• 제목/요약/키워드: Duplex Stainless Steel

검색결과 189건 처리시간 0.033초

Duplex Stainless Steel(DSS) 침의 생화학적 안전성 (Biochemical Safety of Duplex Stainless Steel Acupuncture Needle)

  • 육근영;이승호;김영곤;이승헌;홍상민;임사비나
    • Journal of Acupuncture Research
    • /
    • 제24권6호
    • /
    • pp.195-206
    • /
    • 2007
  • Objectives : The aim of this study is to investigate the safety of Acupuncture needles made from duplex stainless steel. Methods : In order to check the safety concern of the DSS Acupuncture needle, we employed biochemical measures, DSS and SS304 Acupuncture needles were tested for pH level, heavy metals and UV absorbance spectrum along with cytotoxicity and hemolysis. As a guideline, we have referred to the 'standards for acupuncture needles', 'standards for disposable needles' and 'standards and experimental procedures for stents' for the Korean Food & Drug Administration(KFDA). Results & Conclusions : The DSS Acupuncture needle extract satisfied these requirements. There was no significant difference between the DSS and SS304 Acupuncture needle extract. In conclusion, the DSS Acupuncture needle displayed biochemical safety.

  • PDF

Effects of Sigma ($\sigma$) Phase on the Pitting Corrosion of 25% Cr Duplex Stainless Steel; Investigations by means of Electrochemical Noise Measurement

  • Park, Chan-Jin;Kwon, Hyuk-Sang;Kim, Hee-San
    • Corrosion Science and Technology
    • /
    • 제2권1호
    • /
    • pp.18-25
    • /
    • 2003
  • Effects of the precipitation of $\sigma$ phase on the metastable pitting as a precursor of stable pitting corrosion and also on the progress of stale pitting of the 25Cr-7Ni-3Mo-0.25N duplex stainless steel were investigated in chloride solution. Electrochemical potential and current noises of the alloy were measured in 10 % ferric chloride solution ($FeCl_3$) with zero resistance ammeter (ZRA), and then analyzed by power spectral density (PSD) and by corrosion admittance ($A_c$) spectrum. With aging at $850^{\circ}C$, the passive film of the alloy was found to get significantly unstable as represented by power spectral density (PSD) and a transition from metastable pitting state to stable one was observed. In the corrosion admittance spectrum, the number of negative $A_c$ corresponding to the state of localized corrosion increased with aging, suggesting that the precipitation of $\sigma$ phase considerably degraded the passive film by depleting Cr and Mo around it at $\alpha/\sigma$ or $\gamma/\sigma$ phase boundaries, thereby leading to the initiation of the pitting corrosion. However, the Cr and Mo at $\alpha/\sigma$ or $\gamma/\sigma$ phase boundaries which were once depleted due to the precipitation of the $\sigma$ phase were partly replenished by the diffusion of Cr and Mo from the surrounding matrix with aging time longer. The initiation of pitting seems to be associated with the precipitation density of the $\sigma$ phase with an effective size needed to induce the sufficient depletion of Cr and Mo around it.

Influences of boron and silicon in insert alloys on microstructure and isothermal solidification during TLP bonding of a duplex stainless steel using MBF-35 and MBF-30

  • 원신건;김명복;강정윤
    • 대한용접접합학회:학술대회논문집
    • /
    • 대한용접접합학회 2009년 추계학술발표대회
    • /
    • pp.59-59
    • /
    • 2009
  • The influences of B and Si in the filler metals on microstructure and isothermal solidification during transient liquid-phase (TLP) bonding of a nitrogen-containing duplex stainless steel with MBF-30 (Ni-4.5wt.%Si-3.2wt.%B) and MBF-35 (Ni-7.3wt.%Si-2.2wt.%B), were studied at the temperature range of $1030-1090^{\circ}C$ with various times from 60 s to 3600 s under a vacuum of approximately $10^{-5}$ Torr. In case of the former, BN, $Ni_3B$ and $Ni_3Si$ precipitates were formed in the bonding region. BN and $Ni_3Si$ secondary phases were present in the joint for the latter case. The formation of $Ni_3B$ within the joint centerline is dependent on B content. The morphology of $Ni_3Si$ is dominated by Si concentration. A difference between the times for complete isothermal solidification obtained by the experiments and the conventional TLP bonding diffusion model was observed when using MBF-35. According to the simulated results, the isothermal solidification completion time for MBF-35 case was smaller than that in MBF-30. However, this experimental value obtained using MBF-35 was notably larger than that obtained using MBF-30. Isothermal solidification of liquid MBF-30 is controlled by the first isothermal solidification regime dependent on B diffusion model, whereas that of liquid MBF-35 experiences two isothermal solidification regimes and is mainly controlled by the second isothermal solidification dependent on Si diffusion model. In addition, only if Si content exceeds a critical value, the slower 2nd solidification regime will commence.

  • PDF

화학적 부동태 처리에 따른 듀플렉스 스테인리스 강의 피막 특성에 관한 연구 (Study on Passive Layer Characteristics of Chemically Passivated Duplex Stainless Steel)

  • 장휘운;이정훈;김용환;정원섭
    • 한국표면공학회지
    • /
    • 제45권6호
    • /
    • pp.219-225
    • /
    • 2012
  • The aim of the present study was to investigate the corrosion resistance and characteristics of passive layer between naturally passivated and chemically passivated duplex stainless steel, UNS S31803 (EN 1.4462) using CPT, XPS, and EIS. The treatment of $HNO_3$(II) and $HNO_3$(III) in ASTM A 967 was applied. In case of chemically passivated specimen, CPT of $HNO_3$(II) and $HNO_3$(III) were higher than that of naturally passivated specimen. In addition, from XPS results, the protectiveness index (Cr/(Fe+Cr)) of chemically passivated specimens was also higher than that of naturally passivated specimen. The reason for this result is considered due to post-cleaning treatment in chemical passivation process, that is, immersion in $Na_2Cr_3O_7$ solution. The fact that $HNO_3$(II) passivation treatment showed the highest film resistance and 'n', which is exponent related with constant phase element (CPE) of passivation film, was in good agreement with results of CPS and XPS. The chemical passivation treatment was an effective method to improve corrosion resistance of duplex stainless steel.