• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2004년도 춘계학술강연 및 발표대회 강연 및 발표논문 초록집
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• pp.21-21
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• 2004

• 분석과학
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• 제32권4호
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• pp.121-130
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• 2019

Alumina is one of the most important ceramic materials because of its useful physical and chemical properties. Recently, high-purity alumina has been used in various industrial fields. This leads to increasing demand for reliable elemental analysis of impurities in alumina samples. However, the chemical inertness of alumina makes the sample preparation for conventional elemental analysis a tremendously difficult task. Herein, we demonstrated the feasibility of laser ablation for effective sampling of alumina powder. Laser ablation performs sampling rapidly without any chemical reagents and also allows simultaneous optical emission spectroscopy and mass spectrometry analyses. For six alumina samples including certified reference materials and commercial products, laser-induced breakdown spectroscopy (LIBS) and laser-ablation inductively-coupled plasma mass spectrometry (LA-ICP-MS) analyses were performed simultaneously based on a common laser ablation sampling. LIBS was found to be useful to quantify alkali and alkaline earth metals with limits-of-detection (LODs) around 1 ppm. LA-ICP-MS could quantify transition metals such as Ti, Cu, Zn, and Zr with LODs in the range from a few tens to hundreds ppb.

• 한국정밀공학회지
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• 제15권2호
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• pp.28-34
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• 1998

Powder metallurgy processes are able to form Net-Shape products and have been widely used in the production of automobile parts to improve its productivity. However, because of pores in powder products, the toughness of powder products are generally poor. Therefore, forged products are used in parts which suffer severe fatigue loads. In this paper, the choice of powder materials and production processes such as mixing, compaction, sintering, heat treatment to produce automobile spline hub are studied. Three type of materials are selected and processed and its microstructure and properties are investigated by tensile test, compression ring test, and impact test. Materials and processing methods are selected from the results. Finally, experimental spline hubs are manufactured by selected processes from selected powders and proved by torsional durability test.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.722-723
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• 2006

A new method has been developed to fabricate microcomponents by a combination of photolithography and sintering of metallic powder mixtures, without the need for compression and the addition of Mg. This involves (1) the fabrication of a micromould, (2) mould filling of the powder/binder mixture, (3) debinding and (3) sintering. The starting powdered materials consisted of a mixture of aluminium powder(average size of 2.5 um) and alloying elemental powder of Cu and Sn(less than 70nm), at appropriate proportions to achieve nominal compositions of Al-6wt%Cu, Al-6wt%Cu-3wt%Sn. This paper presents detailed investigation of debinding behaviour and microstructural development.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.568-569
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• 2006

The use of the nickel free, high nitrogen stainless steel powder and nitriding during sintering of iron based materials have been shown as an alternative way to the conventional PM stainless steels containing nickel. Nitrogen as an alloying element for iron improves in an effective way the properties of sintered alloyed steels. The powder metallurgy route is a suitable way to introduce nitrogen into these alloys and, in particular, to produce high nitrogen (close to the solubility limit) stainless steels. The paper presents and discusses the nitriding behavior of nickel-free stainless steels produced by powder metallurgy method. Alloyed melt was atomized by nitrogen and in this way nitrogen was introduced into the powder. Further nitriding occurred during sintering in a nitrogen atmosphere. For comparison, compacts having the same composition as an alloyed powder were produced from elemental powders mixture. Sintering-nitriding behaviour of investigated materials has been controlled by dilatometry, chemical and X-Ray phase analysis and metallography. Mechanical properties of sintered compacts were also measured.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1996년도 춘계학술대회 논문집
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• pp.206-211
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• 1996

Closed-die forging of external spine is analysed using an upper bound elemental technique. The kinematically admissible velocity field for three-dimensional deformation in forging of the external spine with trapezoidal teeth was obtained. The upper bound to the deforming load necessary and the the deformed configurations are predicted using integration of the formulation of energy expressions which were obtained from B(upset forging method) were considerd in the present analysis and the theoretical results compared with experimental ones Experiments were carried out on plasticine as model material at room temperature where talcum powder was used as a lubricant. The present investigation revealed that the analytical method B predicts a reducet forging load and improved configuration better than method A for the forged products.

• 한국분말재료학회지
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• 제3권1호
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• pp.13-24
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• 1996

Two grades of Permalloy strips, Fe-45Ni(PB) and Fe-78Ni-4Mo-5Cu(PC) were fabricated by powder rolling process from elemental powder mixtures. The roll compacted green strips were sintered, homogenized, cold rolled with or without an intermediate annealing and finally heat treated to measure magnetic properties. For a given thickness reduction, rolling with an intermediate annealing was found more effective to achieve a full densification with no visible micropores and also to obtain better magnetic properties. Increasing the final rolling reduction also produced a marked improvement of the magnetic properties whereas the cooling rate during the final heat treatment has little effect in both grades. Addition of a small amount, 0.4% Mn slightly degraded the properties. As an overall, The PM strips produced via powder rolling yielded the similar soft magnetic properties to the corresponding commercial grades produced via wrought processing.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.618-619
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• 2006

The binder phase for TiC reinforced steel matrix composite was added in the form of elemental powders and master alloy powders. The microstructures, binder phase variation with TiC content and mechanical properties were evaluated. The addition of a type of binder phase largely effects the microstructure and mechanical properties. The binder phase variation from starting composition was observed with increase in wt% TiC content and this variation was higher when the master alloy powders were used as a binder. The response to heat treatment was decreased with an increase in TiC content due to the shift of binder phase from the starting composition.

• 한국분말재료학회지
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• 제5권4호
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• pp.312-318
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• 1998

The effect of the mechanical alloying of elemental Mo and Si powders on the combustion densification behavior of MoSi$_2$ was investigated. The ignition temperature of the combustion reaction of the mechanically alloyed powder was measured to be significantly lower than that of the powder mixture prepared by the low energy ball milling process. The densification of the products after the combustion reaction under compressive pressure from the mechanically alloyed powders, however, was found to be poorer than that of the products from the ball milled powder.

• 한국분말재료학회지
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• 제4권1호
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• pp.42-47
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• 1997

It was investigated whether mechanical alloying (MA) processing could be more effective to the formation of metallic composite powder in Cu-C system. Elemental powder mixtures of Cu-70vo1.%C were mechanically alloyed with an attritor in an argon atmosphere and microstructural evolution was examined by X-ray diffraction analysis, scanning electron microscopy and transmission electron microscopy. It has been found that even with the high volume fraction of immiscible graphite in Cu-C system, the refinement with a few ten nanometer size as well as the highly uniform distribution of copper phases have been achieved by the MA processing.