차를 조사한 결과 이미지의 개수가 50매 이상인 경우는 이로 인한 오차가 1 % 이하로 감소함을 파악하였다. 촬영된 이미지의 해상도가 유속계산시 미치는 영향을 조사하기 위해 세 가지 이미지 해상도로 변화시키면서 유속측정 오차를 분석한 결과 저해상도의 이미지를 이용한 경우 고해상도 이미지를 이용한 경우와 비교하여 3 % 가량의 차이를 나타내었다. 추적자의 성질과 바람의 영향에 대해서는 흐름의 평균유속이 큰 경우에는 바람이 추적자에 마치는 영향이 현격히 줄어듬을 보이고 있다. 즉, 유속이 증가함에 따라 바람의 영향은 감소하나, 바람의 영향을 최소화시키기 위해서는 가급적 비중이 큰 물질(0.5

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2016년도 추계 학술논문 발표대회
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• pp.140-141
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• 2016

Dynamic nature and diverse requirements on construction sites make the automation technology harder to be employed actively. In this study, we analyzed optimal type of automation system and importance of core technologies for developing efficient construction automation system on 11 construction operations. As a result, it showed that man-machine cooperation system may be the most suitable for most operations, while autonomous robot will be best suited in hard working environment such as maintenance of exterior wall. In elemental technology, ease and accuracy of control and operation showed higher priority than others regardless of automation system type. These findings will provide useful information for developing the construction automation system.

• 한국정보통신학회논문지
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• 제15권12호
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• pp.2664-2669
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• 2011

본 논문에서는 커브형 집적영상 시스템에서 먼 거리 물체의 해상도를 향상하는 방법을 제안한다. 커브형 집적영상은 비록 기존의 집적영상보다 향상된 샘플링 비율 때문에 더 많은 요소영상을 픽업 할 수 있지만, 먼 거리 물체에 대한 샘플링 효율이 여전히 낮은 원인 때문에 픽업된 요소영상으로 물체를 재생하면 해상도가 낮은 문제점이 있다. 이러한 문제점을 해결하기 위하여 본 논문에서는 커브형 집적영상 시스템에서 픽업된 원 요소영상에 다이렉트 픽셀매핑 방법을 적용하여, 먼 거리에 위치한 물체를 마치 가까이에서 픽업한 것과 같은 새로운 요소영상을 생성한다. 이 새로운 요소영상을 이용하여 커브형 집적영상 시스템에서 최종 해상도가 향상된 물체의 영상을 재생하게 된다. 실험결과에서 기존 방법과의 비교를 통하여 제안방법의 유용성을 검증하였다.