• Title/Summary/Keyword: Dynamic X-ray

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Fabrication of Nano-sized Metal Dispersed Magnesia Based Composites and Related Mechanical and Magnetic Properties

  • Choa, Yong-Ho;Tadachika Nakayama;Tohru Sekino;Koichi Niihara
    • The Korean Journal of Ceramics
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    • v.5 no.4
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    • pp.395-399
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    • 1999
  • MgO/metal nanocomposite powder mixtures were prepared by solution chemical processes to obtain suitable structure for ceramic/metal nanocomposites. Nickel or cobalt nitrate, as a source of metal dispersion, was dissolved into alcohol and mixed with magnesia powder. After calcined in air, these powders were reduced by hydrogen. Densified nanocomposites were successively obtained by Pulse Electric Current Sintering (PECS) process. The dispersed metal partical size depended on temperature and time in calcination and reduction processes. The phase analyses in the synthesized powders as a functioni of temperature were tracked using a dynamic high temperature X-ray diffractioni (HTXRD) system. Phase and crystallite size analyses were done using X-ray diffractioni and TEM. The MgO/metal nanocomposites were successfully fabricated, and ferromagnetic responses with enhanced coercive force were also investigated for these composites.

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Evolution of Spin and Superorbital Modulation in 4U 0114+650

  • Hu, Chin-Ping;Ng, Chi-Yung;Chou, Yi
    • Journal of Astronomy and Space Sciences
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    • v.33 no.3
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    • pp.173-176
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    • 2016
  • We report on a systematic analysis of the spin and superorbital modulations of the high-mass X-ray binary 4U 0114+650, which consists of the slowest spinning neutron star known. Utilizing dynamic power spectra, we found that the spin period varied dramatically during the RXTE ASM and Swift BAT observations. This variation consists of a long-term spin-up trend, and two ~1,000 day and one ~600 day random walk epochs previously, MJD 51,000, ~MJD 51,400-52,000, and ~MJD 55,100-56,100. We further found that the events appear together with depressions of superorbital modulation amplitude. This provides evidence of the existence of an accretion disk, although the physical mechanism of superorbital modulation remains unclear. Furthermore, the decrease of the superorbital modulation amplitude may be associated with the decrease of mass accretion rate from the disk, and may distribute the accretion torque of the neutron star randomly in time.

Small-Angle X-ray Scattering Station 4C2 BL of Pohang Accelerator Laboratory for Advance in Korean Polymer Science

  • Yoon, Jin-Hwan;Kim, Kwang-Woo;Kim, Je-Han;Heo, Kyu-Young;Jin, Kyeong-Sik;Jin, Sang-Woo;Shin, Tae-Joo;Lee, Byeong-Du;Rho, Ye-Cheol;Ahn, Byung-Cheol;Ree, Moon-Hor
    • Macromolecular Research
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    • v.16 no.7
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    • pp.575-585
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    • 2008
  • There are two beamlines (BLs), 4C1 and 4C2, at the Pohang Accelerator Laboratory that are dedicated to small angle X-ray scattering (SAXS). The 4C1 BL was constructed in early 2000 and is open to public users, including both domestic and foreign researchers. In 2003, construction of the second SAXS BL, 4C2, was complete and commissioning and user support were started. The 4C2 BL uses the same bending magnet as its light source as the 4C1 BL. The 4C1 BL uses a synthetic double multilayer monochromator, whereas the 4C2 BL uses a Si(111) double crystal monochromator for both small angle and wide angle X-ray scattering. In the 4C2 BL, the collimating mirror is positioned behind the monochromator in order to enhance the beam flux and energy resolution. A toroidal focusing mirror is positioned in front of the monochromator to increase the beam flux and eliminate higher harmonics. The 4C2 BL also contains a digital cooled charge coupled detector, which has a wide dynamic range and good sensitivity to weak scattering, thereby making it suitable for a range of SAXS and wide angle X-ray scattering experiments. The general performance of the 4C2 BL was initially tested using standard samples and further confirmed by the experience of users during three years of operation. In addition, several grazing incidence X-ray scattering measurements were carried out at the 4C2 BL.

Surface Properties of Unsaturated Polyester Resin/Siloxane-ester Copolymer Blends (불포화폴리에스테르 수지/실록산-에스테르 공중합체 블렌드의 표면특성)

  • Chang, Young-Wook;Cheong, Yongjoo;Kim, Dongkook;Jung, Jin-Soo
    • Applied Chemistry for Engineering
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    • v.10 no.1
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    • pp.93-97
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    • 1999
  • In order to lower the surface energy of unsaturated polyester(UPE) resin, small amount of siloxane-ester copolymers were incorporated. The copolymers were synthesized by a condensation polymerization using ethylene glycol and hydroxy termintated polydimethylsiloxane as diols and maleic anhydride and phthalic anhydride as dibasic acids. The modified UPE resin surface was characterized by dynamic contact angle (DCA), peel strength measurements of pressure sensitive adhesives and X-ray photoelectron spectroscopy(ESCA). As the copolymer content in the blend and PDMS content in the copolymer are increased, both advancing and receding contact angles against water are increased. The strength required to peel-off the pressure sensitive adhesive tape from the modified UPE resin decreased dramatically with the addition of the copolymer. ESCA results indicated that polydimethylsiloxane segments are predominated at the outer surface of the modified UPE resin.

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Implementation of 3D Video using Time-Shortening Algorithm (시간단축 알고리즘을 통한 3D 동영상 구현)

  • Shin, Jin-Seob;Jeong, Chan-Woong
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.20 no.6
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    • pp.123-128
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    • 2020
  • In this paper, we presents a new cone beam computerized tomography (CBCT) system for the reconstruction of 3 dimensional dynamic images. The system using cone beam has less the exposure of radioactivity than fan beam, relatively. In the system, the reconstruction 3-D image is reconstructed with the radiation angle of X-ray in the image processing unit and transmitted to the monitor. And in the image processing unit, the Three Pass Shear Matrices, a kind of Rotation-based method, is applied to reconstruct 3D image because it has less transcendental functions than the one-pass shear matrix to decrease a time of calculations for the reconstruction 3-D image in the processor. The new system is able to get 3~5 3-D images a second, reconstruct the 3-D dynamic images in real time. And we showed the Rotation-based method was good rather than existing reconstruction technique for 3D images, also found weakness and a solution for it.

The Effect of Unleached Agents on the Stabilization/Solidification of Hazardous Sludge Containing Heavy Metals (有害슬러지 固形化에 따른 重金屬 溶出防止剖의 影饗)

  • 이성호
    • Journal of Environmental Health Sciences
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    • v.19 no.2
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    • pp.46-54
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    • 1993
  • This study was carried out on the stabilized/solidified treatment for the reducing leachability of hazardous heavy metals copper, lead, chromium and cadmium in the hazardous sludge which treated to be unleached heavy metals by sodium diethyl dithiocarbamate. Cement matrix was analyzed for the leachability of 24 hrs and dynamic leaching test, structure and the optimum condition for the stabilization and solidification of the hazardous sludge. In 28 days of curing time the unconfined compressive strength was 21.5 kg/cm$^2$ at the ratio of portland cement (0.5)+fly ash (0.25) and 23.5 kg/cmz at the ratio of portland cement (0.5)+fly ash (0.25) + cake (0.25). High concentration of Pb, Cr and Cd in the sea water and Cu in the distilled water were leached at the dynamic leaching test. The concentration of leaching heavy metals for specimens which were tested 24 hrs were found low leachability with decreasing pH of leachant. According to dynamic leaching test, the low level of copper, lead, cadmium and chromium were leached in the cement matrix with sodium diethyl dithiocarbamate. But the effective diffusion coefficient of unleached cement matrix which was treated sodium diethyl dithiocarbamate was decreased above 2 times than that of cement matrix. The relation of leachant renewal period (Y) and cumulative fraction ion leached (X) was the following regression equations. Solidification with unleached agent. Y$_{Cu}$ = 1413752X + 247, Y$_{Pb}$ = 223501IX + 214, Y$_{Cr}$ = 8310601X - 472, Y$_{Cd}$ = 168787X + 1061 The structure of' solidified matrix with X-ray diffraction analysis was composed more Ca(OH)$_2$, Si, Mg(OH)$_2$ and Al in the unleached cement matrix than those in cement matrix.

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Investigation of Radiation Effects on the Signal and Noise Characteristics in Digital Radiography (디지털 래디오그라피의 신호 및 잡음 특성에 대한 방사선 영향에 관한 연구)

  • Kim, Ho-Kyung;Cho, Min-Kook;Graeve, Thorsten
    • Journal of Biomedical Engineering Research
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    • v.28 no.6
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    • pp.756-767
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    • 2007
  • For the combination of phosphor screens having various thicknesses and a photodiode array manufactured by complementary metal-oxide-semiconductor (CMOS) process, we report the observation of image-quality degradation under the irradiation of 45-kVp spectrum x rays. The image quality was assessed in terms of dark pixel signal, dynamic range, modulation-transfer function (MTF), noise-power spectrum (NPS), and detective quantum efficiency (DQE). For the accumulation of the absorbed dose, the radiation-induced increase both in dark signal and noise resulted in the gradual reduction in dynamic range. While the MTF was only slightly affected by the total ionizing dose, the noise power in the case of $Min-R^{TM}$ screen, which is the thinnest one among the considered screens in this study, became larger as the total dose was increased. This is caused by incomplete correction of the dark current fixed-pattern noise. In addition, the increase tendency in NPS was independent of the spatial frequency. For the cascaded model analysis, the additional noise source is from direct absorption of x-ray photons. The change in NPS with respect to the total dose degrades the DQE. However, with carefully updated and applied correction, we can overcome the detrimental effects of increased dark current on NPS and DQE. This study gives an initial motivation that the periodic monitoring of the image-quality degradation is an important issue for the long-term and healthy use of digital x-ray imaging detectors.

Current Status of the Synchrotron Small-Angle X-ray Scattering Station BL4C1 at the Pohang Accelerator Laboratory

  • Jorg Bolze;Kim, Jehan;Huang, Jung-Yun;Seungyu Rah;Youn, Hwa-Shik;Lee, Byeongdu;Shin, Tae-Joo;Moonhor Ree
    • Macromolecular Research
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    • v.10 no.1
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    • pp.2-12
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    • 2002
  • The small-angle X-ray scattering (SAXS) beamline BL4C1 at the 2.5 GeV storage ring of the Pohang Accelerator Laboratory (PAL) has been in its first you of operation since August 2000. During this first stage it could meet the basic requirements of the rapidly growing domestic SAXS user community, which has been carrying out measurements mainly on various polymer systems. The X-ray source is a bending magnet which produces white radiation with a critical energy of 5.5 keV. A synthetic double multilayer monochromator selects quasi-monochromatic radiation with a bandwidth of ca. 1.5%. This relatively low degree of monochromatization is sufficient for most SAXS measurements and allows a considerably higher flux at the sample as compared to monochromators using single crystals. Higher harmonics from the monochromator are rejected by reflection from a flat mirror, and a slit system is installed for collimation. A charge-coupled device (CCD) system, two one-dimensional photodiode arrays (PDA) and imaging plates (IP) are available its detectors. The overall performance of the beamline optics and of the detector systems has been checked using various standard samples. While the CCD and PDA detectors are well-suited for diffraction measurements, they give unsatisfactory data from weakly scattering samples, due to their high intrinsic noise. By using the IP system smooth scattering curves could be obtained in a wide dynamic range. In the second stage, stating from August 2001, the beamline will be upgraded with additional slits, focusing optics and gas-filled proportional detectors.

Influence of water content on dynamic mechanical properties of coal

  • Gu, Helong;Tao, Ming;Wang, Jingxiao;Jiang, Haibo;Li, Qiyue;Wang, Wen
    • Geomechanics and Engineering
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    • v.16 no.1
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    • pp.85-95
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    • 2018
  • Water affects the mechanical properties of coal and stress wave propagation. To comprehensively investigate the effect of water content on the properties of coal, laboratory tests including X-Ray Diffraction (XRD) analysis, P-wave test, S-wave test, static and dynamic compression test with different water contents were conducted. The compressive strength, elastic modulus and failure strain and their mechanism of coal specimen under coupled static-dynamic load with the increased water content were observed. Meanwhile, energy transmission and dissipation characteristics of a stress wave in coal specimens with different water contents under dynamic load and its relation with the failure features, such as fragmentation and fractal dimension, of coal was analyzed. Furthermore, the dynamic interpretation of water infusion to prevent coal burst based on water infusion model of coal seam roadway was provided.

A Clinical Study on Idiopathic Scoliosis with the Dynamic Corrective Brace (Dynamic Corrective Brace를 이용한 특발성 척추측만증의 치료효과에 관한 증례보고)

  • Kim, Chang-Nyun;Yoon, Min-Young;Lee, Joo-Kang;Min, Ji-Yun;Cho, In-Hee;Kim, Tae-Soo
    • Journal of Acupuncture Research
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    • v.22 no.4
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    • pp.21-26
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    • 2005
  • Objectives : This study is designed to evaluate the Effectiveness of dynamic corrective brace on patient of idiopathic scoliosis. Methods : We have investigated 3 patients with idiopathic scoliosis, confirmed X-ray and weared dynamic corrective brace from December 2003 to December 2004. Results : After 12 months of application with dynamic corrective brace, One case, the T-spine Cobb's angle correctability was 47% and the L-spine was 84%, another case, the L-spine Cobb's angle correctability was 59%, the other case, the T-spine Cobb's angle correctability was 32% and the L-spine was 52%. Conclusion : These results suggest that the dynamic corrective brace was effective treatment modality on patient of idiopathic scoliosis.

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