• Proceedings of the KSME Conference
• /
• 2008.11a
• /
• pp.1-6
• /
• 2008

Due to the self-similarity of Berkovich and conical indenters, different materials may show the same loaddepth curve for single indentation. In this study, we first compare the load-depth characteristics of conical and Berkovich indenters via finite element method. We also analyze the variation of load-depth curves with angle of Berkovich indenter, indentation parameters, and material properties. With numerical regressions of obtained data, we then propose dual-Berkovich indentation formulae for material property evaluation. The proposed approach provides the values of elastic modulus, yield strength and strain-hardening exponent and corresponding stress-strain curve with an average error of less than 3%. The method is valid for any elastic indenters made of tungsten carbide and diamond for instance.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.36 no.1
• /
• pp.17-28
• /
• 2012

In this study, we suggest a method for material property evaluation by dual-triangular pyramidal indenters using the reverse analysis. First, we demonstrated that load-displacement curves of conical and triangular pyramidal indenters are different for the same material. For this reason, an independent research on the triangular pyramidal indenter is needed. From FE indentation analyses on various materials, we then investigated the relationships among material properties, indentation parameters and load-displacement curves. From this, we established property evaluation formula using dual-triangular pyramidal indenters having two different half-included-angles. The approach provides the values of elastic modulus, yield strength and strain-hardening exponent within an average error of 3% for various materials.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.33 no.9
• /
• pp.859-869
• /
• 2009

The sharp indenters such as Berkovich and conical indenters have a geometrical self-similarity in theory, but different materials have the same load-depth curve in case of single indentation. In this study, we analyze the load-depth curves of conical indenter with angles of indenter via finite element method. From FE analyses of dual-conical indentation test, we investigate the relationships between indentation parameters and load-deflection curves. With numerical regressions of obtained data, we finally propose indentation formulae for material properties evaluation. The proposed approach provides stress-strain curve and the values of elastic modulus, yield strength and strain-hardening exponent with an average error of less than 2%. It is also discussed that the method is valid for any elastically deforming indenters made of tungsten carbide and diamond for instance. The proposed indentation approach provides a substantial enhancement in accuracy compared with the prior methods.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2002.05a
• /
• pp.154-157
• /
• 2002

A cyto-indentation technique was used to obtain the biomechanical compressive compliance property of an chondrocyte cell attached to glass surface, which was tried to generate joint cartilage by tissue engineering. Piezo-transducer system and dual photo-diode system were used to conduct mechanical indentation through displacement-controlled testing and the measurement of corresponding cell reaction force. The Poisson's ratio of 0.37 was quoted from other report. The compressive compliance of chondrocyte, that was determined by elastic contact theory, was 1.38${\pm}$0.057 kPa. This value is 30% higher than that of MG63 osteoblast-like cell. The cyto-indentation technique employed in this study is so precise that it can quantify the biomechanical property of single cell.

• Journal of Powder Materials
• /
• v.18 no.1
• /
• pp.64-72
• /
• 2011

Nondestructive instrumented indentation test is the method to evaluate the mechanical properties by analyzing load - displacement curve when forming indentation on the surface of the specimen within hundreds of micro-indentation depth. Resistance spot welded samples are known to difficult to measure the local mechanical properties due to the combination of microstructural changes with heat input. Particularly, more difficulties arise to evaluate local mechanical properties of resistance spot welds because of having narrow HAZ, as well as dramatic changed in microstructure and hardness properties across the welds. In this study, evaluation of the local mechanical properties of resistance spot welds was carried out using the characterization of Instrumented Indentation testing. Resistance spot welding were performed for 590MPa DP (Dual Phase) steels and 780MPa TRIP (Transformation Induced Plasticity) steels following ISO 18278-2 condition. Mechanical properties of base metal using tensile test and Instrumented Indentation test showed similar results. Also it is possible to measure local mechanical properties of the center of fusion zone, edge of fusion zone, HAZ and base metal regions by using instrumented indentation test. Therefore, measurement of local mechanical properties using instrumented indentation test is efficient, reliable and relatively simple technique to evaluate the tensile strength, yield strength and hardening exponent.

• Proceedings of the KSME Conference
• /
• 2003.04a
• /
• pp.1321-1325
• /
• 2003

Nickel thin film is one of the most important materials used in micromachined structure. To measure the mechanical properties of electroplated nickel thin film, two techniques are adopted and compared quantitatively with. One is nano-indentation test to measure the elastic modulus. The other is tensile test to measure not only elastic modulus but also yield strength and plastic deformation, ultimate strength. To perform the tensile test, the test apparatus was constructed with linear guided servo motor for actuation, load cell for force measurement and dual microscope for strain measurement.

• Journal of Adhesion and Interface
• /
• v.22 no.2
• /
• pp.47-56
• /
• 2021

Steel plates coated by self-healable polymer still can be rusted since it takes time to be healed. In this study, dual self-healing coating material is developed using corrosion inhibitor (DTBEDA) which can form hindered urea (HUB) as reversible cross-linking bond at the same time. Developed dual self-healing polymer is coated on steel plate, and scratch healing property was investigated by surgical blades and nano/micro indentation tester. The anticorrosion effect of DTBEDA was investigated by electrochemical impedance spectroscopy (EIS).

• Korean Journal of Metals and Materials
• /
• v.49 no.12
• /
• pp.967-976
• /
• 2011

Conventional fracture tests of resistance spot welds have been performed without consideration of the paint baking process in the automobile manufacturing line. The aim of this paper is to investigate the effect of the paint baking process on load carrying capacity and fracture mode for resistance spot welded 590 dual phase (DP), 780DP, 980DP, 590 transformation in duced plasticity (TRIP), 780TRIP and 1180 complex phase (CP) steels. With paint baking after resistance spot welding, the l-shape tensile test (LTT) and nano-indentation test were conducted on the as-welded and paint baked samples. Paint baking increased the load-carrying capacity of the resistance spot welded samples and improved the fracture appearance from partial interfacial fracture (PIF) to button fracture (BF). Improvement in fracture appearance after LTT is observed on weldments of 780 MPa grade TRIP steels, especially in the low welding current range with paint baking conditions. The higher carbon contents (or carbon equivalent) are attributed to the low weldability of the resistance spot welding of high strength steels. Improvement of the fracture mode and load carrying ability has been achieved with ferrite hardening and carbide formation during the paint baking process. The average nano-indentation hardness profile for each weld zone shows hardening of the base metal and softening of the heat affected zone (HAZ) and the weld metal, which proves that microstructural changes occur during low temperature heat treatment.

• Proceedings of the Korean Vacuum Society Conference
• /
• 2011.08a
• /
• pp.177-179
• /
• 2011

The purpose of this study is to enhance an adhesion between substrate and Diamond-like Carbon (DLC) film. DLC has many outstanding properties such as low friction, high wear resistance and corrosion resistance. However, it is difficult to achieve enough adhesion because of weak bonding between DLC film and the substrate. For improvement adhesion, a layer between DLC film and the substrate was prepared by dual post plasma. DLC film was deposited on nitrided layer by linear ion source. The composed compound layer between substrate and DLC film was investigated by Glow Discharge Spectrometer (GDS) and Scanning Electron Microscope (SEM). The synthesized bonding structure of DLC film was analyzed using a micro raman spectrometer. Mechanical properties were measured by nano-indentation. In order to clarify the mechanism for improvement in adhesive strength, it was observed by scratch test.

• Structural Engineering and Mechanics
• /
• v.7 no.6
• /
• pp.575-588
• /
• 1999

A boundary element method is applied to the analysis of crack trajectory in materials with complex microstructure, such as discontinuously reinforced composite materials, and systems subjected to complex loading, such as indentation. The path followed by the crack(s) has non-trivial geometry. A study of the stress intensity factors and fracture toughness of such systems must therefore be accompanied by an analysis of crack trajectory. The simulation is achieved using a dual boundary integral method in planar problems, and a single boundary integral method coupled with substructuring in axisymmetric problems. The direction of crack propagation is determined using the maximum mechanical energy release rate criterion. The method is demonstrated by application to (i) a composite material composed of components having the elastic properties of aluminium (matrix) and silicon carbide (reinforcement), and (ii) analysis of contact damage induced by the action of an indenter on brittle materials. The chief advantage of the method is the ease with which problems having complex geometry or loading (giving rise to complex crack trajectories) can be treated.