• 소성∙가공
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• 제31권5호
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• pp.290-295
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• 2022

Recently, the use of high-tech ceramic parts in functional electronic parts, automobile parts and semiconductor equipment parts is increasing. These ceramics materials are required to have high reproducibility, reliability, large size and complex shapes. The researchers initiated the work to develop a new shaping method called gel casting, which allows high performance ceramic materials with a complex shape to be produced. The manufacturing process parameters of gel casting include uniform mixing of the initiator, bubble removal, and slip injection. In this study, we analyzed the dispersion and gelation characteristics according to the change in the additive content of the alumina slurry in the gel casting process. The alumina slurry for gel casting was prepared by mixing a solvent, a monomer and a dispersant through a ball mill. Alumina powder and a gelation initiator were added to the mixed solution, and ball milling was performed for 24 hours. A viscosity of 6,435 cps and a stable zeta potential value were obtained under the conditions of alumina powder content of 55 vol% and dispersant 2.0 wt%. After curing for 12 hours by adding aps 0.1wt%, TEMED 0.2wt%, and Monomer 3, 5wt%, it was possible to separate from the molding cup, confirming that the gelation was completed.

• Advances in nano research
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• 제15권2호
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• pp.175-189
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• 2023

The under-evaluation structure includes a functionally graded porous (FGP) core which is confined by two piezoelectric carbon nanotubes reinforced composite (CNTRC) layers. The whole structure rests on the Pasternak foundation. Using quasi-3D hyperbolic shear deformation theory, governing equations of a sandwich plate are driven. Moreover, face sheets are subjected to the electric field and the whole model is under thermal loading. The properties of all layers alter continuously along with thickness direction due to the CNTs and pores distributions. By conducting the current study, the results emerged in detail to assess the effects of different parameters on buckling of structure. As instance, it is revealed that highest and lowest critical buckling load and consequently stiffness, is due to the V-A and A-V CNTs dispersion type, respectively. Furthermore, it is revealed that by porosity coefficient enhancement, critical buckling load and consequently, stiffness reduces dramatically. Current paper results can be used in various high-tech industries as aerospace factories.

• 한국전기전자재료학회논문지
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• 제36권2호
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• pp.164-169
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• 2023

Nano Pt particles were dispersed on carbon-based supports by a polyol process for a catalyst application in a polymer electrolyte fuel cell. We tried to optimize the effect of pH on the electrostatic forces between the support and the Pt colloids. We investigated the relationship among the surface charges on the carbon support, the solution pH, and the concentration of a glycolate, and the Pt particle size. The produced catalyst with nano Pt particles on the support was evaluated by the long-term cyclic voltammetry (CV) performance test and compared with the results from a commercial catalyst. Our experimental results reveal that the pH-control can modify the particle size distribution and the dispersion of the nano Pt particles. This resulted in a cost-effective method for the synthesis of highly Pt loaded Pt/C catalysts for fuel cells better than a commercial catalyst system.

• Advances in nano research
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• 제14권5호
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• pp.463-474
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• 2023

The purpose of this paper is to present the analysis of propagating and evanescent waves in functionally graded (FG) nanoplates with the consideration of nonlocal effect. The analytical integration nonlocal stress expansion Legendre polynomial method is proposed to obtain complete dispersion curves in the complex domain. Unlike the traditional Legendre polynomial method that expanded the displacement, the presented polynomial method avoids employing the relationship between local stress and nonlocal stress to construct boundary conditions. In addition, the analytical expressions of numerical integrations are presented to improve the computational efficiency. The nonlocal effect, inhomogeneity of medium and their interactions on wave propagation are studied. It is found that the nonlocal effect and inhomogeneity of medium reduce the frequency bandwidth of complex evanescent Lamb waves, and make complex evanescent Lamb waves have a higher phase velocity at low attenuation. The occurrence of intersections of propagating Lamb wave in the nonlocal homogeneous plate needs to satisfy a smaller Poisson's ratio condition than that in the classical elastic theory. In addition, the inhomogeneity of medium enhances the nonlocal effect. The conclusions obtained can be applied to the design and dynamic response evaluation of composite nanostructures.

• 품질경영학회지
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• 제51권3호
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• pp.419-434
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• 2023

Purpose: Measurement results obtained under non-ideal measurement environment conditions may contain uncertain factors. As a result, the reliability of measurement results may be deteriorated. In this study, we tried to find ways to improve quality by evaluating and applying measurement uncertainty based on GUM. Methods: In the flatness measurement of semiconductor parts, uncertainty factors that could occur under actual environmental conditions of workers were derived, and measurement uncertainties were calculated, and methods for minimizing the main factors affecting the measurement results were analyzed. Results: Depending on the part and the coordinate measuring machine, it was shown that the effect of dispersion caused by repeated measurements as type A uncertainty and the effect of the calibration results of equipment as type B uncertainty have the main influence. Conclusion: Depending on the uncertainty factors of type A and type B and the influence of the total expanded uncertainty, the central value and confidence interval of the initial measurement results showed fluctuations. It is considered that analysis and measures for the main uncertainty factors are needed as quality improvement in the industrial field.

• 접착 및 계면
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• 제10권2호
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• pp.90-97
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• 2009

세 가지의 다른 산처리를 한 단일 탄소섬유로 함침된 CNT-에폭시 나노복합재료는 전기-미세역학적 기술과 젖음성 시험법을 사용하여 분산과 자체-감지능을 조사하였다. 자체-감지능은 접촉저항의 노이즈가 산 처리되지 않은 CNT보다, 산 처리된 단일 탄소섬유 CNT-에폭시 나노복합재료가 다소 더 크게 나타났다. 반면에, 겉보기 강성도는 산 처리를 한 경우가 응력전달이 더 잘되어, 산처리 하지 않은 경우보다 더 컸다. 탄소섬유와 CNT-에폭시간의 계면전단강도는 CNT 첨가로 인하여 점도가 증가하기 때문에 탄소섬유와 순수 에폭시간의 경우보다 낮게 나타났다. CNT-에폭시 나노복합재료는 순수 에폭시보다 더 큰 소수성을 보여 주었다. 열역학적인 접착일은 계면전단강도와 대략 비례적인 관계를 보여주지만, 겉보기 강성도는 접착일과는 반비례를 나타내었다. 요구되는 물성에 따라서, 최대조건 대신에 최적의 산처리 조건이 필요로 할 것이다.

• 한국터널지하공간학회 논문집
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• 제10권1호
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• pp.69-79
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• 2008

터널 막장 전방의 암반 물성 변화의 예측은 터널 시공 시 붕괴를 막을 수 있는 중요한 요소이다. 본 연구에서는 표면파에 대한 웨이블렛 변환을 이용한 모형 암반의 위상속도를 예측하는 비파괴 시험법을 제안함으로써 터널 막장 전방의 암반 물성 변화를 예측하고자 한다. 실내 실험에서는 암반을 모사하기 위하여 강도가 각각 틀린 두 층으로 이루어진 석고 모형을 사용하였다. 가진윈은 진동 발생 가능한 주파수 대역이 150 Hz에서 5 kHz인 액츄에이터를 사용하였으며, 감지기는 두 개의 가속도계가 사용되었다. 분산곡선을 계산하기 위하여 웨이블렛 변환 해석을 수행하였다. 실내 실험 결과, 근접장 효과를 없애기 위한 최소 감지기 간격이 탐측 가능 깊이의 3배 이상으로 나타났다. 정규 분포 곡선에 기초한 가중치를 이용한 간단한 역산을 제안하였고, 파장 반영계수가 0.2일 때 예측치와 실측치가 잘 일치하였다. 표면파의 전파 깊이는 파장의 $0.42{\sim}0.63$배로 나타났으며, 분산곡선에서 파장에 따라 위상속도가 변하는 구간이 역산을 통해 계산된 구간과 잘 일치하였다. 표면파에 대한 웨이블렛 변환을 이용한 위상속도의 예측은 기존의 표면파 시험법에 비해 실험 구성 및 실험 방법, 역산과정이 간단하므로 터널 막장 전방의 암반 물성 변화를 예측하는데 효율적인 적용이 가능할 것으로 판단된다.

• Asian-Australasian Journal of Animal Sciences
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• 제15권8호
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• pp.1085-1090
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• 2002

Genetic parameters for birth weights (BWT), calving ease scores observed from calves born by heifers (CEH), and calving ease scores observed from calves born by cows (CEC) were estimated using Bayesian methodology with Gibbs sampling in different threshold animal models. Data consisted of 77,458 records for calving ease scores and birth weights in Gelbvieh cattle. Gibbs samplers were used to obtain the parameters of interest for the categorical traits in two univariate threshold animal models, a bivariate threshold animal model, and a three-trait linear-threshold animal model. Samples of heritabilities and genetic correlations were calculated from the posterior means of dispersion parameters. In a univariate threshold animal model with CEH (model 1), the posterior means of heritabilities for calving ease was 0.35 for direct genetic effects and 0.18 for maternal genetic effects. In the other univariate threshold model with CEC (model 2), the posterior means of heritabilities of CEC was 0.28 for direct genetic effects and 0.18 for maternal genetic effects. In a bivariate threshold model with CEH and CEC (model 3), heritability estimates were similar to those in unvariate threshold models. In this model, genetic correlation between heifer calving ease and cow calving ease was 0.89 and 0.87 for direct genetic effect and maternal genetic effects, respectively. In a three-trait animal model, which contained two categorical traits (CEH and CEC) and one continuous trait (BWT) (model 4), heritability estimates of CEH and CEC for direct (maternal) genetic effects were 0.40 (0.23) and 0.23 (0.13), respectively. In this model, genetic correlation estimates between CEH and CEC were 0.89 and 0.66 for direct genetic effects and maternal effects, respectively. These estimates were greater than estimates between BWT and CEH (0.82 and 0.34) or BWT and CEC (0.85 and 0.26). This result indicates that CEH and CEC should be high correlated rather than estimates between calving ease and birth weight. Genetic correlation estimates between direct genetic effects and maternal effects were -0.29, -0.31 and 0.15 for BWT, CEH and CEC, respectively. Correlation for permanent environmental effects between BWT and CEC was -0.83 in model 4. This study can provide genetic evaluation for calving ease with other continuous traits jointly with assuming that calving ease from first calving was a same trait to calving ease from later parities calving. Further researches for reliability of dispersion parameters would be needed even if the more correlated traits would be concerned in the model, the higher reliability could be obtained, especially on threshold model with property that categorical traits have little information.

• 한국대기환경학회지
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• 제33권1호
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• pp.31-44
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• 2017

The aim of this study is to evaluate the accuracy and variability of the oak pollen concentrations over the Seoul metropolitan region (SMR) simulated by the Community Multiscale Air Quality (CMAQ)-based pollen dispersion model, which is the CMAQ-pollen model integrated with the improved oak pollen emission model(PEM-oak). The PEM-oak model developed is based on hourly emission flux parameterization that includes the effects of plant-specific release, meteorological adjustment, and diurnal variations of oak pollen concentrations. A 33 day-run for oak pollen simulation was conducted by the CMAQ-pollen model with a 3 km spatial resolution for the SMR during the 2014 spring pollen season. Modeled concentrations were evaluated against the hourly measurements at three Burkard sampling sites. Temporal variations of oak concentrations were largely well represented by the model, but the quantitative difference between simulations and measurements was found to be significant in some periods. The model results also showed that large variations in oak pollen concentrations existed in time and space and high concentrations in the SMR were closely associated with the regional transport under strong wind condition. This study showed the effective application of the CMAQ-pollen modeling system to simulate oak pollen concentration in the SMR. Our results could be helpful in providing information on allergenic pollen exposure. Further efforts are needed to further understand the oak pollen release characteristics such as interannual variation of the oak pollen productivity and its spatio-temporal flowering timing.

• 한국건축시공학회지
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• 제11권6호
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• pp.530-537
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• 2011

연구는 SHCC의 건축시공 현장적용을 목적으로 현장 제조설비인 배치플랜트 2-Shaft 믹서를 이용하여 SHCC 제조 및 타설을 통해 실부재 실험을 실시하고, 이를 실내실험 결과와 비교 검토함으로서 향후 SHCC의 현장적용을 위한 기초자료로 제시하고자 하였다. 그 결과, 실내 Omni 믹서와 2-Shaft 믹서에서 SHCC 제조시 인장강도는 유사하였지만, 변형률에서 Omni 믹서가 2.5 % 이상 우수하였다. 배치플랜트 3500 L 2-Shaft 믹서에서 제조된 SHCC의 경우, 실내 100 L 2-Shaft 믹서에서 제조한 SHCC에서 인장 성능이 보다 높게 나타났다. SHCC의 현장적용 확대를 위해서는 배치플랜트 현장 제조시 건비빔, 모르타르 비빔시간을 충분히하여 매트릭스를 균질성을 확보하고, 비빔단계에서 적절한 점성 및 유동성을 확보할 수 있는 다양한 방법을 고려해야 한다.