• 제목/요약/키워드: Electrical impedance spectroscopy

검색결과 206건 처리시간 0.029초

전기 임피던스 분광법을 이용한 시멘트계 재료의 응결 특성 평가 (Setting Characteristic Assessment of Cementitious Materials using Electrical Impedance Spectroscopy)

  • 이준철;박인용
    • 한국건설순환자원학회논문집
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    • 제5권4호
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    • pp.474-480
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    • 2017
  • 본 연구에서는 전기 임피던스 분광법을 이용하여 시멘트계 재료의 응결 시점을 평가하였다. 시멘트 페이스트 시편을 제작한 후 전기노드를 매립하여 전기 임피던스 응답 스펙트럼의 변화를 연속적으로 모니터링하였으며, 이와 동시에 간이단열시험을 통한 수화온도측정과 비카트침 시험을 함께 수행하였다. 전기 임피던스 분광법에서는 시멘트 페이스트의 수화와 동시에 컨덕턴스가 서서히 증가하는 경향을 나타냈다. 이후, 특정시점에 이르러 컨덕턴스는 급격히 감소하는 경향을 나타냈으며, 이후 또다른 특정시점에서 완만하게 감소하는 경향을 나타냈다. 이러한 특정 시점은 간이단열시험 및 비카트침 시험에 의해 측정된 응결시점과 부합하는 것으로 나타났다. 이를 통해 전기 임피던스 분광법을 이용하여 시멘트계 재료의 응결을 효과적으로 모니터링하는 것이 가능하리라 판단된다.

임피던스 분석법을 이용한 유기발광 다이오드의 전기적 특성 분석 (Electrical property analysis of Organic Light Emitting Diodes using impedance spectroscopy)

  • 박재일;박형준;남은경;정동근;이준신
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 추계학술대회 논문집
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    • pp.452-453
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    • 2007
  • In this work, enhanced simulation is proposed by using impedance spectroscopy. The impedance spectroscopy is one of the popular methods to measure the electrical property of Organic Light Emitting Diodes. The results show that the equivalent circuit needs a inductance element linked by serial connection and the element of resistance is more important role to decide the electrical property.

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Impedance Spectroscopy Analysis of Hydration in Ordinary Portland Cements Involving Chemical Mechanical Planarization Slurry

  • Hwang, Jin-Ha
    • 한국세라믹학회지
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    • 제49권3호
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    • pp.260-265
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    • 2012
  • Impedance spectroscopy was used to monitor the hydration in the electrical/dielectric behaviors of chemical mechanical planarization (CMP)-blended cement mixtures. The electrical responses were analyzed using their equivalent circuit models, leading to the separation of the bulk and electrode based responses. The role of the CMP slurry was monitored as a function of the relative compositions of the CMP-blended cements, i.e. water, CMP slurry, and ordinary Portland cement. The presence of $Al_2O_3$ nanocrystals in the CMP slurries appeared to accelerate the hydration process, along with a more tortuous microstructure in the hydration, with enhanced hydration products. The frequency-dependent impedance spectroscopy was proven to be a highly efficient approach for evaluating the electrical/dielectric monitoring of the change in the pore structure evolution that occurs in CMP-blended cements.

온라인 임피던스 분광법을 이용한 배터리 진단 기능을 가진 3kW 충전기 (A 3kW Battery Charger with Battery Diagnosis Function Using Online Impedance Spectroscopy)

  • 도안반투안;최우진
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2014년도 추계학술대회 논문집
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    • pp.68-69
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    • 2014
  • In the battery based applications such as electric vehicle and energy storage system, the performance of the system highly depends on the reliability of the battery. However, it is difficult to obtain the accurate information about the state-of-health (SOH) of battery during its operation. In this paper a 3kw battery charger with battery diagnosis function which can estimate the SOH of the battery by using online impedance spectroscopy technique is introduced. For the charger phase shift full bridge converter with synchronous rectification has been adopted to implement the charge and diagnosis functions. The impedance spectroscopy is performed after the charge to obtain the information about the internal impedance of the battery module, hence the SOH can be estimated online by observing the impedance variation of the battery over time. All the design procedure of the proposed charger is detailed and the feasibility of the system is verified by the experimental results.

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Application of Impedance Spectroscopy to Cement-Based Materials: Hydration of Calcium Phosphate Bone Cements

  • Kim, Sung-Moon;Hwang, Jin-Ha
    • 한국세라믹학회지
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    • 제43권3호
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    • pp.156-161
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    • 2006
  • Impedance spectroscopy was applied to the initial hydration of calcium phosphate bone cements in order to investigate the electrical/dielectric properties. Hydration or equivalently setting was monitored as a function of the amount of water and initial powder characteristics. Higher amounts of water produced more open microstructures, leading to higher conductivity and enhanced dielectric constant. The effects of the initial characteristics in the powder were investigated using bone cement powder prepared with and without granulation. Granulated powder exhibited a significant change in resistance and produced a higher dielectric constant than those of conventional powder. Through a simplified modeling, the effects of thickness in reaction products and pore sizes were estimated by the frequency-dependent impedance measurements. Furthermore, impedance spectroscopy was proven to be a highly reliable tool for evaluating the continuous change in pore structure occurring in calcium phosphate bone cements.

전기화학적 임피던스 Fitting 개선을 위한 전극/전해질 계면의 전기회로 모델 연구 (A Study on the Electrical Circuit Model of the Electrode/Electrolyte Interface for Improving Electrochemical Impedance Fitting)

  • 장종현;박정호
    • 전기학회논문지
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    • 제56권6호
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    • pp.1087-1091
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    • 2007
  • Exact impedance modeling of the electrode/electrolyte interface is important in bio-signal sensing electrode development. Therefore, the investigation of the equivalent circuit models for the interface has been pursued for a long time by several researchers. Previous circuit models fit the experimental results in limited conditions such as frequency range, type of electrode, or electrolyte. This paper describes a new electrical circuit model and its capability of fitting the experimental results. The proposed model consists of three resistors and two constant phase elements. Electrochemical impedance spectroscopy was used to characterize the interface for Au, Pt, and stainless steel electrode in 0.9% NaCl solution. Both the proposed model and the previous model were applied to fit the measured impedance results for comparison. The proposed model fits the experimental data more accurately than other models especially at the low frequency range, and it enables us to predict the impedance at very low frequency range, including DC, using the proposed model.

Impedance spectroscopy analysis of the $Li_2CO3$ doped $(Ba,Sr)TiO_3$ thick films

  • 함용수;고중혁
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 추계학술대회 논문집
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    • pp.27-28
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    • 2009
  • In this study, we have fabricated the 3 wt% $Li_2CO3$ doped $(Ba,Sr)TiO_3$ thick films on the Ag/Pd printed $Al_2O_3$ substrates for the LTCCs (Low Temperature Co-fired Ceramics) applications. From the X-ray diffraion analysis, 3 wt% $Li_2CO3$ doped BST thick films on the Ag/Pd printed $Al_2O_3$ substrates, which sintered at 900 $^{\circ}C$ have perovskite structure without any pyro phase. The dielectric properties of 3 wt% $Li_2CO3$ doped BST thick films were measured from 1 kHz to 1 MHz. To investigate the electrical properties of 3 wt% $Li_2CO3$ doped BST thick films, we employed the impedance spectroscopy. The complex impedance of 3 wt% $Li_2CO3$ doped BST thick films were measured from 20 Hz to 1 MHz at the various temperatures.

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임피던스 측정법을 이용한 엑시머 레이져 열처리 Poly-Si의 특성 분석 (APPLICATION OF IMPEDANCE SPECTROSCOPY TO POLYCRYSTALLINE SI PREPARED BY EXCIMER LASER ANNEALING)

  • 황진하;김성문;김은석;류승욱
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.200-200
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    • 2003
  • Polycrystalline Si(polysilicon) TFTs have opened a way for the next generation of display devices, due to their higher mobility of charge carriers relative to a-Si TFTs. The polysilicon W applications extend from the current Liquid Crystal Displays to the next generation Organic Light Emitting Diodes (OLED) displays. In particular, the OLED devices require a stricter control of properties of gate oxide layer, polysilicon layer, and their interface. The polysilicon layer is generally obtained by annealing thin film a-Si layer using techniques such as solid phase crystallization and excimer laser annealing. Typically laser-crystallized Si films have grain sizes of less than 1 micron, and their electrical/dielectric properties are strongly affected by the presence of grain boundaries. Impedance spectroscopy allows the frequency-dependent measurement of impedance and can be applied to inteface-controlled materials, resolving the respective contributions of grain boundaries, interfaces, and/or surface. Impedance spectroscopy was applied to laser-annealed Si thin films, using the electrodes which are designed specially for thin films. In order to understand the effect of grain size on physical properties, the amorphous Si was exposed to different laser energy densities, thereby varying the grain size of the resulting films. The microstructural characterization was carried out to accompany the electrical/dielectric properties obtained using the impedance spectroscopy, The correlation will be made between Si grain size and the corresponding electrical/dielectric properties. The ramifications will be discussed in conjunction with active-matrix thin film transistors for Active Matrix OLED.

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온라인 임피던스 분광법을 이용한 배터리 진단기능을 갖춘 지능형 충전기의 개발 (Development of the Intelligent Charger with Embedded Battery Diagnosis Function Using Online Impedance Spectroscopy)

  • 응웬탄두안;최우진
    • 전력전자학회:학술대회논문집
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    • 전력전자학회 2013년도 전력전자학술대회 논문집
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    • pp.329-330
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    • 2013
  • In this research, a novel battery charge system with embedded diagnosis function is proposed by using online impedance spectroscopy. The impedance spectroscopy technique is employed to investigate the impedance variation of the battery thereby estimating the state of health of the battery. A small voltage perturbation is applied to the battery by the voltage controller of the bidirectional converter with no additional hardware and the impedance of the battery is then calculated by the digital lock-in amplifier embedded in the DSP of the charger. The design procedure of the proposed charger is detailed and the feasibility of the system is verified by the experiments.

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Interfacial Electrical/Dielectric Characterization in Low Temperature Polycrystalline Si

  • Hwang, Jin-Ha
    • 마이크로전자및패키징학회지
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    • 제12권1호
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    • pp.77-85
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    • 2005
  • Impedance spectroscopy was applied to low temperature polycrystalline Si in order to investigate the electrical/dielectric information in polycrystalline Si. By combined microstructure and impedance spectroscopy works, it was shown that the electrical information is sensitive to the corresponding microstructure, i.e., the grain size and distribution, judged from the capacitance vs. grain size relationship. At $360 mJ/cm^2$, the maximum in capacitance and the minimum in resistance correspond to the largest grain sizes of unimodal distribution in polycrystalline Si. The electrical/dielectric characterization is compared with Raman spectroscopic characterizations in terms of microstructure.

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