• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.352-355
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• 2007

Polycrystalline materials such as steels(BCC) and aluminum alloys(FCC) show the strain hardening and the strain rate hardening during the plastic deformation. The strain hardening is induced by deformation resistance of dislocation glide on some crystallographic systems and increase of the dislocation density on grain boundaries or inner grain. However, the phenomenon of the strain rate hardening is not demonstrated distinctly. In this paper, tensile tests for various strain rates are performed in the rage of $10^{-2}$ to $10^2s^{-1}$ then, specimens are extracted on the same strain position to investigate the microscopic behavior of deformed materials. The extracted specimen is investigated by using the electron backscattered diffraction(EBSD) and transmission electron microscopy(TEM) results which contain grain size, grain shape, aspect ratio and dislocation substructure.

• Journal of the Korean Society of Hazard Mitigation
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• v.11 no.2
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• pp.39-44
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• 2011

Plastic gradient from geometrically necessary dislocation(GND) can strongly affect micro-scale plastic behavior of polycrystalline solids. In this research, mechanical behavior of polycrystalline solid is investigated using the finite element method incorporating plastic gradient from GND effect. Gradient hardness coefficient and material length parameter are used to evaluate the effect of the plastic gradient on the behavior of materials. Sensitivity of the modeling parameters on the plastic gradient from GND is presented and effects of plastic gradient and material parameters on the behavior of single crystal inside a polycrystalline aggregate are investigated. It is confirmed that the plastic gradient from GND amplifies hardening response of polycrystals and affects single crystal behavior embedded in polycrystalline solids.

• Korean Journal of Materials Research
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• v.26 no.4
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• pp.167-172
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• 2016

The high temperature deformation behavior of $Ni_3Al$ and $Ni_3(Al,Mo)$ single crystals that were oriented near <112> was investigated at low strain rates in the temperature range above the flow stress peak temperature. Three types of behavior were found under the present experimental conditions. In the relatively high strain rate region, the strain rate dependence of the flow stress is small, and the deformation may be controlled by the dislocation glide mainly on the {001} slip plane in both crystals. At low strain rates, the octahedral glide is still active in $Ni_3Al$ above the peak temperature, but the active slip system in $Ni_3(Al,Mo)$ changes from octahedral glide to cube glide at the peak temperature. These results suggest that the deformation rate controlling mechanism of $Ni_3Al$ is viscous glide of dislocations by the <110>{111} slip, whereas that of $Ni_3(Al,Mo)$ is a recovery process of dislocation climb in the substructures formed by the <110>{001} slip. The results of TEM observation show that the characteristics of dislocation structures are uniform distribution in $Ni_3Al$ and subboundary formation in $Ni_3(Al,Mo)$. Activation energies for deformation in $Ni_3Al$ and $Ni_3(Al,Mo)$ were obtained in the low strain rate region. The values of the activation energy are 360 kJ/mol for $Ni_3Al$ and 300 kJ/mol for $Ni_3(Al,Mo)$.

• Journal of the Computational Structural Engineering Institute of Korea
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• v.24 no.2
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• pp.185-191
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• 2011

Plastic gradient from geometrically necessary dislocation(GND) can affect material behavior significantly. In this research, mechanical behavior of polycrystalline solid is investigated using the finite element method incorporating plastic gradient from long range dislocation or GND effect. Plastic gradient effect is implemented in the analysis model by considering a long range strain term as well as elastic and plastic terms in the multiplicative decomposition. In the model, gradient hardness coefficient and length parameter are used to evaluate the effect of the long range strains and sensitive study is conducted for the parameters. It is confirmed that the GND amplifies hardening response of polycrystals compared with the single crystal.

• Transactions of Materials Processing
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• v.15 no.6 s.87
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• pp.441-444
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• 2006

The deformation behavior of copper during equal channel angular pressing(ECAP) was calculated using a three-dimensional version of a constitutive model based on the dislocation density evolution. Finite element simulations of the variation of the dislocation density and the dislocation cell size with the number of ECAP passes are reported. The calculated stress, strain and cell size are compared with the experimental data for Cu deformed by ECAP in a modified Route C regime. The results of FEM analysis were found to be in good agreement with the experiments. After a rapid initial decrease down to about 200nm in the first ECAP pass, the average cell size was found to change little with further passes. Similarly, the strength increased steeply after the first pass, but tended to saturate with further pressings. The FEM simulations also showed strain non-uniformities and the dependence of the resulting strength on the location within the workpiece.

• Korean Journal of Metals and Materials
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• v.47 no.11
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• pp.699-706
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• 2009

Deformation behavior of pure aluminum during equal channel angular pressing (ECAP) was simulated using a three-dimensional version of the finite element method in conjunction with a constitutive model based on the dislocation density and cell evolution. The three-dimensional finite element analyses for the prediction of microstructural features, such as the variation of the dislocation density and the cell size with the number of ECAP, are reported. The calculated stress and strain and their distributions are also investigated for the route Bc ECAP processed pure aluminum. The results of finite element analyses are found to be in good agreement with experimental results for the dislocation cell size. Due to the accumulation of strain throughout the workpiece and an overall trend to saturation in cell size, a decrease of the difference in cell size with the number of passes (1~4) was predicted.

• Journal of Mechanical Science and Technology
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• v.20 no.8
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• pp.1209-1216
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• 2006

An AZ31 magnesium alloy was tested at constant temperatures ranging from 423 to 473 K (0.46 to 0.51 Tm) under constant stresses. All of the creep curves exhibited two types depending on stress levels. At low stress (${\sigma}/ G < 4 {\times}10^{-3}$), the creep curve was typical of class A (Alloy type) behavior. However, at high stresses (${\sigma}/ G > 4 {\times}10^{-3}$), the creep curve was typical of class M (Metal type) behavior. At low stress level, the stress exponent for the steady-state creep rate was of 3.5 and the true activation energy for creep was 101 kJ/mole which is close to that for solute diffusion. It indicates that the dominant deformation mechanism was glide-controlled dislocation creep. At low stress level where n=3.5, the present results are in good agreement with the prediction of Fridel model.

• Journal of the Korean Society for Nondestructive Testing
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• v.31 no.1
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• pp.32-39
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• 2011

The object of this study is to evaluate and discriminate nondestructively the dislocation substructures of Cu and Cu-Zn alloy subjected to the low-cycle-fatigue. The ultrasonic wave velocity, electrical resistivity and positron annhilation lifetime(PAL) were measured to the nondestructive testing. Cyclic fatigue test of Cu and Cu-Zn alloy with much different stacking fault energies was conducted and the correlations between dislocation behavior and nondestructive parameters were studied. Dislocation cell substructure was developed in Cu, while planar array of dislocation structure was developed in Cu-35Zn alloy only increasing dislocation density with fatigue cycles. Decrease in ultrasonic wave velocity, increase in electrical resistivity and PAL were shown because of the development of lattice defects, dislocations and vacancies, by cyclic fatigue at room temperature. In contrast to Cu-Zn alloy of the planar-array dislocation substructure showing continuous changes in the nondestructive parameters, it does not make any noticeable changes in the nondestructive parameters after the evolution of dislocation cell substructure in Cu.

• Korean Journal of Materials Research
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• v.25 no.2
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• pp.81-89
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• 2015

A strain-gradient crystal plasticity constitutive model was developed in order to predict the Hall-Petch behavior of a Ni-base polycrystalline superalloy. The constitutive model involves statistically stored dislocation and geometrically necessary dislocation densities, which were incorporated into the Bailey-Hirsch type flow stress equation with six strength interaction coefficients. A strain-gradient term (called slip-system lattice incompatibility) developed by Acharya was used to calculate the geometrically necessary dislocation density. The description of Kocks-Argon-Ashby type thermally activated strain rate was also used to represent the shear rate of an individual slip system. The constitutive model was implemented in a user material subroutine for crystal plasticity finite element method simulations. The grain size dependence of the flow stress (viz., the Hall-Petch behavior) was predicted for a Ni-base polycrystalline superalloy NIMONIC PE16. Simulation results showed that the present constitutive model fairly reasonably predicts 0.2%-offset yield stresses in a limited range of the grain size.

• Journal of the Korean Society for Heat Treatment
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• v.23 no.3
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• pp.131-136
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• 2010

The LCF (low cycle fatigue) behavior and the serration phenomena in the plastically deformed and non-deformed 5052 Al alloy were investigated. The plastic deformation was performed by 1 pass or 4 passes in ECAP (equal channel angular pressing) followed by annealing. Only cyclic hardening continued from the beginning until fracture at all strain amplitudes during LCF in the non-deformed alloy, which was caused by the increase in dislocation density during fatigue. Slight cyclic hardening followed by plateau until fracture was observed during LCF in the ECAPed alloy, which was caused by the slight increase in dislocation density in the beginning and then keeping constant in dislocation density afterward until fracture by forming subgrains in this stage of fatigue. The serrations on the stress-strain curves of this alloy were observed, which indicate that the dynamic strain aging (DSA) is occurring during plastic deformation. The variation in amplitudes of serration was studied by changing the strain rate in tensile or fatigue tests.