• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.6 no.2
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• pp.166-174
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• 1994

An experimental study has been performed to identify the evaporation characteristics of HCFC-22 for transport refrigeration system. Heat transfer coefficients were measured in a horizontal, smooth evaporating tube with an inner diameter of 10.7mm and a length of 2.8m. The refrigerant was heated electrically by surface-wrapped heaters and uniform power is applied along the tube. The entire tube was divided into 7 sections. Surface temperatures of tube and refrigerant temperature in each test section were measured. Pressure drops in each section and the inlet pressure were also measured. The mass flowrate of the refrigerant was controlled and measured. A single tube evaporation test was conducted for different ranges of mass flux of refrigerant, heat flux of evaporator and condensing temperature of transport refrigeration system. The evaporation heat transfer coefficients of HCFC-22 were compared with predictions from the well known Chen's correlations. Averaged heat transfer coefficients in this experiment range from $2kW/m^2/^{\circ}C$ to $3kW/m^2/^{\circ}C$. Most of the experimental results differ from the predicted ones by less than ${\pm}30%$.

• YAKHAK HOEJI
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• v.45 no.6
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• pp.623-633
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• 2001

Various bupivacaine-loaded microspheres were prepared using poly(d,1-lactide) (PLA) and poly(d,1-lactic-co-glycolide) (PLGA) by a solvent evaporation method for the sustained release of drug. The effects of process conditions such as drug loading, polymer type and solvent type on the characteristics of microspheres were investigated. The prepared microspheres were characterized for their drug loading, size distribution, surface morphology and release kinetics. Drug loading efficiency and yield of PLGA micro- spheres were higher than those of PLA microspheres. The prepared microspheres had an average particle size below 5${\mu}{\textrm}{m}$. The particle size range of microspheres was 1.65~2.24${\mu}{\textrm}{m}$. As a result of SEM, the particle size of PLA microspheres was smaller than that of PLGA microspheres. In morphology studies, microspheres showed a spherical shape and smooth surface in all process conditions. In thermal analysis, bupivacaine-loaded microspheres showed no peaks originating from bupivacaine. This suggested that bupivacaine base was molecular-dispersed in the polymer matrix of microspheres. The release pattern of the drug from microspheres was evaluated for 96 hours. The initial burst release of bupivacaine base decreased with increasing the molecular weight of PLGA, and the drug from microspheres released slowly. In conclusion, bupivacaine-loaded microspheres were successfully prepared from poly(d,1-lactide) and poly (d,1- lactic-co-glycolide) polymers with different molecular weights allowing control of the release rate.

• Journal of Power System Engineering
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• v.8 no.1
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• pp.41-47
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• 2004

Cooling towers are widely used not only for cooling products and equipment in manufacturing process but HVAC(Heating, Ventilation and Air Conditioning) system. As a cooling tower is the terminal apparatus which discharges heat from industrial process, the efficiency of heat exchange in the cooling tower greatly affects to the overall performance of a thermal system. In this paper, we constituted a new water cooling system by using a Latent heat of evaporation in an enclosed tank, and this system is consisted of an enclosed vacuum tank and water driven ejector system. Several experimental cases were carried out for improvement methods of high vacuum pressure and water cooling characteristics. The ejector performance was tested in case of water temperature variations that flows into the ejector. Based on the vacuum pressure by water driven ejector, the water cooling characteristics were investigated for the vaporized air condensing effects.

• Korean Journal of Materials Research
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• v.25 no.6
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• pp.265-268
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• 2015

ZnO micro/nanocrystals at large scale were synthesized through the thermal evaporation of Al-Zn mixtures under air atmosphere. The effect of synthetic temperature and time on the morphology of the micro/nanocrystals was examined. It was found that the temperature and time affected the morphology of the ZnO crystals. At temperatures below $900^{\circ}C$, no crystals were synthesized. At a temperature of $1000^{\circ}C$, ZnO crystals with a rod shape were synthesized. With an increase in temperature from $1000^{\circ}C$ to $1100^{\circ}C$, the morphology of the crystals changed from rod shape to wire and granular shapes. As the time increased from 2 h to 3 h at $1000^{\circ}C$, tetrapod-shaped ZnO crystals started to form. XRD patterns showed that the ZnO crystals had a hexagonal wurtzite structure. EDX analysis revealed that the ZnO crystals had high purity. It is believed that the ZnO nanowires were grown via a vapor-solid mechanism because no catalyst particles were observed at the tips of the micro/nanocrystals in the SEM images.

• Elastomers and Composites
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• v.44 no.4
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• pp.397-400
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• 2009

Ozone caused the crack on the surface of a rubber article by oxidation of double bond at room temperature. Wax migrates to the surface of a rubber article and makes a physical barrier to prevent process of ozonation. We investigated change of molecular weight distribution of waxes in unfilled NR, SBR, and BR vulcanizates before and after aging at room temperature for 6 months. Migration and evaporation behaviors of wax in a rubber article at ambient conditions help understand a role of wax as an antidegradant and appearance contamination of a rubber article. The relative intensity distribution of n-alkanes of the NR specimen after the aging was shifted to higher molecular weight compared with the relative intensity distribution before the aging, while those of the SBR specimen before and after the aging did not show a big difference.

• Journal of Powder Materials
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• v.11 no.2
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• pp.105-110
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• 2004

In this study the possibility to obtain a homogeneous mixture and to produce solid solutions and intermetallic compounds of Fe and Al nano particles by simultaneous pulsed wire evaporation (S-PWE) have been investigated. The Fe and Al wires with 0.45 mm in diameter and 35 mm in length were continuously co-fed by a special mechanism to the explosion chamber and simultaneously exploded. The characteristics, e.g., phase composition, particle shape, and specific surface area of Fe-Al nano powders have been analyzed. The synthesized powders, beside for Al and $\alpha$-Fe, contain significant amount of a high-temperature phase of $\gamma$-Fe, Fe Al and traces of other intermetallics. The phase composition of powders could be changed over broad limits by varying initial explosion conditions, e.g. wire distance, input energy, for parallel wires of different metals. The yield of the nano powder is as large as 40 wt ％ and the powder may include up to 46 wt % FeAl as an intermetallic compound.

• Archives of Pharmacal Research
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• v.18 no.1
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• pp.22-26
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• 1995

The solubility and dissolution rate of naproxen (NPX) complexed with 2-hydroxypropyl-.betha.-cyc-lodextrin (2-HP.betha.CD) using coprecipitation, evaporation, freeze-drying and kneading method were investigated. Solubility of NPX linearly increased (correlation cefficient, 0.995) as $2-HP\betaCD$ concentraction increased, resutling in $A_l$ type phase solubility curve. Inclusion complexes prepared by four different methods were compared by different methods were compared by dfferential scanning calorimetry(DSC). The NPX showed sharp endothemic peak around $156^{\circ}C$ but inclusion complexes by evaporation, freeze-drying and kneading method showed very broad peak without distinct phase transtion temperature. In contrast, inclusion complex prepared by coprecipitation method resulted in detectable peak around $156^{\circ}C$ which is similar to NPX, suggesting incoplete formation of indusion co plex. Dissolution rate of inclusion complexes prepared by evaporation, frezz-drying and kneding except coprecipitation method was largely enhanced in the simultaed gastric and intestinal fluid when compared to NPX powder and commercial $NA-XEN^\registered$tablet. However, about 65% of NPX in gstric fluid. in case of inclusion complex prepared by coprecipitation method, formation of inclusion complex appeared to be incoplete, resulting in no marked enhancement of dissolution rate. From these findings, inclusion complexes of poorly water-soluble NPX with $2-HP\betaCD$ were useful to increase soubility and dissolution rate, resting in enhancement of bioavailability and minimization of gastrointestinal toxicity of drug upon oral administration of inclusion complex.

• Journal of the Korean Ceramic Society
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• v.17 no.2
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• pp.80-88
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• 1980

The sintering phenomena and piezoelectric properties of PZT ceramics of composition $Pb(Zr_{0.54} Ti_{0.46})O_3$ were investigated when a small quantity of $La_2O_3$ , $LaMnO_3$, $LaCrO_3$ were added. The unwanted chemical composition change in PZT during sinterin porces du to PbO evaporation poses a severe problem in PZt manufacturinig. It is observed tat an addition of small amount of $LaMnO_3$ to PZT markedly decreases the evaporation of PbO during sintering . The green compact of (1-x) PZT.xLaMnO3(x=0.02~0.10) could be sintered of under O2 atmosphere alone with no significant loss of PbO. The planar coupling factor kp of the sintered $0.98Pb(Zr_{0.54} Ti_{0.46})O_{3.0.02}LaMnO}3$ is similar to that of commercial PZT 6A. Microstructure investigation shows that part of sintering process of $Pb(Zr, Ti)O_3$.$LaMnO_3$ system progresses via liquid phase sintering. It is believed that the evaporation of PbO in PZT sintering is restricted by the addition of $LaMnO_3$ due to the above phenomena. Furthermore the solid solution of $LaMnO_3$ in PZT causes diffuses phase transition.

• Journal of computational fluids engineering
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• v.14 no.2
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• pp.9-18
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• 2009

The cargo containment system (CCS) for ships carrying cryogenic fluid consists of at least two levels of barriers and insulation layers. It is because, even though there is a small amount of leak through the primary barrier, the liquid tight secondary barrier blocks further leakage of the cryogenic fluid. However, once the secondary barrier is damaged, it is highly possible that the leaked cryogenic fluid flows through the flat joint made of glass wool and reaches the inner hull of the ship. The primary objective of the present study is to investigate the influence of the damage extent in the secondary barrier on the amount of leaked cryogenic fluid reaching the inner hull and the temperature distribution there. Simulation results using a computational fluid dynamics tool were compared with the experimental data for the leaked cryogenic fluid flow and evaporation in the secondary insulation layer. The experimental and computational results suggest that, unless there is a massive leak, the cryogenic fluid mostly evaporates in the insulation layer and does not reach the inner hull in the state of liquid.

• Proceedings of the SAREK Conference
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• 2007.11a
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• pp.247-251
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• 2007

Because of the ozone layer depletion and global warming, new alternative refrigerants are being developed. In this study, evaporation heat transfer characteristics of carbon dioxide flowing upward in a vertical micro-fin tube have been investigated by experiment. Before a test section, a pre-heater is installed to adjust the inlet quality of the refrigerant to a desired value. The micro-fin tube with outer diameter of 5 mm and length of 1.44 m was selected as the test section. The test was conducted at mass fluxes of 318 to $530\;kg/m^2s$, saturation temperature of -5 to $5^{\circ}C$, and heat fluxes of 15 to $30\;kW/m^2$. As the vapor quality increases, the heat transfer coefficients of carbon dioxide are increased, and the heat transfer coefficients increase when the heat fluxes and saturation temperatures increase, and there was not much of influence of mass flux on the heat transfer coefficients.