• Applied Microscopy
• /
• v.44 no.2
• /
• pp.74-78
• /
• 2014

Dislocation density and distribution in epitaxial GaAs layer on Si are evaluated quantitatively and effectively using image processing of transmission electron microscopy image. In order to evaluate dislocation density and distribution, three methods are introduced based on line-intercept, line-length measurement and our coding with line-scanning method. Our coding method based on line-scanning is used to detect the dislocations line-by-line effectively by sweeping a thin line with the width of one pixel. The proposed method has advances in the evaluation of dislocation density and distribution. Dislocations can be detected automatically and continuously by a sweeping line in the code. Variation of dislocation density in epitaxial GaAs films can be precisely analyzed along the growth direction on the film.

• Transactions of Materials Processing
• /
• v.30 no.5
• /
• pp.226-235
• /
• 2021

The strain aging behavior of a low carbon dual phase steel was examined in two conditions: representing room temperature strain aging (100 ℃ × 1 hr after 7.5 % prestrain) and bake hardening process (170 ℃ × 20 min after 2 % prestrain), basing on carbon effective diffusion and dislocation distribution. The first principle calculations revealed that (Mn or Cr)-vacancy-C complexes exhibit the strongest attractive interaction compared to other complexes, therefore, act as strong trapping sites for carbon. For room temperature strain aging condition, the carbon effective diffusion distance is smaller than the dislocation distance in the high dislocation density region near ferrite/martensite interfaces as well as ferrite interior considering the carbon trapping effect of the (Mn or Cr)-vacancy-C complexes, implying ineffective Cottrell atmosphere formation. Under bake hardening condition, the carbon effective diffusion distance is larger compared to the dislocation distance in both regions. Therefore, formation of the Cottrell atmosphere is relatively easy resulting in to a relatively large increase in yield strength under bake hardening condition.

• Journal of the Korean Ceramic Society
• /
• v.27 no.4
• /
• pp.447-456
• /
• 1990

ZnWO4 single crystals were grown by Czochralski method. And the orientation of grown crystals were determined by Laue back reflection, and the crystals were siliced at (100), (010), (001) face before polishing. The morphologys and distribution of etch pits on each face were observed by optical microscopy. In the present study, we understood that dislocation distributjioon rely on shape of solid-liquid interface, and secondary phase acts on the dislocation source. We also observed dislocation trace(etch pits) of (100) slip plane on (010) cleavage plane.

• Journal of Ocean Engineering and Technology
• /
• v.4 no.2
• /
• pp.262-262
• /
• 1990

In order to check the effect of dislocation behavior on creep rate in 12% Chromium steel, 14 samples of different compositions were examined by creep rupture test, and subgrain sizes, distribution of dislocations and precipitates were checked. And, authors reviewed the behaviors of dislocations, the formation and growth of subgrains and precipitates during creep. The results are as the following: 1) Creep rates calculated by .epsilon. over dot = .rho.bv show 10-15% higher values than actual data measured. However, authors conclude that the density and velocity of dislocations together with subgrain size are important factors governing deformation during creep in 12% chromium steel. 2) The values of the strength of obstacles in the mobility of dislocations are more clearly depended on the effective stress in the range of $10{\pm}5kgf/mm^{2}$ and increase with the increase of temperature. 3) Creep rates decrease with the smaller sizes of subgrains formed and can result in the longer creep rupture lives(hours). The smaller subgrains can be made by forming shorter free gliding distances of dislocations with very fine precipitates formed in the matrix during creep by applying proper alloy design. 4) Dislocation mobility gets hindered by precipitates occurring, which are coarsened by the softening process governed by diffusion during long time creep.

• Journal of Ocean Engineering and Technology
• /
• v.4 no.2
• /
• pp.112-120
• /
• 1990

In order to check the effect of dislocation behavior on creep rate in 12% Chromium steel, 14 samples of different compositions were examined by creep rupture test, and subgrain sizes, distribution of dislocations and precipitates were checked. And, authors reviewed the behaviors of dislocations, the formation and growth of subgrains and precipitates during creep. The results are as the following: 1) Creep rates calculated by .epsilon. over dot = .rho.bv show 10-15% higher values than actual data measured. However, authors conclude that the density and velocity of dislocations together with subgrain size are important factors governing deformation during creep in 12% chromium steel. 2) The values of the strength of obstacles in the mobility of dislocations are more clearly depended on the effective stress in the range of $10{\pm}5kgf/mm^{2}$ and increase with the increase of temperature. 3) Creep rates decrease with the smaller sizes of subgrains formed and can result in the longer creep rupture lives(hours). The smaller subgrains can be made by forming shorter free gliding distances of dislocations with very fine precipitates formed in the matrix during creep by applying proper alloy design. 4) Dislocation mobility gets hindered by precipitates occurring, which are coarsened by the softening process governed by diffusion during long time creep.

• The Journal of Engineering Geology
• /
• v.16 no.2 s.48
• /
• pp.179-187
• /
• 2006

Two specimens of mortar containing artificial slit and Geochang granite containing the straight notch were selected to be used in this research. Source mechanism of micro-crack by radiation pattern based on dislocation the-ory was estimated by the first motion of longitudinal wave and spatial distribution between the location of transducers for monitoring acoustic emission and source coordinates determined by the application of the least square method. Result of analysis showed that the orientation of dislocation surfaces due to shear dislocation and tensile dislocation squares considerably with crack direction visually observed. The ultimate goal of this study is to provide fundamental information for source mechanism of micro-crack within materials.

• Advances in materials Research
• /
• v.4 no.1
• /
• pp.1-12
• /
• 2015

Low carbon steel of composition 0.05C - 0.18 Mn - 0.012 Si is intercritically annealed at temperatures $750^{\circ}C$, $775^{\circ}C$ and $800^{\circ}C$. The equilibrated alloys of different amounts of austenite with varying carbon contents are quenched in iced water. The same alloys are subcritically annealed at $675^{\circ}C$ and $700^{\circ}C$ for varying periods of times; the subcritically annealed alloy samples are quenched in iced water. Optical, scanning electron and transmission electron microscopy are carried out for all the samples. The dislocation structure, its distribution and density present in the above prepared duplex ferrite martensite steels are studied. The martensites are found to be highly dislocated due to lattice invariant deformation. At the same time ferrite adjoining the martensite areas also exhibits quite a high dislocation density. The high dislocation density is favorable for strain ageing and hence bakes hardenability. EDS analyses were carried out for both martensite and ferrite phases; it is found that the degree of supersaturation in ferrite together with carbon content in martensite varies with the process parameters. The microhardness test results show that the hardness values of different phases differ appreciably with process parameters. The microstructures and the corresponding microanalyses reveal that differently processed steels contain phases of varying compositions and different distribution.

• Structural Engineering and Mechanics
• /
• v.86 no.4
• /
• pp.535-546
• /
• 2023

In the present paper, multiple interface cracks between a functionally graded orthotropic coating and an orthotropic half-plane substrate under concentrated loading are considered by means of the distribution dislocation technique (DDT). With the use of integration of Fourier transform the problem is reduced to a system of Cauchy-type singular integral equations which are solved numerically to compute the dislocation density on the surfaces of the cracks. The distribution dislocation is a powerful method to calculate accurate solutions to plane crack problems, especially this method is very good to find SIFs for multiple unequal cracks located at the interface. Hence this technique allows considering any number of interface cracks. The primary objective of this paper is to investigate the effects of the interaction of multiple interface cracks, load location, material orthotropy, nonhomogeneity parameters and geometry parameters on the modes I and II SIFs. Numerical results show that modes I/II SIFs decrease with increasing the nonhomogeneity parameter and the highest magnitude of SIF occurs where distances between the load location and crack tips are minimal.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.9 no.1
• /
• pp.10-17
• /
• 1985

A new method is suggested for the solution of plane elasticity problems. With use of the dislocation model in the crack problems, the basic scheme of this method is to find equilibrium Burgers vectors of dislocations which are distributed along the boundary of the first fundamental boundary value problems. The stress distribution in the region can be found by superposition of the contributions of each dislocation. The method is applied to three cases with known analytical solutions, and to a V-notched specimen under uniaxial tension. The numerical results are compared with other available solutions. This method is effective and simple in its use, compared with other numerical methods. The method also provides very accurate solutions in the region except near the boundary where the discretization error is significant. The extrapolation method is suggested for the stresses in the boundary region. Extensive application are also suggested for a general estimate of the computational efficiency of the method.

• Journal of the Korean Society for Heat Treatment
• /
• v.10 no.2
• /
• pp.81-92
• /
• 1997

The effect of alloying elements, precipitate size, its distribution, and dislocation substructure resulted from warm rolling or cold rolling in the superplastic Al-Mg alloy system was investigated. One of the major requirements for fine structure superplasticity is that the grain size should be very small. Fine grain structure is controlled by the dislocation substructure and the dynamic recrystallization during hot or warm working. The recovery of Al-Mg base alloys was constrained resulting in relatively high dislocation density when the alloys were warm rolled. In particular, Al-Mg-Zr alloy exhibited the smallest sub-grain size among Al-Mg alloys containing Mn, Cu, Zr as a third element. The Al-Mg-Mn alloy cold rolled 80% after hot rolling showed the maximun strain rate sensitivity exponent, m, of 0.75 under strain rate of $7.1{\times}10^{-4}/s$ at $500^{\circ}C$. The elongation of the alloys was limited in spite of high m values due to large dispersoids containing appreciable amount of Fe impurities.