• Title/Summary/Keyword: Electron backscatter diffraction

Search Result 55, Processing Time 0.018 seconds

Microfabrics of omphacite and garnet in eclogite from the Lanterman Range, northern Victoria Land, Antarctica

  • Kim, Daeyeong;Kim, Taehwan;Lee, Jeongmin;Kim, Yoonsup;Kim, Hyeoncheol;Lee, Jong Ik
    • Geosciences Journal
    • /
    • v.22 no.6
    • /
    • pp.939-953
    • /
    • 2018
  • We examined the microfabrics of omphacite and garnet in foliated eclogite to determine the influence of the layered structure on seismic observations in subduction zone. The analyzed eclogite, from the Lanterman Range, northern Victoria Land, Antarctica, is characterized by layering in which the modal abundances of garnet and omphacite vary. For garnet, the low aspect ratios, similar angular distribution of long axes relative to the foliation in both layers, uniform grain size distribution, near-random crystallographic preferred orientations (CPOs), and misorientation angle distributions are indicative of passive behavior during deformation. In contrast, omphacite shows relatively high aspect ratios, a low angle between the long axes of crystals and the foliation, a wide grain-size distribution, and distinctive CPOs, suggesting dislocation creep as the main deformation mechanism. The results of fabric analyses are consistent with strain localization into omphacite or omphacite-rich layers rather than garnet or garnet-rich layers. The single-crystal seismic anisotropy of garnet is very weak ($AV_P=0.2%$, $AV_S=0.5-0.6%$), whereas that of omphacite is much stronger ($AV_P=3.7-5.9%$ and $AV_S=2.9-3.8%$). Seismic anisotropy of the omphacite-rich layers shows an increase of 329% for $AV_P$ and 146% for $AV_S$ relative to the garnet-rich layers. Our results demonstrate the importance of the layered structure in strain localization and in the development of the seismic anisotropies of subducting oceanic crust.

Tensile and Charpy Impact Properties of High-Strength Bainitic Steels Fabricated by Controlled Rolling Process (제어압연한 베이나이트계 고강도강의 인장 및 충격 성질)

  • Sung, Hyo Kyung;Shin, Sang Yong;Hwang, Byoungchul;Lee, Chang Gil;Kim, Nack J.;Lee, Sunghak
    • Korean Journal of Metals and Materials
    • /
    • v.48 no.7
    • /
    • pp.615-624
    • /
    • 2010
  • This study is concerned with tensile and Charpy impact properties of high-strength bainitic steels fabricated by controlled rolling process. Six kinds of steels were fabricated by varying finish rolling temperature, start cooling temperature, and cooling rate, and their microstructures and tensile and Charpy impact properties were investigated. Their effective grain sizes were also characterized by the electron backscatter diffraction analysis. The microstructures of the steels rolled in the single phase region were most similar to those of the steels rolled in the two phase region. The steels cooled from $700{^{\circ}C}$ were composed mainly of granular bainites, while those cooled from $600{^{\circ}C}$ contained a number of bainitic ferrites, which resulted in the decrease in ductility and upper shelf energy in spite of the increase in strength. In the steels cooling from $600^{\circ}C$, fine acicular ferrites were well formed when the cooling rate was slow, which led to the best combination of high ductility, high upper shelf energy, and low energy transition temperature according to the decrease in the overall effective grain size due to the presence of acicular ferrites having smaller effective grain size.

Microstructure Evolution of Ti-6Al-4Fe-0.25Si through Aging Heat Treatment (시효처리에 따른 Ti-6Al-4Fe-0.25Si 합금의 미세조직 변화)

  • Song, Yong Hwan;Kang, Joo-Hee;Park, Chan Hee;Kim, Seong-Woong;Hyun, Yong-Taek;Kang, Nam Hyun;Yeom, Jong-Taek
    • Korean Journal of Metals and Materials
    • /
    • v.50 no.7
    • /
    • pp.477-485
    • /
    • 2012
  • The effect of aging heat treatment on microstructure evolution of the Ti-6Al-4Fe-0.25Si alloy with an initial microstructure of an elongated alpha was investigated. Aging treatments of the samples were carried out at $550^{\circ}C$ for up to 100 hours. The microstructure of the 5 hours heat-treated sample consisted of alpha grains, beta matrix and some TiFe intermetallic compounds that were precipitated from the beta matrix. Increasing the aging time to 10 hours, most of the beta matrix was decomposed to very fine alpha grains (${\sim}0.5{\mu}m$) and TiFe, and thus the volume fraction of the beta matrix was significantly decreased. EBSD analysis revealed that newly formed tertiary-alpha-grains in the vicinity of TiFe had high angle boundaries with respect to the primary and secondary alpha grains. As a result of these phase transformations during aging, the fraction of the alpha/alpha grain boundary was increased while that of the alpha/beta phase boundary was decreased.

Gradient Microstructure and Mechanical Properties of Fe-6%Mn Alloy by Different Sized Powder Stacking (다른 크기의 분말 적층을 통해 얻은 Fe-6%Mn합금의 경사 미세조직과 기계적 특성)

  • Seo, Namhyuk;Lee, Junho;Shin, Woocheol;Jeon, Junhyub;Park, Jungbin;Son, Seung Bae;Jung, Jae-Gil;Lee, Seok-Jae
    • Journal of Powder Materials
    • /
    • v.29 no.5
    • /
    • pp.382-389
    • /
    • 2022
  • A typical trade-off relationship exists between strength and elongation in face-centered cubic metals. Studies have recently been conducted to enhance strength without ductility reduction through surface-treatment-based ultrasonic nanocrystalline surface modification (UNSM), which creates a gradient microstructure in which grains become smaller from the inside to the surface. The transformation-induced plasticity effect in Fe-Mn alloys results in excellent strength and ductility due to their high work-hardening rate. This rate is achieved through strain-induced martensitic transformation when an alloy is plastically deformed. In this study, Fe-6%Mn powders with different sizes were prepared by high-energy ball milling and sintered through spark plasma sintering to produce Fe-6%Mn samples. A gradient microstructure was obtained by stacking the different-sized powders to achieve similar effects as those derived from UNSM. A compressive test was performed to investigate the mechanical properties, including the yielding behavior. The deformed microstructure was observed through electron backscatter diffraction to determine the effects of gradient plastic deformation.

Effects of Plastic Deformation on Surface Properties and Microstructure of Alloy 690TT Steam Generator Tube (증기발생기 전열관 Alloy 690TT의 소성변형이 표면특성 및 미세조직에 미치는 영향)

  • Soon-Hyeok Jeon;Ji-Young Han;Hee-Sang Shim;Sung-Woo Kim
    • Transactions of the Korean Society of Pressure Vessels and Piping
    • /
    • v.20 no.1
    • /
    • pp.16-24
    • /
    • 2024
  • Denting of steam generator (SG) tube is defined as the reduction in tube diameter due to the stresses exerted by the corrosion products formed on the outer diameter surface. This phenomenon is mostly observed in the crevices between SG tube and the top-of tubesheet or tube support plate. Despite the replacement of SG tube with Alloy 690, which has better corrosion resistance than Alloy 600, the denting of SG tube still remains a potential problem that could decrease the SG integrity. Deformation of SG tube by denting phenomenon can affect the surface properties and microstructure of SG tube. In this study, the effects of plastic deformation on surface properties and microstructure of Alloy 690 thermally treated (TT) tube was investigated by using the various analysis techniques. The plastic deformation of Alloy 690 increased the surface roughness and area. Many surface defects such as ripped surface and micro-cracks were observed on the deformed Alloy 690TT specimen. Based on the electron backscatter diffraction analysis, the dislocation density of deformed SG tube increased compared to non-deformed SG tube. In addition, the effects of changes in surface properties and microstructure of SG tube on general corrosion behavior were discussed.