• The Korean Journal of Community Living Science
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• v.14 no.2
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• pp.125-130
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• 2003

To develop natural dyeing materials from the unused plant materials, we had several dyeing experiments to investigate the optimum conditions of dyeing fabrics with the dyebath extracted from wisteria. Dyeing experiments were done under different dyeing conditions of dyeing temperature, pH of dyebath, dyeing time, concentration of dyebath and mordant treatment which were treated after dyeing. Experimental fabrics were silk, wool, cotton, ramie and hemp. Color difference(ΔE) and Munsell's HV/C of the dyed fabrics and color fastness of silk and cotton fabrics to dry cleaning, washing, rubbing, perspiration and light were measured. In silk and wool fabrics(non mordant, dyeing time-20min), color differences increased in case of dyeing temperature of $100^{\circ}C$, but in cotton, ramie and hemp fabrics, color differences did not increase. Without mordant treatment, color differences of all experimental fabrics were about 10-20, so in wisteria dyeing mordant treatment was necessary. Color differences were increased by the mordant treatment; the color of dyed fabrics with Al mordant is dull yellow, Cu mordant is gold and Fe mordant is olive tone. Color difference was not affected by pH of dyebath in all experimental fabrics. On the whole, the color fastness of dyed silk and cotton fabrics were good, but color fastness to washing and perspiration in Fe mordant was weak and improved in Cu mordant.

• Textile Coloration and Finishing
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• v.13 no.2
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• pp.7-7
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• 2001

This paper investigated the dyeability and surface color of silk and cotton fabrics dyed with chustnut bur extract. Some experiments were performed under the various dyeing conditions such as dyeing temperature, dyeing time, repetition of dyeing, dyeing pH, mordanting condition, washing fastness and light fastness with silk and cotton fabrics. The results obtained were as follows 1. △E value was increased when dyeing temperature and time was higher, value of munsell was shifted from Yellow to Yellow-Red at hither dyeing temperature and time in silk and cotton fabrics. 2. Optimal dyeing pH was increased with acidity of dyeing solution in silk and cotton fabrics, and repetition of dyeing did not change the dye-uptake. 3. When mordanting time and temperature was higher, △E value was larger in silk and cotton fabrics. Silk and cotton fabrics with Fe-premordanting treatment had best dyeability, but treatment with Sn-mordanting was worst. 4. Washing fastness and light fastness was excellent in various dyeing condition at silk fabric but cotton was without practical use.

• Textile Coloration and Finishing
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• v.13 no.2
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• pp.93-103
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• 2001

This paper investigated the dyeability and surface color of silk and cotton fabrics deed with chustnut bur extract. Some experiments were performed under the various dyeing conditions such as dyeing temperature, dyeing time, repetition of dyeing, dyeing pH, mordanting condition, washing fastness and light fastness with silk and cotton fabrics. The results obtained were as follows 1. $\Delta{E}$ value was increased when dyeing temperature and time was higher, value of munsell was shifted from Yellow to Yellow-Red at hither dyeing temperature and time In silk and cotton fabrics. 2. Optimal dyeing pH was increased with acidity of dyeing solution in silk and cotton fabrics, and repetition of dyeing did not change the dye-uptake. 3. When mordanting time and temperature was higher, $\Delta{E}$ value was larger in silk and cotton fabrics. Silk and cotton fabrics with Fe-premordanting treatment had best dyeability, but treatment with Sn-mordanting was worst. 4. Washing fastness and light fastness was excellent in various dyeing condition at silk fabric but cotton was without practical use.

• Textile Coloration and Finishing
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• v.15 no.4
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• pp.32-38
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• 2003

To get the variety of color by natural dyeing, cotton and silk fabrics were dyed with natural indigo and safflower in turn. The two ways of dyeing processes were carried. First, silk and cotton fabrics were dyed repeatedly in safflower dyebath to five times to get the five fabrics dyed in different shades. And then indigo dyeing process was carried on the top of the dyed fabrics with safflower. In second way, the fabrics were dyed in five stages of shade by repetition of dyeing process in indigo dyebath. And then safflower dyeing was carried on the top of the dyed fabrics with indigo. When indigo dyeing process was added on the top of the fabrics dyed in five shades with safflower, the color differences decreased between five shades of fabrics, their color values got similar in hue, shade and chroma. When safflower dyeing process was added on the top of the fabrics dyed in five shades with indigo, the fabrics showed different hue of colors between red and blue of Munsell color circle such as RP, P and PB. Like almost of fabrics dyed with plants materials, the lightfastness and laundering fastness of dyed samples were poet and drycleaning fastness were good.

• Korean Journal of Rural Living Science
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• v.8 no.2
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• pp.73-81
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• 1997

Parsimon juice dyeing is the one of the most popular natural dyeing methods which have been done traditionally among the farmers. The clothes dyed with parsimon juice has several merits, that is, it become much more durable, cool, easy to wash and wear after dyeing and these merits are the reason why people likes to wear the parsimon juice dyeing clothes as work wear. Especially in Cheju province, parsimon juice clothes became a folk costume and many people still enjoy wearing it in the hot summer days. But one of the demerits of parsimon dyeing is that the possible period of dyeing is very short. So, if parsimon juice dyeing could be done with the preserved parsimon juice, it would be possible to enlength the period. With this idea, we compared the color and colorfastness of fabrics which were dyed with 4 kinds of parsimon juice. The experimental parsimon juice 96-8 was preserved during 13 months, 96-9 was 12 months, 97-8 was 1 month and 97-9 was not preserved one. The experimental fabrics were cotton, silk. nylon and polyester fabrics. The results were as follows ; 1. The colors of fabrics dyed with experimental parsimon juice 96-9, 97-8, 97-9 were yellow-red and dyeing states were good. But the colors of fabrics dyed with 96-8 were dark and the state were bad, because the color of experimental parsimon juice 96-8 was changed during preservation. 2. The best state of dyeing could see in the fabrics dyed with experimental parsimon juice 97-8, although that was preserved 1 month. 3. There were differences of color between experimental fabrics dyed with same juice and the colors were thicker in cotton and silk than in nylon and polyester fabrics. 4. During wetting and drying process, the color changes in fabrics dyed with no preserved one were more than in fabrics dyed with preserved ones. 5. The color fastness to the light of the dyed fabrics was over 4, to the acidic perspiration was 3~4 or 4~5, to the alkaline perspiration was 2, 3 or 3~4 and to the washing was 1~2. There was no significant difference in colorfastness between the 96-9 dyed fabrics and 97-9 dyed fabrics.

• Textile Coloration and Finishing
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• v.16 no.3
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• pp.1-7
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• 2004

To study the dyeability(K/S value) and surface color of silk fabrics dyed with Impatiens balsamina extract, its flower, leaf and stem, was extracted by water. This paper investigated some experiments with Impatiens balsamina extract under the various dyeing conditions such as dyeing temperature, dyeing time, repetition of dyeing, dyeing pH with silk fabrics. The results obtained were as follows. 1. It was found that it $\lambdamax$. of silk fabrics dyed with Impatiens balsamina extract was 260nm and its flower, leaf, stem and flowers(white, pink, violet) had same it $\lambdamax$ at 260nm. 2. K/S value was increased when dyeing temperature, repetition of dyeing and time was higher, value of munsell of silk fabrics dyed with Impatiens balsamina extract was yellow-red. dyeing temperature, repetition of dyeing and time was higher, shifted to longer wavelength side. 3. pH added acetic acid was colored reddish yellow-red, but pH added alum was colored yellowish yellow-red in silk fabrics dyed with Impatiens balsamina extract and repetition of dyeing was increased the dye-uptake.

• Textile Coloration and Finishing
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• v.16 no.1
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• pp.18-25
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• 2004

In this study, the effect of microwave which can increase temperature rapidly on polyester alkaline dyeing was investigated. The final K/S values of polyester fabrics dyed by microwave lower than those of atmospheric dyeing because of the evaporation loss of dyeing solution. If the dyeing time makes longer as much as that in atmospheric dyeing, the K/S values of polyester fabrics dyed under microwave were similar to those of atmospheric dyeing. The K/S values of polyester fabrics dyed in pH 9.5 were higher than those in pH 5.5 in case of aliphatic carriers. The K/S values of organic reagent pretreated polyester fabrics dyed by use of aromatic carriers were not higher than those of non-treated polyester fabrics. But the K/S values of polyester fabrics dyed by use of aliphatic carriers were higher than those of non-treated polyester fabrics. The tensile strength were decreased with increasing of dyebath pH because the polyester fabrics were easily decomposed by high alkali.

• Journal of the Korean Home Economics Association
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• v.42 no.7
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• pp.63-72
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• 2004

This study discussed the dyeing of wool and cotton fabrics with Betel Palm Tree White woolen fabrics and cotton fabrics purchased from HATH (Korea Apparel Testing ＆ Research Institute) were used as experimental fabrics. Using dyeing powder extracted from dyeing material, various temperatures, dyeing times, and pH were used in the dyeing process. Al, Cr, Fe, Cu, and Sn were used as mordant and the absorption was compared with different mordanting methods. The optimum condition for pre-mordanting dyeing was dye concentration of 25% (o.w.f) and mordant concentration of 0.5$^{\circ}$∼1%. Woolen fabric showed an increase of absorption and the maximum absorption was achieved at weak acidity. According to the mordanting methods, woolen fabrics and cotton fabrics were treated with various mordanting agents, a mordant rate of 1:100, at 60$^{\circ}C$, for 30 minutes and dyed with a dyeing material concentration of 25% (o.w.f), at a rate of 1:100, at 60$^{\circ}C$ for 60 minutes. The best dyeing effect w3s achieved at the temperature of 60$^{\circ}C$ for cotton and 80$^{\circ}C$ for wool fabrics. The light fastness of cotton and wool fabrics was low and particularly the fastness to perspiration was decreased with Fe mordanting. I concluded that pre-mordanting method was better than post-mordanting method for cotton and woolen fabrics.

• Fashion & Textile Research Journal
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• v.14 no.5
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• pp.866-877
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• 2012

The natural dyeing of hanji cotton fabrics with guava leaf extract was investigated. The temperature and time of dyeing were $40^{\circ}C$ and $90^{\circ}C$ for eighty minutes, respectively. In addition, the dyebath has been set at pH 5. Sn pre-mordanted fabrics showed the highest K/S value. Regardless of dyeing temperature, K/S values were high when Al, Cu, Fe-mordanted fabrics were dyed in post-mordanting and Sn-mordanted fabrics in pre-mordanting. The dyeing equilibrium was shown at the fourth time of repeated dyeing. In the processing of hanji cotton fabrics, K/S value was high when hanji cotton fabric was treated with soybean milk at $90^{\circ}C$. Similar K/S value of dyeing was shown when fabrics were processed with chitosan, regardless of dyeing temperature. High K/S value of dyeing was seen when fabrics processed with gallnut tannin at 40. Fabrics dyed with acidic water extract showed yellowish color. Fabrics dyed with alkaline water extract showed reddish color, and fabrics dyed with ethanol extract showed greenish yellow color. In case of Sn-mordanted fabrics, the washing fastness level was between 3 to 4, and other dyed fabrics showed low fastness. The dry cleaning fastness also showed very excellent result with level 4-5. The rubbing fastness of the fabrics was better in dry rubbing than in wet rubbing. For the light fastness, all dyed fabrics showed low fastness. For antibacterial activity, the dyed fabrics with guava leaf extract showed 99.9% of high antibacterial activity. Hanji cotton fabric maintained certain deodorization in the state of raw fabric. All dyed fabrics showed higher UV protection rate than control fabric.

• Fashion & Textile Research Journal
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• v.4 no.1
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• pp.79-85
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• 2002

To develope natural dyeing materials from the unused plant materials, we had several dyeing experiments to investigate the optimum conditions of dyeing fabrics with the waste grape juice. Dyeing experiments were done under different dyeing conditions of dyeing time, dyeing temperature, pH and concentration of dyebath and mordants which were treated after dyeing. Experimental fabrics were silk, cotton, ramie and hemp. Color difference(${\Delta}E$) and Munsell's HV/C of the dyed fabrics and color fastness of silk dyed fabrics to dry cleaning, washing, rubbing, perspiration and light were measured. The color differences of dyed experimental fabrics were very slightly increased with dyeing time and the color of dyed silk was light purple and the cotton, ramie and hemp was light red purple. The color differences of dyed experimental fabrics were decreased and the color became lighter with dyeing temperature increased. The color differences of dyed experimental fabrics were decreased and the color changed from light purple to blue with the pH of dyebath increased. The color differences of dyed experimental fabrics were slightly increased with the concentration of dyebath increased. The color of dyed fabric changed with the mordant treatment and were different among the experimental fabrics. On the whole, blue tone increased with the Al and Fe mordant and green tone increased with the Cu mordant. The color fastness of dyed silk fabrics to light, washing (change) and perspiration (change) was bad and color fastness to dry cleaning and rubbing were good.