• Title/Summary/Keyword: EVAPORATION

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Synthesis and Luminescence Properties of $YGdO_3:Eu^{3+}$ Phosphor by Solvent Evaporation Method (용매 증발법에 의한 $YGdO_3:Eu^{3+}$ 형광체의 제조와 발광 특성)

  • Lee, Dong-Kyu;Jeon, Sang-Bae;Lee, Jin-Hwa
    • Journal of the Korean Applied Science and Technology
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    • v.24 no.3
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    • pp.238-245
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    • 2007
  • $Eu^{3+}$ doped $YGdO_3$ phosphors particles which have fine size and narrow size distribution with non aggregated uniform morphology were prepared by solvent evaporation method for the improvement of emission efficiency. Several parameters have been investigated in this study such as the influences of composition ratio of host materials, calcination temperature, amount of activator, surfactant, pH and flux on the photoluminescence intensity, particle size and dispersion. $Eu^{3+}$ doped $YGdO_3$ phosphor presented a strong narrow band emission peak at 612nm. The maximum emission intensity of$YGdO_3:Eu^{3+}$ occurred when $Eu^{3+}$ concentration is 3wt% under vacuum ultra violet excitation. Prepared phosphors were found to have small round-shaped particles about 150nm in size. The addition of PVA as a surfactant inhibits the grain growth and the agglomeration of particles efficiently by reducing the oxygen bridge bonds. As the pH reduces, PL intensity increase due to reducing the formation of oxygen bridge bonds. The particles prepared from solvent evaporation method with 5wt% LiCl were found to have 120% PL intensity compare to particles prepared without LiCl flux.

Preparation and Evaluation of Bupivacaine Microspheres by a Solvent Evaporation Method (용매증발법에 의한 부피바카인 microsphere의 제조 및 평가)

  • Kwak, Son-Hyok;Hwang, Sung-Joo;Lee, Byung-Chul
    • YAKHAK HOEJI
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    • v.44 no.6
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    • pp.511-520
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    • 2000
  • Various bupivacaine-loaded microspheres were prepared from poly (d,l-lactide) (PLA) or poly (d,l-lactic-co-glycolide) (PLGA) by a solvent evaporation method for the sustained release of drug. PLA and PLGA microspheres were prepared by w/o/w and w/o/o multiple emulsion solvent evaporation, respectively. The effects of process conditions such as emulsification speed, emulsifier type, emulsifier concentration and internal/external phase ratio on the characteristics of microspheres were investigated. The prepared microspheres were characterized for their drug loading, size distribution, surface morphology and release kinetics. Drug loading efficiency was higher in the microspheres prepared by w/o/o multiple emulsion than that by w/o/w multiple emulsion method, because the solubility of bupivacaine HCI was decreased in oil phase compared with water phase. The prepared microspheres had an average diameter between 1 and $2\;{\mu}M$ in all conditions of two methods. In morphology studies the PLA microspheres showed an irregular shape and smooth surface, but PLGA microspheres had a spherical shape and smooth surface. The release pattern of the drug from microspheres was evaluated on the basis of the burst effect and the extent of the release after 24h. The in vitro release of bupivacaine HCl from microspheres showed a large initial burst release and $60{\sim}80%$ release within one day in all conditions of two methods. The extents of the burst release against PLA and PLGA microspheres were $30{\sim}50%$ and $50{\sim}80%$ within 20min, respectively. This burst release seems to be due to the smaller size of microspheres and the solubility of drug in water.

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Fabrication of Sub-Micron Size $Al-AlO_x-Al$ Tunnel Junction using Electron-Beam Lithography and Double-Angle Shadow Evaporation Technique (전자빔 패터닝과 double-angle 그림자 증착법을 이용한 sub-micron 크기의 $Al-AlO_x-Al$ 터널접합 제작공정개발)

  • Rehmana, M.;Choi, J.W.;Ryu, S.J.;Park, J.H.;Ryu, S.W.;Khim, Z.G.;Song, W.;Chong, Y.
    • Progress in Superconductivity
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    • v.10 no.2
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    • pp.99-102
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    • 2009
  • We report our development of the fabrication process of sub-micron scale $Al-AlO_x-Al$ tunnel junction by using electron-beam lithography and double-angle shadow evaporation technique. We used double-layer resist to construct a suspended bridge structure, and double-angle electron-beam evaporation to form a sub-micron scale overlapped junction. We adopted an e-beam insensitive resist as a bottom sacrificing layer. Tunnel barrier was formed by oxidation of the bottom aluminum layer between the bottom and top electrode deposition, which was done in a separate load-lock chamber. The junction resistance is designed and controlled to be 50 $\Omega$ to match the impedance of the transmission line. The junctions will be used in the broadband shot noise thermometry experiment, which will serve as a link between the electrical unit and the thermodynamic unit.

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Estimation of Potential Water Resources in Mega Cities in Asia

  • Takuya, Komura;Toshitsugu, Moroizumi;Kenji, Okubo;Hiroaki, Furumai;Yoshiro, Ono
    • Proceedings of the Korea Water Resources Association Conference
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    • 2008.05a
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    • pp.75-81
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    • 2008
  • The water shortage in mega cities in Asia, which face a rapid growth in urban population, is an outstanding problem. It is important, therefore, to accurately estimate the water balance in each city in order to use the limited water resources effectively. In this study, we estimated the potential water resources in し sixteen mega cities in Asia. The target cities were Delhi and Calcutta, India; Colombo, Sri Lanka; Dhaka, Bangladesh; Yangon, Myanmar; Bangkok, Thailand; Kuala Lumpur, Malaysia; Singapore; Jakarta, Indonesia; Hanoi, Vietnam; Beijing and Hong Kong, the People's Republic of China; Seoul, the People's Republic of Korea; Manila, the Philippines, and Sapporo and Tokyo, Japan. The potential water resources were estimated by subtracting the actual evaporation from the amount of rainfall. The actual evaporation was estimated using the potential evaporation obtained by Hamon's equation which requires the air temperature and the possible hours of sunshine. When the results of Hamon's and Penman's evaporation equations were compared, a considerable error appeared in the low latitude region. The estimation using Hamon's equation was corrected with the linear regression line of Hamon's and Penman's equations. A classification of the land cover was carried out based on satellite photographs of the target cities, and the volume of surface runoff for each city was obtained using the runoff ratios which depended on the land cover. As a result, the potential water resources in the above mega cities in Asia were found to be greater than the world average. However, the actual water resources which are available for one person to use are probably very limited.

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Performance Change of Gas Turbine with a Evaporation Cooling System in Summer Season (하절기 기화냉각장치 설치에 따른 가스터빈 성능변화)

  • Chung, Hyeon-Jo;Yoo, HoSeon;Moon, Seung-Jae
    • Plant Journal
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    • v.13 no.1
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    • pp.37-43
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    • 2017
  • This study analyzed the change of gas turbine performance with air temperature decrease by the evaporation cooling system in summer season. Gas turbine performance was tested on the condition that ambient temperature is $29{\pm}1^{\circ}C$. As a result, Air temperature at the compressor inlet was decreased by $4.12^{\circ}C$ after the installation of evaporation cooling system. Decreased air temperature followed by increased air density affected gas turbine performance, Which increased compressor pressure ratio by 0.27, improved compressor efficiency of 0.29 %p, improved gas turbine enthalpy drop efficiency of 0.31 %p, improved the gas turbine efficiency by 0.44 %p, improved electric power output by 4,489 kW. On the other side, the influence of the humidity increase and flow resistance increase was negligible.

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Different morphologies of three dimensional ZnO structures synthesized by thermal evaporation method without a catalyst (촉매를 사용하지 않는 열 기화법으로 다양한 형태의 ZnO 3차원 구조체 합성)

  • Bang, Sin Young;Tran, Van Khai;Oh, Dong Keun;Maneeratanasarn, Prachuporn;Choi, Bong Geun;Ham, Heon;Kim, Kyoung Hun;Shim, Kwang Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.23 no.1
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    • pp.8-13
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    • 2013
  • ZnO with different morphologies can be used various application depending on their shapes. Different morphologies of ZnO structures were synthesized by a catalysis-free thermal evaporation process. Their morphologies were dependent on the distance from the source to substrate on the same processing condition; in the result were products morphologies of the hollow, cage and star. Their shapes and crystalinity were evaluated by SEM and XRD, respectively. This work demonstrates what kind of growth factors would be involved in the final structure morphologies.

A study on Cu(In,Ga)Se2 thin film fabarication using to co-evaporation (동시진공증발법을 이용한 Cu(In,Ga)Se2 박막 제작에 관한 연구)

  • Park, Jung-Cheul;Chu, Soon-Nam
    • Journal of the Korea Institute of Information and Communication Engineering
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    • v.16 no.10
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    • pp.2273-2279
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    • 2012
  • This research is based on fabricating Cu(In,Ga)$Se_2$ thin-film by co-evaporation method. On $1^{st}$ - stage, $In_2Se_3$ phase appeared when the substrate temperature reached to $400^{\circ}C$, however, there was small effect between the substrate temperature and absorbency spectrum on $2^{nd}$, $3^{rd}$ - stage because the average thickness of the thin-film was $1{\mu}m$ or higher. SEM and XRD was measured on $2^{nd}$ and $3^{rd}$ stage and it showed as the substrate temperature increases, the density of the crystal structure increased with the decreament of the vacancy. Furthermore, the formation of Cu(In0.7Ga0.3)$Se_2$ phase showed at $480^{\circ}C$ and $500^{\circ}C$.

Structural characteristics of ZnO nanostructures synthesized by the thermal evaporation method (열증착법으로 합성된 ZnO 나노 구조체의 구조적 특성)

  • Bang, Sin-Young;Kim, Woo-Sik;Chung, Jun-Ho;Choi, Bong-Geun;Shim, Kwang-Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.2
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    • pp.81-86
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    • 2008
  • ZnO nanowires were synthesized by the thermal evaporation method and their growth mechanisms were confirmed by the characterization of the structural features depending on the growth conditions. The increase of vaporization temperature accelerates the growth rate and morphologies of ZnO nanowires were drastically changed at the temperature over 1000$^{\circ}C$, because of changed $CO/CO_2$ partial pressure. Au particles play their role on growth of ZnO nanowire as catalyst at growth temperature over 700$^{\circ}C$. The synthesized ZnO nanowires exhibit blue emission at 380 nm.

Effects of Sintering Atmosphere on Piezoelectric Properties of 0.75BF-0.25BT Ceramic

  • Kim, Dae Su;Kim, Jeong Seog;Cheon, Chae Il
    • Journal of the Korean Ceramic Society
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    • v.53 no.2
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    • pp.162-166
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    • 2016
  • 0.75BF-0.25BT ceramics were prepared by sintering at $980-1040^{\circ}C$ in air or under atmosphere powder. A sample with 1 mole %-excess $Bi_2O_3$ was also prepared to compensate for $Bi_2O_3$-evaporation. Physical and piezoelectric properties of these three samples were compared. When the sintering temperature increased from $980^{\circ}C$ to $1040^{\circ}C$, the density of the sample sintered in air decreased continuously due to Bi-evaporation. Due to the suppression of Bi-evaporation, the sample sintered under atmosphere powder had a higher density at sintering temperatures above $1000^{\circ}C$ than did the sample sintered in air. The addition of 1 mole %-excess $Bi_2O_3$ successfully compensated for Bi-evaporation and kept the density at the higher value until $1020^{\circ}C$. Grain size increased continuously when the sintering temperature increased from 980 to $1040^{\circ}C$, irrespective of the sintering atmosphere. When the sintering temperature increased, the piezoelectric constant ($d_{33}$) and the electromechanical coupling factor ($k_p$) increased for all samples. The sample with 1 mole % excess-$Bi_2O_3$ showed the highest density and the best piezoelectric properties at sintering temperature of $1020^{\circ}C$.

An Experimental Study on Evaporation/Condensation Heat Transfer with Flow Direction in Brazed Plate Heat Exchanger using Refrigerant 410A (R410A를 이용한 브레이징 타입 판형열교환기에서 물 측 유동방향에 따른 응축/증발 성능 평가)

  • Lee, Sung-Woo;Jeong, Young-Man;Lee, Jae-Keun;Lee, Dong-Hyuk
    • Proceedings of the SAREK Conference
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    • 2009.06a
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    • pp.1096-1101
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    • 2009
  • The plate heat exchanger(PHE) in heat pump has two flow streams of the refrigerant and water. The flow direction of the refrigerant, unlike that of water, can be changed by a 4-way valve depending on operating condition. Therefore the flow arrangement is a parallel flow for heating and a counter flow for cooling, respectively. In this study, the effects of the flow direction of the water on the heat transfer rate are investigated experimentally. The experiments are carried out for brazed plate heat exchangers under a parallel and counter flow conditions in evaporation and condensation. The experimental parameters in this study include the mass flux of the refrigerant 410A from 3 to $14\;kg/m^2s$ and the flow patterns for the pressure of PHE fixed at 0.97 and 2.46 MPa. The results show that both the heat transfer rate and frictional pressure drop across the PHE increase with the mass flux. The heat transfer rate of the refrigerant 410A for evaporation show great sensitivity to flow direction of the water. The heat transfer rate for evaporation with a counter flow are 5-30% higher than that with a parallel flow.

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