• Journal of Mechanical Science and Technology
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• v.18 no.9
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• pp.1604-1613
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• 2004

This paper presents an effective and reliable evaluation method for fracture strength and material degradation of the micro-structure of high temperature service steel weldment using advanced small punch (ASP) test developed from conventional small punch (CSP) test. For the purpose of the ASP test, a lower die with a minimized ${\Phi}$1.5 mm diameter loading ball and an optimized deformation guide hole of ${\Phi}$3 mm diameter were designed. The behaviors of fracture energy (E$\_$sp/), ductile-brittle transition temperature (DBTT) and material degradation from the ASP test showed a definite dependency on the micro-structure of weldment. Results obtained from ASP test were compared and reviewed with results from CSP test, Charpy impact test, and hardness test. The utility and reliability of the proposed ASP test were verified by investigating fracture strength, behavior of DBTT, and fracture location of each micro-structure of steel weldment for test specimen in ASP test. It was observed that the fracture toughness in the micro-structure of FL＋CGHAZ and ICHAZ decreased remarkably with increasing aging time. From studies of all micro-structures, it was observed that FGHAZ microstructure has the most excellent fracture toughness, and it showed absence of material degradation.

• Journal of Welding and Joining
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• v.7 no.4
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• pp.56-67
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• 1989

In this study, the possibility of evaluating the peculiar fracture strength of weldment in high strength steels was investigated by means of a small punch(SP) test. In order to obtain the ductile-brittle transition temperature(DBTT) of SP energy by which the fracture strength of weldment in structural steels such as SS41 and SM53B steels had been evaluated in our preceding publication, the effects of notches and loading rates on SP energy were discussed. It was found that the correspondence of SP energy to critical COD at test temperature -196.deg. C showed a linear relation with some deviation. The empirical correlation with scatter band, Esp/(Esp)p = 1.67[.delta./(.delta./sub c//(.delta./sub c/)/sub p/]-0.55, was developed between the SP energy ratio and critical COD ratio of each weld structure compared with parent material at test temperature -196.deg. C. In addition, there did not appear to be a significant effect of test materials and specimen size etc. on the correlation.

• Transactions of the Korean Society of Mechanical Engineers
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• v.15 no.5
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• pp.1665-1673
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• 1991

본 연구에서는 운전이력이 다른 보일러 과열기 및 재열기에서 수취한 Cr-Mo강 증기관을 대상으로 이 SP 시험법을 도입하여 SP시험에 의한 재질열화의 평가 가능성을 연구 검토하였다.

• Korean Journal of Materials Research
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• v.11 no.6
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• pp.508-511
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• 2001

Experimental studies of the brittle-ductile transition (BDT) for pre-cracked sapphire single crystals were carried out. The BDT temperature in sapphire single crystals were $1000\pm$$25^{\circ}C$ and 1100$\pm$$25^{\circ}C$ at constant strain rate 3.3$\times$$10^{-5}$/sec and 3.3$\times$$10^{-6}$/sec, respectively. With aid of the BDT model, the activation energy for prism plane slip {1120} <1100> dislocation velocity was in the range of 4.6$\pm$2.3eV This activation energy for dislocation velocity with BDT model was compatible with the result of the dislocation velocity (3.8eV) using the etch-pit techniques.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1161-1162
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• 2006

In order to overcome the recrystallization embrittlement and irradiation embrittlement of Mo, which are major problems for its fusion applications, internally nitrided Mo alloys were prepared by a novel multi-step internal nitriding. Neutron irradiation was performed in the Japan Material Testing Reactor (JMTR). After irradiation, nitrided Mo alloys exhibited $\iota$ ower ductile-brittle transition temperature than irradiated TZM. These results suggested that multi-step internal nitriding was effective to the improvement in the embrittlement by irradiation. Transmission electron microscope observation revealed that TiN particles precipitated by nitriding acted as a sink for irradiation-induced defects.

• Journal of Welding and Joining
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• v.7 no.3
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• pp.28-35
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• 1989

It was reported that the toughness for welded region was influenced by various factors such as the gradient for prior austenite grain size, the variation of microhardness and the characteristic microstructure depending on distance from the fusion boundary. Therefore, in order to evaluate the fracture strength of the weldment in which the microstructures change continuously, it is important to assess the peculiar strength of each microstructure in welded region. It was known that the small punch(SP) test technique which was originally developed to study the irradiation damage effect for the structures of nuclear power plant was also useful to investigate the strength evaluating of nonhomogeneous materials. In this paper, by means of a small punch test technique the possibility of evaluating strength of parent and welded region in SS41 and SM53B steels was investigated. The obtained results are summerized as follows: 1) The small punch test which showed markedly the ductile-brittle transition behavior in this experiment may be applied to evaluation for the fracture strength of welded region. 2) It was shown that the ductile-brittle regime lied in Region III(plastic membrane stretching region) of the flow characteristics observed in SP test. 3) The SP test technique which shows a more precipitous energy change transition behavior than the other test technique is able to estimate the more precise transition temperature. 4) It could be seen that in comparision with the structure of parent the structure of weld HAZ in SS41 steel was improved while it in SM53B steel was deteriorated.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.24 no.6 s.177
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• pp.1398-1407
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• 2000

The structural steels of power plant show the decrease of mechanical properties due to degradation such as temper embrittlement, creep damage and softening during long-term operation at high temper ature. The typical causes of material degradation damage are the creation and coarsening of carbides(M23C6, M6C) and the segregation of impurities(P, Sb and Sn) to grain boundary. It is also well known that material degradation induces the cleavage fracture and increases the ductile-brittle transition temperature of steels. So, it is very important to evaluate degradation damage to secure the reliable and efficient service condition and to prevent brittle failure in service. However, it would not be appropriate to sample a large test piece from in-service components. Therefore, it is necessary to develop a couple of new approaches to the non-destructive estimation technique which may be applicable to assessing the material degradation of the components with not to influence their essential strength. The purpose of this study is to propose and establish a new electrochemical technique for non-destructive evaluation of material degradation damage for Cr-Mo steels which is widely used in the high temperature structural components. And the electrochemical anodic polarization test results are compared with those of semi-nondestructive SP test.

• Nuclear Engineering and Technology
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• v.34 no.6
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• pp.574-585
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• 2002

The microstructural characteristics and its related mechanical properties of RPV cladding have been investigated using small punch (SP) tests. SA508 Cl.3 RPV steel plates were overlay cladded with the type ER309L welding consumables by submerged arc welding process. Although the RPV clad material had a small portion of 5 ferrite phase, it still showed the ductile to brittle transition behavior The transition temperature was determined by the SP test and it depended on the content of $\sigma$ phase, specimen size, and determination methods. The fracture appearance of SP specimen was changed from circumferential to radial cracking as test temperature became low, and below the transition temperature region, ER309L cladding usually fractured along the 6 ferrite by the low temperature failure of ferrite phase.

• Elastomers and Composites
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• v.39 no.2
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• pp.142-152
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• 2004

Tensile tests of two types of injection-molded polystyrene(PS) samples have been carried out over a wide range of temperature and strain rates in order to characterize their crazing behaviors. Mechanical properties were affected by the formation of crazes as well as test variables. Below the brittle-ductile transition temperature, the tensile stress and the ultimate elongation increased with the molecular weight, strain rate, and with decreasing temperature while the number and average length of crazes also increase. The crazing stress increased with molecular weight, strain rate, and with decreasing temperature. However, the dependence was small compared to the tensile stress. The gap between crazing stress and tensile stress which represents time fur craze formation and growth increased with molecular weight, strain rate, and with decreasing temperature. Crazing was activated near the ${\beta}$-relaxation temperature; crazing stress abruptly decreased at this temperature. During the tensile test, the craze density changed exponentially with the applied stress. At the initial stage, crazes formed slowly. Once a certain number of craze formed, however, the craze density increased rapidly. Craze nucleation and growth occur simultaneously.

• Journal of the Korean Institute of Gas
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• v.2 no.4
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• pp.42-46
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• 1998

Miniaturized specimen technology Permits mechanical behavior to be determined using a minimum volume of material. The technology is useful in case of not collecting a large amount of materials from industrial equipments. Five kinds of accelerated degradation materials were prepared by isothermal aging heat treatment at $630^{\circ}C$. Three kinds of specimens were prepared for impact testing. In order to increase plastic constraint of subsize specimen, side-groove was introduced. Results between subsize and full size impact testing were compared. Size effects correlations were developed for the impact properties of turbine rotor material. These correlations successfully predict the ductile brittle transition temperature (DBTT) of full size Charpy impact specimens based on subsize specimen data.