• Korean Journal of Materials Research
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• v.7 no.3
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• pp.244-250
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• 1997

본 연구에서는 에폭시/산무수물계에 경화촉진제를 첨가한 시료를 몰드(mold)내에서 등온 경화시킬 때 시료 내부의 온도변화를 측정하여 얻어진 온도-시간 곡선(temperature-time profile)을 조사하였다. 실험에 사용한 경화촉진제의 종류는 1-cyanoethy1-2-ethy1-4-methy1 imidazole(1E4MZ-CN), N,N-dimethy1 benzy1 amine(BDMA), 2,4,6-tris(dimethy1-aminomethy1)-phenol(DMP-30)이며 그들의 농도(c)는 1.0,1.5,2.0,2.5,phr그리고 경화온도(T$_{cure}$ )는 65,70,85,95$^{\circ}C$로 하였다. 경화가 진행되는 동안 시료내부의 온도는 초기에 경화온도로 상승한 후 본격적인 경화 반응이 일어나기 시작하여 온도가 급격히 상승하였다가 다시 감소하는 양상을 보였다. 온도-시간 곡선상에 나타나는 온도가 최고로 상승되는 시점(t$_{peak}$ )과 그 때의 온도(T$_{peak}$ )는 촉진제의 종류와 농도 그리고 경화온도에 의하여 영향을 받았다. 사용한 경화촉진제중에 DMP-30이 가장 짧은 t$^{peak}$ 값을 가져 가장 우수한 촉진 효과를 갖는 것으로 나타났으며, T$_{peak}$ 는 촉진제의 농도와 경화온도가 증가할수록 상승하였다. 그리고 경화촉진제의 농도와 경화온도의 변화에 따른 t$_{peak}$ 과 T$_{peak}$ 의 변화를 보면 촉진제 농도와 경화온도가 낮을 때 그 변화가 민감하여 2E4MZ-CN 이 가장 민감한 촉진제로 나타났으며 또한 T$_{peak}$ 에 영향을 주는 여러가지 요소들을 본 연구에서 얻어진 결과로부터 자세히 살펴보았다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.55-59
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• 2007

Technologies of super-precision micro pattern mold machining and high-performance optical films manufacturing using thereof forms the basis of recent display industries which have developed remarkably. Especially, it is the light guide plates and high luminous intensity prism sheets at BLU or FLU in LCD and lenses at virtual keyboard's display to be manufactured by micro machining technology. One way the industry requires to do that is by developing high-performance light guide plates or films which are existing light guide plates, diffusion films and luminance enhancement prism films all in one. In this research effort, basic processing of the micro pyramid structure by shaping method is proposed. Experiments of mold machining of pitch $20{\mu}m$ tetrahedral pyramid and pitch $100{\mu}m$ trihedral pyramid using a $90^{\circ}$ diamond tool were conducted to identify a variety of machining features, such as cutting forces, conditions of the surface, shapes of chips, and influence of materials.

• Journal of Environmental Health Sciences
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• v.7 no.1
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• pp.51-57
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• 1981

This Study was carried out to investigate yeast and mold contamination in fermented milk products produced by 9 different domestic manufacturers from October 20. to December 5. 1980 The results obtained in the study were as follows 1) pH values of the products were ranged from pH 3.14 to pH 4.20 and average of sour milk drinks was pH $3.66\pm 0.19$ and fermented milks pH $3.74\pm 0.11$. Therefore the difference of pH average among sour milk drinks and fermented milks was statistically significant. (p<0.01) 2) In case of yeast contamination, yeast was found on all the four producted at the same date. From this result, it seemed that yeast contamination occured during the manufacturing progress. 3) Degree of contamination by the indicator organisms was E. coli positive, 3.7%: over 1,000 yeasts/ml, 14.8% over 10 molds/ml, 0.9%. 4) In the range of over 1,000 yeasts/ml, degree of contamination by yeast was 8.4% in fermented milk and 16.7% in sour milk drink. 5) Yeasts in product C increased to the spoilage number within 5 days and in H increased within 10 days at 5C. At 15$\circ$C, yeast increased to the spoilage number within 15 days in product A.D. 6) It seems that the yeast number of initial contamination should be important than the increase rate as criteria on the fermented Milk products.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.1597-1600
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• 2005

Recently, the trends of TFT-LCD are large scale and thin thickness, so, the demands of Light Guide Panel(LGP) which is able to substitute for prism sheets are appeared. Functions of LGP obtaining polarization of light of the prism sheet as well as the incidence and reflection of light are demanded. This prismless type LGP to complete functions of the existing LGP and polarization at once must be supported by micro machining technology of LGP surface. In this research, we have used the STAMPER method for the mass product and In-Line process, and the optimized conditions are established by analyzing the cutting force and conditions according to the material and processing properties when the prismless type LGP mold is fabricated. Parameters of the cutting condition were the workpiece and cutting depth.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.113-116
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• 2006

Some nano hair systems in the nature are found to show excellent adhesive characteristic, which is called dry adhesive, and synthetic nano hairs to mimic these adhesiveness are believed to have many applications. To develop a practical synthetic dry adhesive system, we mold nano hairs on plastic substrates using thermoplstic materials including COC, PP, PC and PMMA. and estimate the moldability and the adhesive characteristic. As a template for molding nano hairs, AAO membrane is first adopted, which is 60um thick and 13mm in diameter. This membrane has about a billion of through-holes of which diameter is around 200nm. This AAO membrane and the pellet of materials are stacked in the mold and pressed to mold after heating up to be melted. The AAO membrane is removed using KOH to obtain the molded nano hairs. As a result, the diameter of the molded hairs is around 200nm and the length is $2um{\sim}60um$ depending on the molding conditions and materials. The molded nano hair substrates is estimated to show much better adhesive characteristic than a substrate without nano hairs.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.95-98
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• 2006

LCD-BLU (Back Light Unit) is one of kernel parts of LCD unit. The fabrication method of a 3-D micro mold patterned with micro-lenses for the LGP (Light Guiding Plate), one of the most important parts of LCD-BLU, was presented. Instead of dot pattern made by etching, 3-D optical pattern design with $50{\mu}m$ micro-lens was applied in the present study. The micro-lens pattern fabricated by modified LiGA with thermal reflow process was applied to the optical design of LGP. The positive micro-lens patterned injection mold with different aspect ratios (i.e. 0.3 and 0.4) was fabricated with modified LiGA with thermal reflow process. The brightness of LCD-BLU increased as aspect ratio of micro-lens increased.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.11a
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• pp.73-76
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• 2004

High-temperature Superconductor(HTS) tubes were fabricated in term of different processing variables such as preheating temperature, speed of mold rotation and cooling rate by centrifugal forming method. For powder melting by induction the optimum range of melting temperatures and preheating temperature were $1050^{\circ}C{\sim}1100^{\circ}C$ and $550^{\circ}C$ for 30min, respectively. The mould roating speed was 1000rpm. A tube was annealed at $840^{\circ}C$ for 72hours in oxygen atmosphere. The plate-like grains were well developed along the roating direction and typical grain size was about more than $40{\mu}m$. It was found that Ic values increased with increasing the preheating temperature and speed of mold rotation. While Ic decreased with increasing the cooling rate. The measured Ic in $50mm{\times}70mm{\times}2.5mm$ tube was about 896Amp.

• Research in Plant Disease
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• v.20 no.3
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• pp.182-188
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• 2014

Because bacterial isolates from only a few genera have been developed commercially as biopesticides, discovery and characterization of novel bacterial strains will be a key to market expansion. Our previous screen using plant bioassays identified 24 novel biocontrol isolates representing 12 different genera. In this study, we characterized the 3 isolates showing the best biocontrol activities. The isolates were Pantoea dispersa WCU35, Proteus myxofaciens WCU244, and Exiguobacterium acetylicum WCU292 based on 16S rRNA sequence analysis. The isolates showed differential production of extracellular enzymes, antimicrobial activity against various fungal or bacterial plant pathogens, and induced systemic resistance activity against tomato gray mold disease caused by Botrytis cinerea. E. acetylicum WCU292 lacked strong in vitro antimicrobial activity against plant pathogens, but induced systemic resistance against tomato gray mold disease. These results confirm that the trait of biological control is found in a wide variety of bacterial genera.

• Journal of Korea Foundry Society
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• v.23 no.1
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• pp.40-46
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• 2003

Semisolid forming requires alloys with non-dendritic microstructure of the thixotropy. Recently, low pouring temperture method without stirring, i.e. liquidus casting has been found out new fabrication method of the semisolid metals. Effects of melt superheat and mold conditions on the globulization of primary Al of $AlSi_7Mg$ alloy were investigated in gravity casting process without stirring. The microstructures of primary Al as function of melt superheat and mold temperature show globular, rosette and dendritic shapes. The conditions for globular microstructure of primary Al were low melt superheat < 35 K and low mold temperature < 500 K. The thermal conditions for globular microstructure of primary Al were undercooled melt at early solidification stages and slow cooling < 0.6 K/s. It was found that the initial microstructure was maintained throughout the solidification and the globules of primary Al can be obtained by high nucleation of fine and spherical nuclei due to enhanced undercooling of melt.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.364-367
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• 2007

In nano-imprint lithography (NIL) process, which has shown to be a good method to fabricate polymeric patterns, several kinds of pattern defects due to thermal effects during polymer flow and mold release operation have been reported. A typical defect in NIL process with high aspect ratio and low resist thickness pattern is a resist fracture during the mold release operation. It seems due to interfacial adhesion between polymer and mold. However, in the present investigation, FEM simulation of NIL molding process was carried out to predict the defects of the polymer pattern and to optimize the process by FEA. The embossing operation in NIL process was investigated in detail by FEM. From the analytical results, it was found that the lateral flow of polymer resin and the applied pressure in the embossing operation induce the weld line and the drastic lateral strain at the edge of pattern. It was also shown that the low polymer-thickness result in the delamination of polymer from the substrate. It seems that the above phenomena cause the defects of the final polymer pattern. To reduce the defect, it is important to check the initial resin thickness.