• Title/Summary/Keyword: Dynamic mechanical analyser

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The Properties of DSC and DMA for Epoxy Nano-and-Micro Mixture Composites

  • Lee, Chang-Hoon;Park, Jae-Jun
    • Transactions on Electrical and Electronic Materials
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    • v.11 no.2
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    • pp.69-72
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    • 2010
  • This study investigates the thermal and mechanical properties of insulation elements through the mixing of epoxy based micro and nano particles. Regarding their thermal properties, differential scanning calorimeter and dynamic mechanical analyser were used to calculate the cross-linking densities for various types of insulation elements. The mechanical properties of the bending strength, the shape and scale parameters, were obtained using the Weibull plot. This study obtained the best results in the scale parameters, at 0.5 phr, for the bending strength of the epoxy nano-and-micro mixture composites.

A Study of the Dynamic Characteristics of a Passenger Radial Tire (승용차용 레이디얼 타이어의 동적 특성에 관한 연구)

  • 김두만;김상욱
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.10 no.5
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    • pp.724-734
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    • 1986
  • The dynamic characteristics of a passenger radial tire were studied by the analytical method and the experiments. The purpose of this study is to obtain the natural frequencies and the mode shapes of a 2 ply steel belt radial tire fixed on the wheel in order to give datum of the dynamic design of tire. The governing equations are derived with the energy method. The composite toroidal finite elements with three degrees of freedom at each node are defined by specifying geometry, internal displacement functions, strain displacement and stress displacement relationships. In order to verify the capability of the present analysis, the natural frequencies and mode shapes of the passenger radial tire are obtained experimentally by using the multi-channel F.F.T. analyser and compared the numerically obtained values. The results show that the analytically obtained values are in good agreement with the experiment and in addition they are in line with the Pott's experimental results.

Reliability Enhancement of Anisotropic Conductive Adhesives Flip Chip on Organic Substrates by Non-Conducting Filler Additions

  • Paik, Kyung-Wook;Yim, Myung-Jin
    • Journal of the Microelectronics and Packaging Society
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    • v.7 no.1
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    • pp.41-49
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    • 2000
  • Flip chip assembly on organic substrates using ACAs have received much attentions due to many advantages such as easier processing, good electrical performance, lower cost, and low temperature processing compatible with organic substrates. ACAs are generally composed of epoxy polymer resin and small amount of conductive fillers (less than 10 wt.%). As a result, ACAs have almost the same CTE values as an epoxy material itself which are higher than conventional underfill materials which contains lots of fillers. Therefore, it is necessary to lower the CTE value of ACAs to obtain more reliable flip chip assembly on organic substrates using ACAs. To modify the ACA composite materials with some amount of conductive fillers, non-conductive fillers were incorporated into ACAs. In this paper, we investigated the effect of fillers on the thermo-mechanical properties of modified ACA composite materials and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACAs composites with different content of non-conducting fillers, dynamic scanning calorimeter (DSC), and thermo-gravimetric analyser (TGA), dynamic mechanical analyzer (DMA), and thermo-mechanical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in the content of filler brought about the increase of $Tg^{DSC}$ and $Tg^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significantly affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.

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On the In situ Composites Containing TLCP Polymerized in PMMA Solution (PMMA 용액에서 중합된 TLCP in situ 복합재료에 관한 연구)

  • Kim, Sung-Kug;Yun, Doo-Soo;Choi, Soo-Kyung;Bang, Moon-Soo;Choi, Jae-Kon;Jo, Byung-Wook
    • Applied Chemistry for Engineering
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    • v.10 no.1
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    • pp.148-153
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    • 1999
  • In situ composites containing a thermotropic liquid crystalline polymer were prepared by polycondensation of 1,4-bis(p-hydroxy-benzoyloxy)butane with 2-bromoterephthaloyl chloride in a poly(methyl methacrylate) solution. Morphology and mechanical, thermal properties of the composites were examined by differential scanning calorimeter(DSC), dynamic mechanical thermal analyser(DMTA), optical microscope and scanning electron microscope(SEM). The TLCP domains showed nematic phase. The glass transition temperature($T_g$) and mechanical properties of the PMMA in the composites increased with increasing the content of TLCP. The TLCP domains were finely dispersed in the PMMA matrix. The 20 wt % TLCP/PMMA composite prepared by in situ polymerization showed more improved mechanical property with finely well dispersed morphology compared with that prepared by solution blending of the same composition.

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Developement of the reinforced acrylic-based hybrid denture composite resin with vinyloligosilsesquioxane (POSS)

  • Nam, Kwang-Woo;Chang, Myung-Woo;Chang, Bok-Sook;Han, Dong-Hoo;Shim, June-Sung;Chang, Ik-Tae;Heo, Seong-Joo;An, Jung-Ho;Chung, Dong-June
    • The Journal of Korean Academy of Prosthodontics
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    • v.38 no.6
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    • pp.782-790
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    • 2000
  • The mainly used polymeric material for the denture is PMMA because of its cost and easiness to handle. So it was widely used material among dentists for past decades. But the acrylic-based denture materials have several common weak points such as shrinkage after curing and lack of strength. In order to solve these problems, we adapted one of hybrid system using acrylic polymer and vinyloligosilsesquioxane(POSS). POSS, which is a well known expandable monomer during polymerization process, may eventually suppress volumetric shrinkage. And the hybrid system makes it possible for the polymer to be stable in various severe conditions. Eight different kinds of samples were designed and synthesized. Each samples were characterized with dynamic mechanical analyser(DMA) to confirm their thermodynamic properties, fractured to analyze the cross-sectional morphology of the samples. And elongation, flexural and impact tests were also executed to evaluate the mechanical properties of the samples. From the results, hybrid composites had well defined crosslinked network structure compared to the widely used denture materials, and the mechanical strength improved without changing any surface condition as increment with POSS ratio in hybrid system. Fractured morphology showed homogeneous surfaces in spite of mutli component system, therefore we can conclude that the adoption of the POSS brought the reinforcement of the denture resin.

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Dynamic response of a laminated hybrid composite cantilever beam with multiple cracks & moving mass

  • Saritprava Sahoo;Sarada Prasad Parida;Pankaj Charan Jena
    • Structural Engineering and Mechanics
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    • v.87 no.6
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    • pp.529-540
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    • 2023
  • A novel laminated-hybrid-composite-beam (LHCB) of glass-epoxy infused with flyash and graphene is constructed for this study. The conventional mixture-rule and constitutive-relationship are modified to incorporate filler and lamina orientation. Eringen's non-local-theory is used to include the filler effect. Hamilton's principle based on fifth-order-layer-wise-shear-deformation-theory is applied to formulate the equation of motion. The analogous shear-spring-models for LHCB with multiple-cracks are employed in finite-element-analysis (FEA). Modal-experimentations are conducted (B&K-analyser) and the findings are compared with theoretical and FEA results. In terms of dimensionless relative-natural-frequencies (RNF), the dynamic-response in cantilevered support is investigated for various relative-crack-severities (RCSs) and relative-crack-positions (RCPs). The increase of RCS increases local-flexibility in LHCB thus reductions in RNFs are observed. RCP is found to play an important role, cracks present near the end-support cause an abrupt drop in RNFs. Further, multiple cracks are observed to enhance the nonlinearity of LHCB strength. Introduction of the first to third crack in an intact LHCB results drop of RNFs by 8%, 10%, and 11.5% correspondingly. Also, it is demonstrated that the RNF varies because of the lamina-orientation, and filler addition. For 0° lamina-orientation the RNF is maximum. Similarly, it is studied that the addition of graphene reduces weight and increases the stiffness of LHCB in contrast to the addition of flyash. Additionally, the response of LHCB to moving mass is accessed by appropriately modifying the numerical programs, and it is noted that the successive introduction of the first to ninth crack results in an approximately 40% to 120% increase in the dynamic-amplitude-ratio.

Study on the Statistical Turbulent Characteristics of $45^{\circ}$ Circular Cross Jet Flow ($45^{\circ}$ 圓形 衝突噴流의 統計學的 亂流特性 硏究)

  • 노병준;김장권
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.10 no.1
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    • pp.110-120
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    • 1986
  • 45.deg. corss jet flow, at the mixing of two jet flows, was experimentally studied. For this study, only the statistical turbulent characteristics and high order moments will be analysed by on-line computer system (hot-wire anemometer system, dynamic analyser and computer system, plotting and printing system). Since mean velocity distributions, intensities of turbulence, Reynolds stresses, correlation coefficients, and other general results were already studied and presented. One dimensional probability density distributions of u', v', and w' were analysed comparing with Gaussian curve, which showed skew and flat tendency according to the Y and Z directions. For the analysis of the joint flow of turublent components, the joint probability density distributions were examined. The fagures were drawn so as to be read joint probabilities, joint probability densities, fluctuating velocities u', v', and w'. For further detailed examination of the variations of skewness and flatness phenomena, iso-joint probability density contours obtained from the profiles of the joint probability density distributions were studied. According to the displacement of positions from the center of the mixing flow and the directions, the flatness and skewness factors were increased.